ANALÍTICAS SEPARATIVAS

EN EL SECTOR

Organizado por:

ORGANIZACIÓN

Dr. Antonio L. Crego. Profesor Titular de Universidad.

Dpto. de Química Analítica. Universidad de Alcalá.

Dr. José Luis Novella. Director Técnico. Planta Piloto de

Química Fina. Universidad de Alcalá.

LUGAR DE IMPARTICIÓN

PLANTA PILOTO DE QUIMICA FINA

Campus Universitario

Carretera Madrid-Barcelona, km. 33,6.

28871 Alcalá de Henares. Madrid

Tel.: 91 885 50 68. Fax: 91 885 50 57.

http://www.ppqf.net

CALENDARIO CLASES TEÓRICAS Y

HORARIO

PLAZAS MÁXIMAS Y PRECIOPrecio: 6000.- €. + Gastos de matrículaNúmero máximo de alumnos: 12

SECRETARIA E INFORMACIÓNFundación General de la Universidad de Alcalá

Departamento de Formación y Congresos

c/ Imagen, 1 y 3. 28801 Alcalá de Henares. Madrid

Tel.: 91 879 74 30 - Fax: 91 879 74 55

E-mail: cursos@fgua.es; WEB: www.fgua.es

tríptico v8:Maquetación 1 07/04/2011 13:36 Página 1

14 de Enero 2013 al 1 de Julio 2013

MÁSTER EN TÉCNICAS

De Lunes a Viernes de 16 h a 20:15 h

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Prácticas de empresa: 15 de Abril al 14 de Junio de 2013

PROFESORADO

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Director del Máster:

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Entrega del Proyecto Fin de Máster: 1 de Julio de 2013

Del 14 de Enero al 5 de Abril de 2013

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Subdirector del Máster:

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QUÍMICO-FARMACÉUTICO

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Dra. CONCEPCION ALONSO. - Profesora Titular de Matemáticas Aplicada de la UAH.Dra. CORAL BARBAS. - Catedrática de Química Analítica de San Pablo CEU.Dra. FLOR CASTRO. - Investigador en la PPQF de la UAH.

Dr. ALBERTO ESCARPA. - Profesor Titular de Química Analítica de la UAH.Dr. ALFONSO ESPADA. - Investigador Sénior en los laboratorios LILLY.Dra. SONSOLES ESPINOSA. - Jefe de Control de Calidad en los laboratorios NORMON.Dra. MERCEDES de FRUTOS. - Investigador Científico del CSIC.Dra. Mª ANGELES GARCIA. - Profesora Titular de Química Analítica de la UAH.Dra. CONCEPCION GARCIA. - Profesora Titular de Química Analítica de la UAH.Dra. BELEN GOMARA. - Científico Titular del CSIC.Dr. PEDRO GUTIERREZ. - Especialista de producto en SIGMA-ALDRICH.

Dr. ANTONIO L. CREGO. - Profesor Titular de Química Analítica de la UAH.

Dr. JOSE LUIS NOVELLA. - Director Técnico de la PPQF de la UAH.Dra. LEONOR NOZAL. - Responsable de la Unidad de Análisis y Control en la PPQF de la UAH.Dra. Mª LUZ de la PUENTE. - Investigador Sénior en los laboratorios LILLY.Dra. Mª PAZ SAN ANDRES. - Profesora Titular de Química Analítica de la UAH.Dra. CAROLINA SIMO. - Científico Titular del CSIC.D. ALFONSO VEGA. - Jefe de laboratorio en la Policía Científica de Madrid.

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PRÁCTICAS

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Se dotará de Becas a los inscritos

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OBJETIVOS FORMATIVOS DEL MÁSTER

DIRIGIDO A

PROGRAMA

tríptico v8:Maquetación 1 07/04/2011 13:36 Página 2

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COMPETENCIAS A ADQUIRIR POR

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EL ESTUDIANTE

El Máster va dirigido a licenciados o graduados en Química, Farmacia o Biología que requieran de las técnicas analíticas de separación acopladas o no a espectrometría de masas para el desarrollo de su profesión.

