LABORATORIO DE CARACTERIZACIÓN DE MATERIALES · LABORATORIO DE CARACTERIZACIÓN DE MATERIALES...
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LABORATORIO DE CARACTERIZACIÓN DE MATERIALES Página 1 de 3 Measurement Conditions: Dataset Name M1 Scan Axis Gonio Start Position [°2Th.] 4.0140 End Position [°2Th.] 69.9890 Step Size [°2Th.] 0.0130 Scan Step Time [s] 1.0000 Measurement Temperature [°C] 25.00 Anode Material Cu K-Alpha1 [Å] 1.54060 Generator Settings 40 mA, 45 kV Goniometer Radius [mm] 240.00 Spinning Yes Main Graphics, Analyze View: Position [°2Theta] (Copper (Cu)) 10 20 30 40 50 60 Counts 0 500 1000 1500 M1 Illite-2M2 (NR) (00-043-0685) Kaolinite-1A (01-078-1996) Muscovite-1M, magnesian (01-078-1928) Quartz, syn (01-085-0798) Hematite, syn (01-089-0599)
Transcript of LABORATORIO DE CARACTERIZACIÓN DE MATERIALES · LABORATORIO DE CARACTERIZACIÓN DE MATERIALES...
LABORATORIO DE CARACTERIZACIÓN DE MATERIALES
Página 1 de 3
Measurement Conditions: Dataset Name M1 Scan Axis Gonio Start Position [°2Th.] 4.0140 End Position [°2Th.] 69.9890 Step Size [°2Th.] 0.0130 Scan Step Time [s] 1.0000 Measurement Temperature [°C] 25.00 Anode Material Cu K-Alpha1 [Å] 1.54060 Generator Settings 40 mA, 45 kV Goniometer Radius [mm] 240.00 Spinning Yes Main Graphics, Analyze View:
Position [°2Theta] (Copper (Cu))
10 20 30 40 50 60
Counts
0
500
1000
1500
M1
Illite-2M2 (NR) (00-043-0685)
Kaolinite-1A (01-078-1996)
Muscovite-1M, magnesian (01-078-1928)
Quartz, syn (01-085-0798)
Hematite, syn (01-089-0599)
LABORATORIO DE CARACTERIZACIÓN DE MATERIALES
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Pattern List: Ref. Code Compound Name Chemical Formula 01-078-1996 Kaolinite-1A Al2 ( Si2 O5 ) ( O H )4 01-085-0798 Quartz, syn Si O2 01-078-1928 Muscovite-1M, magnesian ( K0.80 Na0.02 Ca0.01 ) ( Al1.66 Fe0.06 Fe0.02
Mg0.28) (Si3.41 Al0.59) O10 ( O H )2 01-089-0599 á-Fe2 O3, iron(III) oxide Fe2 O3 00-043-0685 Illite-2M2 (NR) K Al2 ( Si3 Al ) O10 ( O H )2
Peak List: Pos. [°2Th.] FWHM [°2Th.] d-spacing [Å] Area [cts*°2Th.] Height [cts]
8.8199 0.2184 10.01795 100.23 344.18 12.2590 0.4992 7.21417 1114.89 1675.01 17.7159 0.4992 5.00241 70.42 105.80 19.8345 0.2496 4.47261 147.11 442.03 20.3618 0.4001 4.35796 117.91 294.69 20.8238 0.2046 4.26231 49.99 244.30 21.2469 0.6439 4.17838 89.67 139.26 22.8640 0.0900 3.88638 6.50 72.20 24.9341 0.5304 3.56821 588.14 831.65 26.6105 0.2184 3.34711 414.96 1425.00 29.0909 0.3120 3.06712 27.12 65.20 32.9520 0.0900 2.71602 3.78 42.00 33.1983 0.7488 2.69643 40.30 40.36 33.4720 0.0900 2.67500 3.87 43.00 34.9514 0.3744 2.56508 184.67 369.93 35.3108 0.2300 2.53980 62.31 270.88 35.9562 0.3744 2.49568 121.98 244.34 36.5306 0.1872 2.45774 31.87 127.70 37.6816 0.0921 2.38527 9.16 99.40 38.3878 0.4992 2.34300 165.96 249.33 39.1695 0.1452 2.29802 24.61 169.53 39.3509 0.4992 2.28784 60.41 90.76 40.2389 0.3120 2.23938 18.29 43.98 40.9730 0.0900 2.20094 3.24 36.00 41.2590 0.0900 2.18634 6.03 67.00 42.3770 0.0900 2.13121 6.12 68.00 45.2611 0.4992 2.00188 69.82 104.89
