Fecha de reporte: 2019-01-07 Página: Revisión:...

Destino Final:

Observaciones:

ZIRACUARETIRO

Aleatorio

EUA,EUROPA,JAPON

La muestra se recibió en condiciones para su análisis.

2303-01(SECTOR 01)

Estado: Michoacán Código postal: 60330

Ext. 133

60330

[email protected], [email protected],

[email protected], [email protected]

Información de Facturación

Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab

Fruits-Giddings SA de CV

Km. 1 Carretera los Reyes- Jacona Sn

Michoacán

Razón social:


2019-01-07 Página: 1 de 7 Revisión: AR271-TS-70

Empresa:

Correo electrónico:

Fecha de reporte:

SUN BELLE MÉXICO S.A. DE C.V.

Dirección: Km 1 Carr. los Reyes-Jacona S/N Ciudad o Localidad: Los Reyes

Solicitante: ALFREDO OSEGUERA DÍAZ


[email protected],

[email protected]

Teléfono: 3545427328

Información del Cliente

Domicilio Fiscal:

Estado:

RFC: SBM040520QN6

Ciudad o Localidad: Los Reyes

Código postal:

Analisis Multiresidual de Pesticidas

Nombre común:

Libro de registro:

Rubus Ulmifoli

ene-19P-19-177No. Reg. de Muestra:

Fecha de recepción:


Nombre científico: Variedad:

Fecha de Término:Fecha de inicio: 2019-01-04

Información de la Muestra

Zarzamora

Ext. SD Correo electrónico:


Telefono: 3545420170

2019-01-07

Menos de 1.5kg

SD

Tupy|Otras

2019-01-04

Parte analizada:

Productor:

Lugar de muestreo:

Uso comercial:

Fruto

JUAN JAVIER ALVAREZ ORTEGA

Fecha de muestreo:03 DE ENERO DEL 2018 Hora:

11:00 AM

SD

SD

Estado de la muestra:

Lugar de cosecha:

Método de muestreo:

Destino Comercial:

Cantidad recibida:

Registro SAGARPA:

RFC de Bodega:

Aduana:Mercado Nacional y Extranjero

Congelado

DIRECCION: ZIRACUARETIRO,

MICHOACÁN

Humano

Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El resultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A. de C.V. , por lo cual no se hace

responsable de la representatividad del resultado para el total del producto. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.

Este formato de interpretación esta protegido y registrado ante el Instituto Mexicano de la Propiedad Intelectual. Se prohibe su reproducción total o parcial sin autorización. El presente informe de resultados no será valido si presenta raspaduras, tachaduras o enmendaduras.

Documento controlado ISO/IEC 17025:2005

Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]

B B

B B

B B

B B

B B

B B

B BB B

B B

B BB BB BB BB B

B B

B BB BB BB BB BB BB B

B B

B BB BB BB BB B

B B

B B

B B

B B

B B

B B

B B

B BB BB B

B B

B BB B

B B

V B

B B

B B

B B

B B

B BB BB BB B

B B

B B

B B

B B

B B

B B

B B

B B

B B

OXYDEMETON

METHYL

METABOLITE

0.02

0.01 - -

0.02 0.5

- -

0.2 0.5

0.01 0.5

0.5 2

0.05 0.1

3 1

0.05 0.05

- - - -

1

- - - -

- - - -

- - - -

0.1 0.2

- - - -

0.01 1

1

0.01 0.3

0.01 1

0.05 0.1

- - - -

- - - -

0.02 - -

3 1

0.01 0.05

- - - -

- -

0.01 1

0.01 - -

0.01 - -

0.9 0.7

0.01 0.2

0.5

0.01 0.05

0.01 1

0.1 0.1

0.01 0.05

0.01 1

0.02 0.02

0.01 - -

- - - -

- -

0.01 0.05

0.05 0.05

0.01 0.1

0.01 0.05

1 1

- - - -

0.01 0.02

0.01 - -

1

0.01 0.1

0.01 - -

0.01 - -

- -

0.01 - -

0.01 0.05

20 5

0.01 0.5

THIOPHANATE

METHYL/ BENOMYL

METABOLITE

0.01

0.01

0.01

- -

0.02

0.01

0.01

7 7

0.01 0.05

1 0.3

0.01 1

0.01 0.1

- - - -

0.01 5

0.05 - -

5 3

- - - -

0.05 0.3

0.01 0.02

0.02 - -

0.01 0.02

0.01 - -

0.5

0.01 0.01

0.08 0.05

0.01 1

2 1

0.01 0.02

0.01 - -

0.02 1

0.01 0.05

- -

0.05 0.3

Carbetamide - - 0.01

- - < LCL

Chlordane- a GC/MSMS

- - < LCL

SD

CA EU

< LCL

- - < LCL

- - < LCL

- - < LCL

0.01

0.3 0.1 0.02 < LCL

0.1 0.1 0.02 0.1 0.02 < LCL

Chlorbromuron LC/MSMS

Fecha de reporte: 2019-01-07

Resultados de AnálisisSe han detectado residuos de pesticidas prohibidos

Analizado

mediante

equipo

Uso autorizado

LMR (ppm)