INAUGURACIÓN DEL MÁSTER- Presentacion del máster.- Conferencia Inaugural.

Legislación aplicable al sector farmacéutico.

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Trazabilidad en los laboratorios analíticos.Gestión de calidad en los laboratorios analíticos.Laboratorio de Control de Calidad

en la Industria Farmacéutica.

CLAUSURA DEL MÁSTER- Conferencia de Clausura.

La importancia de la Espectrometria de Masasen el Laboratorio Farmacéutico.

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1. Toma y Preparación de la muestra para el Análisis

2. La Cromatografía de Líquidos

3. Otras Técnicas de Separación

4. Hibridación Instrumental: Espectrometría de Masas yTécnicas de Separación

5. Control de Calidad en la Industria Farmacéutica

3.1. Cromatografía de gases

3.2. Electroforesis Capilar

5.1. Herramientas estadísticas para el tratamiento de datos

5.2. Control de Calidad

SEMINARIO 7: Calibración Metodológica.

SEMINARIO 6: Diseño de experimentos.

SEMINARIO 5: Contrastes de significación.

SEMINARIO 4: Desarrollo de métodos.SEMINARIO 3: Cálculos de parámetros fundamentales.

SEMINARIO 2: Aplicación de diferentes técnicas de extracción.

SEMINARIO 1: Ejemplos prácticos.

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El objetivo es la especialización en el manejo de las técnicasanalíticas de separación, sin y con espectrometría de masas, con el fin de actualizar la formación académica y atender a las demandas sociales que requiere el mercado laboral, proporcionando al estudiante los conocimientos y experienciapráctica necesaria para considerarse un experto en el manejoy diseño de las complejas metodologías de separación y de espectrometría de masas, estrategias imprescindibles en todolaboratorio de análisis en el sector químico y farmacéutico.

Adquirir los conocimientos teóricos y prácticos necesarios paraseleccionar, planificar y aplicar las metodologías de separaciónmás adecuadas para resolver problemas químico-analíticos deinterés en los laboratorios del sector químico y farmacéutico.Comprender y saber utilizar las herramientas estadísticas básicas empleadas en el tratamiento de datos analíticos obtenidos. Adquirir los conocimientos básicos para el mantenimiento y verificación de los equipos utilizados. Saber utilizar las etapas necesarias para la validación de los métodos desarrollados.

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- Toma de muestra. Representatividad. Estabilidad.

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- Intoducción.

- Técnicas de Extracción.

- Intoducción.

CONFERENCIA 1: Tratamientos de muestra previos a

la separación cromatográfica.

- Descripción del cromatógrafo de líquidos.- Columnas.- Modos de separación.- Desarrollo de métodos con elución isocrática y en gradiente.- Análisis de biomoléculas.- Análisis quiral.- Escalado de cromatografía analítica a preparativa.

CONFERENCIA 2: Métodos ortogonales en el laboratorio farmacéutico.CONFERENCIA 3: Cromatografía de Afinidad en laboratorio farmacéutico.

- Introducción.- Descripción del cromatógrafo.- Columnas.- Derivatización.- Desarrollo de métodos.- Resolución de problemas.

- Introducción.- Descripción de un equipo de Electroforesis Capilar.- Modos de separación.- Desarrollo de métodos.- Resolución de problemas.

CONFERENCIA 4: Determinación de disolventes residualesen la industria farmacéutica.

CONFERENCIA 5: Separaciones de compuestos quiralesen la industria farmacéutica.

- Introducción.- Componentes básicos de un espectrómetro de masas.- Propiedades generales de los acoplamientos.- Espectrometría de Masas en Tándem.- Desarrollo de métodos GC/MS.- Desarrollo de métodos CE/MS.- Desarrollo de métodos LC/MS.- Interpretación de espectros de masas.

- Introducción a la Quimiometría y Estadística descriptiva.

- Introducción al Diseño de Experimentos.- Contrastes de significación.

- Farmacopeas y líneas guía ICH.- Cualificación de un método previo al análisis.- Calibración metodológica.- Validación de Métodos Analíticos según ICH Q2.

CONFERENCIA 6:CONFERENCIA 7:CONFERENCIA 7:

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