LABORATORIO DE CARACTERIZACIÓN DE MATERIALES
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45.7582 0.0171 1.98128 2.08 121.40 50.1097 0.1872 1.81895 29.83 119.53 50.9274 0.4992 1.79165 26.71 40.12 54.2635 0.0819 1.68911 8.34 101.91 54.8310 0.0010 1.67296 0.11 109.70 59.9159 0.3744 1.54256 40.00 80.13 62.2685 0.3120 1.48981 97.66 234.76 63.8530 0.0900 1.45661 7.20 80.00 64.0740 0.0900 1.45212 4.23 47.00 64.3080 0.0900 1.44740 4.32 48.00 65.1140 0.0900 1.43141 2.88 32.00 67.4150 0.0900 1.38804 3.42 38.00 67.7270 0.0900 1.38241 3.24 36.00 68.2194 0.3744 1.37362 47.76 95.68
Atentamente,
Dr. JUAN PABLO HERNANDEZ ORTIZ Coordinador Laboratorio de Caracterización de Materiales
Muestra Santuario km 49+200 10/05/2010 03:21:09 p.m.
Spectrum processing : Peaks possibly omitted : 0.243, 2.141, 2.421 keV Processing option : All elements analyzed (Normalised) Number of iterations = 3 Standard : O SiO2 1-Jun-1999 12:00 AM Al Al2O3 1-Jun-1999 12:00 AM Si SiO2 1-Jun-1999 12:00 AM Fe Fe 1-Jun-1999 12:00 AM
Element Weight% Atomic% O K 45.52 60.01 Al K 21.98 17.18 Si K 28.22 21.19 Fe K 4.28 1.61 Totals 100.00
Cuarzo
Comment:
Muestra Santuario km 49+200
10/05/2010 03:22:15 p.m.
Spectrum processing : Peak possibly omitted : 2.154 keV Processing option : All elements analyzed (Normalised) Number of iterations = 2 Standard : O SiO2 1-Jun-1999 12:00 AM Al Al2O3 1-Jun-1999 12:00 AM Si SiO2 1-Jun-1999 12:00 AM Fe Fe 1-Jun-1999 12:00 AM
Element Weight% Atomic% O K 13.69 27.29 Al K 20.90 24.71 Si K 18.84 21.39 Fe K 46.58 26.60 Totals 100.00
Oxido de hierro
Comment:
Muestra Santuario km 49+200
10/05/2010 03:22:44 p.m.
Spectrum processing : Peak possibly omitted : 2.146 keV Processing option : All elements analyzed (Normalised) Number of iterations = 2 Standard : O SiO2 1-Jun-1999 12:00 AM Al Al2O3 1-Jun-1999 12:00 AM Si SiO2 1-Jun-1999 12:00 AM
Element Weight% Atomic% O K 31.57 44.31 Al K 29.62 24.65 Si K 38.81 31.03 Totals 100.00
Comment:
Muestra Santuario km 49+200
10/05/2010 03:30:11 p.m.
Spectrum processing : Peak possibly omitted : 2.142 keV Processing option : All elements analyzed (Normalised) Number of iterations = 2 Standard : O SiO2 1-Jun-1999 12:00 AM Al Al2O3 1-Jun-1999 12:00 AM Si SiO2 1-Jun-1999 12:00 AM
Element Weight% Atomic% O K 49.98 63.29 Al K 21.18 15.90 Si K 28.85 20.81 Totals 100.00
Cuarzo
Comment:
Muestra Santuario km 49+200
10/05/2010 03:44:43 p.m.
Spectrum processing : Peaks possibly omitted : 0.249, 2.143, 2.417 keV Processing option : All elements analyzed (Normalised) Number of iterations = 3 Standard : O SiO2 1-Jun-1999 12:00 AM Al Al2O3 1-Jun-1999 12:00 AM Si SiO2 1-Jun-1999 12:00 AM
Element Weight% Atomic% O K 50.84 64.25 Al K 12.48 9.35 Si K 36.68 26.40 Totals 100.00
Cuarzo
Comment:
Muestra Santuario km 49+200
10/05/2010 03:30:23 p.m.