Reg. Sagarpa:

No. Reg. Lab.:

Cantidad obtenida en mg/kg

(ppm)MX US JP CA CHN

Cantidad obtenida en mg/kg

(ppm)Analito Analito

Analizado

mediante

equipo


AR271-TS-70Revisión:

Cliente:

Productor:

Cromatograma GC:



P-19-177 01-06-2019.D

P-19-177

US JP

1-Naphthol GC/MSMSCARBARYL

METABOLITE

CARBARYL

METABOLITE

CARBARYL

METABOLITE

Uso autorizado

LMR (ppm)

MX US JP CA CHN

CARBARYL

METABOLITECARBARYL METABOLITE < LCL Carbendazim LC/MSMS

THIOPHANATE

METHYL/ BENOMYL

METABOLITE

THIOPHANATE

METHYL/ BENOMYL

METABOLITE

THIOPHANATE

METHYL/ BENOMYL

METABOLITE

THIOPHANATE

METHYL/ BENOMYL

METABOLITE

THIOPHANATE

METHYL/ BENOMYL

METABOLITE

EU KOR EU KOR

CARBARYL

METABOLITE

CARBARYL

METABOLITE

THIOPHANATE

METHYL/ BENOMYL

METABOLITE

2,6 Dichlorobenzonitrilo GC/MSMS - - - - - - - - - - < LCL

2,3 dihydro-2,2dimethylbenzofuran 7- GC/MSMS - - - - - -

2, 4-D Methyl ester GC/MSMS 0.2 0.2 0.1 0.1 0.1 < LCL0.1 0.05

- - - -

- - - -

Abamectin LC/MSMS 0.2 0.2 0.05 0.2 - - < LCL

3-Hydroxy carbofuran LC/MSMS - - - - - -

- - - - < LCL

3,4 Dichloroaniline GC/MSMSLINURON

METABOLITE

LINURON

METABOLITE

LINURON

METABOLITE

LINURON

METABOLITELINURON METABOLITE < LCL

2,6-Dichlorobenzamide LC/MSMS - - - - - - - - - -

LINURON

METABOLITE

Aclonifen GC/MSMS - - - - 0.01 0.1 - - < LCL

Acetochlor LC/MSMS - - - -

0.1 0.50 < LCL

Acetamiprid LC/MSMS 1.6 1.6 2 4 2 < LCL

Acephate LC/MSMS - - - - 0.01

Aldicarb LC/MSMS - - - -

- -- -LC/MSMSAldicarb-sulfoxide (Aldoxicarb)