Spectrum processing : Peaks possibly omitted : 0.265, 2.142, 2.410, 4.530 keV Processing option : All elements analyzed (Normalised) Number of iterations = 3 Standard : O SiO2 1-Jun-1999 12:00 AM Al Al2O3 1-Jun-1999 12:00 AM Si SiO2 1-Jun-1999 12:00 AM Fe Fe 1-Jun-1999 12:00 AM
Element Weight% Atomic% O K 53.23 67.09 Al K 19.20 14.35 Si K 24.14 17.33 Fe K 3.43 1.24 Totals 100.00
Comment:
Muestra Santuario km 49+200
10/05/2010 03:44:25 p.m.
Spectrum processing : Peak possibly omitted : 2.135 keV Processing option : All elements analyzed (Normalised) Number of iterations = 2 Standard : O SiO2 1-Jun-1999 12:00 AM Al Al2O3 1-Jun-1999 12:00 AM Si SiO2 1-Jun-1999 12:00 AM Fe Fe 1-Jun-1999 12:00 AM
Element Weight% Atomic% O K 27.48 46.21 Al K 17.08 17.02 Si K 21.15 20.25 Fe K 34.29 16.52 Totals 100.00
Oxidos de hierro y aluminio
Comment:
w (%) 19 γg = 26,97 kN/m³ Gs = 2,75 e = 1,02 n = 50,50 %
w(%)Corpos
1 48,38 40,66 40,66 0,00 0,0191 0,0179 6,7 26486,0 5,43 0,0498 0,0465 7,1 25036,9 5,41 0,02 46,62 39,18 40,35 3,00 0,0199 0,0183 8,7 19777,7 5,30 0,0518 0,0473 9,5 17711,1 5,26 2,43 50,75 42,65 46,06 8,00 0,0230 0,0182 26,4 1583,3 4,21 0,0618 0,0485 27,4 1362,4 4,14 8,124 49,78 41,83 47,27 13,00 0,0232 0,0181 28,2 1222,9 4,10 0,0612 0,0470 30,2 913,6 3,97 8,105 47,75 40,13 47,35 18,00 0,0257 0,0187 37,4 324,8 3,52 0,0638 0,0462 38,1 295,4 3,48 19,446 0,00 0,00 23,00 0,0244 0,0180 35,6 425,1 3,64 0,0637 0,0465 37,0 346,2 3,55 18,017 51,22 43,04 55,09 28,00 0,0261 0,0183 42,6 154,5 3,20 0,0301 0,0211 42,7 153,8 3,20 22,968 50,09 42,09 55,98 33,00 0,0252 0,0182 38,5 280,3 3,46 0,0359 0,0254 41,3 185,7 3,28 19,719 49,94 41,97 57,91 38,00 0,0271 0,0183 48,1 75,6 2,89 0,0397 0,0266 49,2 71,3 2,86 25,7210 49,39 41,50 59,35 43,00 0,0270 0,0179 50,8 65,9 2,83 0,0737 0,0481 53,2 58,8 2,78 26,8811 53,15 44,66 66,10 48,00 0,0409 0,0170 140,6 5,3 1,73 0,1113 0,0479 132,4 6,1 1,80 30,97
Cuerpo de
prueba
Phúmedo (g)
Pseco
(g)Pideal (g)
Westimada
(%)
ENSAYO DE SUCCIÓN
Ph (g)
Papel Filtro - Superior
Ph (g) Ps (g)Wpapel
(%)Succión
(kPa)pF
Wpapel (%)
Papel Filtro - Medio
Succión (kPa)Ps (g) pF
Para humedades de papel filtro > 47%, la succión (kPa) = 10(6.05-2.48*log w)
Para humedades de papel filtro ≤ 47%, la succión (kPa) = 10(4.84-0.0622* w)
1
10
100
1000
10000
100000
0 5 10 15 20 25 30 35
(Ua-
Uw
) (k
Pa)
w (%)
Natural matricial
Natural matricial
ANEXO 2