0.01

0.1 - - < LCL

Alachlor LC/MSMS - - - - 0.01 0.1 - - < LCL

Acrinathrin GC/MSMS - - - - 2

0.02 0.02

0.02 0.02

0.02 0.02

Amicarbazone LC/MSMS - - - - 0.01

0.1 - - < LCL

Ametryn GC/MSMS - - - - 0.01 0.1 - - < LCL

Ametoctradin LC/MSMS - - - - 0.01 0.05

0.01 - -

0.01 - -

Atrazine-2-hydroxy LC/MSMS - - - - - - - - - - < LCL

Atrazine GC/MSMS - - - - 0.02

Aminocarb LC/MSMS - - - - - - - - - - < LCL- - - -

0.05 - -

- - - -

Azoxystrobin GC/MSMS 5 5 5 5 - - < LCL

Azinphos-Methyl LC/MSMS - - - - 0.01

0.1 - - < LCL

Azinphos-ethyl LC/MSMS - - - - 0.01 0.1 - - < LCL

Azamethiphos LC/MSMS - - - - 0.01 0.01 - -

0.02

Benfluralin GC/MSMS - - - - 0.01 0.1 - - < LCL

Bendiocarb LC/MSMS - - - - 0.01

- - - - < LCL

Benalaxyl GC/MSMS - - - - 0.05 0.1 - - < LCL

Baycarb LC/MSMS - - - - - -

Benzoximate LC/MSMS - - - - 0.01 0.1 - - < LCL

Benthiavalicarb-isopropyl LC/MSMS - - - - 0.01

0.1 - - < LCL

Bensulide LC/MSMS - - - - 0.01 0.1 - - < LCL

Bensulfuron-methyl LC/MSMS - - - - 0.01

0.01 0.1

0.01

BHC lindane gamma GC/MSMS 0.5 0.5 0.3 0.1 - - < LCL

BHC lindane delta GC/MSMS 0.5 0.5 0.3

< LCL

BHC lindane beta GC/MSMS 0.5 0.5 0.3 0.1 - - < LCL

BHC lindane alpha GC/MSMS 0.5 0.5 0.3

0.01 0.01

0.01 0.01

0.01

Bifenthrin GC/MSMS 1 1 1

Bifenox GC/MSMS - - - - 0.01 0.1 - - < LCL

Bifenazate LC/MSMS 5 5 7

Boscalid LC/MSMS 10 10 10 6 - - < LCL

Bolstar GC/MSMS - - - - - -

Bitertanol LC/MSMS - - - - 0.05 0.1 - - < LCL

- - - -

10 9

0.1 - -

0.1

Carboxin LC/MSMS - - - -

GC/MSMS - - - - 0.01

- - < LCL

0.1 - - < LCL

0.1 - - < LCL

2 1 < LCL

0.1 - - < LCL

0.1 - - < LCL

- -

LINURON METABOLITE

- - - -

0.1 - - < LCL

- - - - < LCL

1 1 0.011

5 7 < LCL

0.1

0.1

Carbofuran GC/MSMS - - - -

0.1

- - < LCL

- - - - < LCL

Chlorpyrifos GC/MSMS - - - - 1 0.1

LC/MSMS - -

- - - - - -

0.1 - - < LCL

Chlorantraniliprole LC/MSMS 1.8 1.8 2 0.9 1 < LCL

Chinometionate GC/MSMS - - - - 0.01

- -

- - 0.01 0.1 - - < LCL

Chloroxuron LC/MSMS - - - - 0.01

0.1 - - < LCL

Chloropropylate GC/MSMS - - - - - - - - - - < LCL

Chloroneb GC/MSMS

< LCL- -0.1 0.01 - -

0.01 - -

0.01 0.05

Chlortal dimethyl GC/MSMS - - - - - - - - - - < LCL

0.1 - - < LCL

Clomazone LC/MSMS - - - - 0.02 0.1 - - < LCL

Clofentezine LC/MSMS - - - - 0.01

- - - - < LCL

Clodinafop-propargyl LC/MSMS - - - - 0.02 0.1 - - < LCL

Chlorthiophos GC/MSMS - - - - - -

0.1 0.05 < LCL

Crimidine LC/MSMS - - - - - - - - - - < LCL

Coumaphos GC/MSMS - - - - - -

0.1 - - < LCL

Clothianidin LC/MSMS - - - - 0.2 0.1 - - < LCL

Cloquintocet-mexyl LC/MSMS - - - - 0.01

0.02 - - < LCL

Cycloate LC/MSMS - - - - 0.01 0.1 - - < LCL

Cyazofamid LC/MSMS - - - - 0.01

0.1 - - < LCL

Cyantraniliprole LC/MSMS 4 4 0.01 0.1 - - < LCL

Cyanazine LC/MSMS - - - - 0.01

0.1 - - < LCL

Cyhalothrin (Isomero Lambda

y gamma)**GC/MSMS - - - - 0.5 0.01 0.2 < LCL

Cyfluthrin GC/MSMS - - - - 0.02

0.1 - - < LCL

Cyflumetofen LC/MSMS - - - - 0.01 0.1 - - < LCL

Cyflufenamid GC/MSMS - - - - 0.01

10 10 10 - - < LCL

Cyproconazole LC/MSMS - - - - 0.5

4 - - < LCL

Cypermethrin a (Zeta-

Cypermethrin)**GC/MSMS 0.8 0.8 0.5 0.1 - - < LCL

Cymoxanil LC/MSMS 4 4

0.1 - - < LCL

Cyprodinil

- - - - < LCLDDD-p,p GC/MSMS - - - - - -

0.1 - - < LCL

DDD-o,p GC/MSMS - - - - - - - - - - < LCL

Cyromazine LC/MSMS - - - - 0.01

- - - -

- - < LCL

Bupirimate LC/MSMS - - - - 0.01 0.1 - - < LCL DDE-o,p GC/MSMS - - - - - - - - - - < LCL

Buprofezin GC/MSMS - - - - 0.01 0.1 - - - - - -

- - - -1.5 - -

0.05

- - < LCL

Butocarboxim* LC/MSMS - - - - 0.01 0.1 - - < LCL DDT-p,p GC/MSMS - - - - - - - - - - < LCL

Butachlor GC/MSMS - - - - 0.01 0.1 - - < LCL

- - < LCL

Buturon LC/MSMS - - - - - - - - - - < LCL Deltamethrin GC/MSMS - - - - 0.1 0.1 - - < LCL

Butocarboxim-sulfoxide LC/MSMS - - - - 0.01 0.1 - - < LCLDEET (Diethyl-m-toluamide,

N,N-)

- -

- - < LCL

Cadusafos GC/MSMS - - - - 0.01 0.1 0.02 < LCL Demeton S GC/MSMS - - - - 0.4 0.1 0.02 < LCL

Butylate GC/MSMS - - - - 0.01 0.1 - - < LCL Demeton O

0.01 0.1

Bromacil

OXYDEMETON

METHYL

METABOLITE

OXYDEMETON

METHYL

METABOLITE

OXYDEMETON

METHYL

METABOLITE

OXYDEMETON

METHYL

METABOLITE< LCL

Carbaryl GC/MSMS 12 12 10 10 - - < LCL Desmedipham LC/MSMS - - - - 0.01 0.1 - - < LCL

Captan GC/MSMS 25 25 0.01 0.1 - - < LCL Demeton-s-methyl-sulfone

Bromuconazole* LC/MSMS - - - - 0.01 0.1 - - < LCL

Bromopropylate GC/MSMS - - - - 2

Bromophos methyl GC/MSMS - - - - - -

0.1 - - < LCL

- - - - < LCL

0.1

- -0.01 0.01

OXYDEMETON

METHYL

METABOLITE

GC/MSMS - -

GC/MSMS - -

GC/MSMS - -

< LCL DDE-p,p GC/MSMS - -

GC/MSMS 10

LC/MSMS

- - - - - -

DDT-o,p

- - - - - -

- - - - - -

- - - - - -

4

0.05

0.01

< LCL0.05

< LCL0.020.1

0.1 - - < LCL

Chlorobenzilate GC/MSMS - - - - 0.01

0.01

0.01

GC/MSMSAldrin

Carfentrazone ethyl LC/MSMS 0.1 0.1 0.1

0.01

0.1 0.02 < LCL

Aldicarb sulfone LC/MSMS - - - - 0.01 0.1 Chlormequat LC/MSMS - - - - 0.05

Chlorimuron-ethyl LC/MSMS - - - - 0.01

Chloridazon (Pyrazon) LC/MSMS - - - - 0.01

< LCL

0.050.05

0.1 - - < LCL

0.1 - - < LCL

0.1 - - < LCL

0.1 - - < LCL

Chlorfluazuron LC/MSMS - - - - 2 0.1 - - < LCL

Chlorfenvinphos LC/MSMS - - - - 0.05

0.02 < LCL

- -0.1

GC/MSMS - -

Página:

Muestra:

Huerto:

Cromatograma LC:

2 de 7

Zarzamora

ZIRACUARETIRO

P-19-177 01-04-2019.d

10- -- -GC/MSMSChlorothalonil

0.1 0.01 < LCL

Chlorfenapyr GC/MSMS - - - - 0.01 0.1 - - < LCL

Chlordimeform GC/MSMS - - - - 0.01

KOR CHN

Chlorpyrifos methyl GC/MSMS - - - - 0.05 0.1 - - < LCL

Chlorsulfuron LC/MSMS - - - - 0.01 0.1 - - < LCL

MX

0.01- -- -LC/MSMSChlorotoluron

- -0.1

- - < LCL

0.1 - - < LCL

Chlorpropham

Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El resultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A. de C.V. , por lo cual no se hace responsable de la representatividad del resultado para el total del producto.

Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto. Este formato de interpretación esta protegido y registrado ante el Instituto Mexicano de la Propiedad Intelectual. Se prohibe su reproducción total o parcial sin autorización. El presente informe de resultados no será valido si presenta raspaduras, tachaduras o enmendaduras.



*Analito no declarado en el alcance acreditado y/o autorizado que se obtiene por método acreditado y/o autorizado. Las bandas de colores son de apoyo visual basadas en los LMRs de México y no representan un resultado. 1Límite Máximo de Residuos (LMR) expresados en ppm para cada país indicado en código ISO 3166-1 alfa-3. LCL = Lowest Calibration Level (Nivel Mínimo de Calibración) ppm = Partes por millón = mg/kg GC/MSMS =Cromatografía de Gases/Masas/Masas LC/MSMS = Cromatografía de Líquidos/MasasMasas

Autoriza Lic. Carlos Sepúlveda Ibarra

Director General

B BB BB BB BB BB BB BB BB BB BB BB BB BB B

B B

B BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB B

B B

B B

B B

B B

B B

B BB B

B B

B BB B

B B

B B

B B

B B

B B

B BB B

0.05

1

0.01 - -

0.01 - -

0.01 - -

0.01 - -

- -

0.01 0.5

3

0.01 0.05

0.01 0.5

5

0.01 5

- -

1.5Imidacloprid

Imazaquin

LC/MSMS - - - - 0.01 0.1

- -

0.01 - -

0.03 0.5

0.01

5

0.05 0.05

3

0.05

0.01 0.02

0.01 0.05

0.01 0.01

0.01 0.01

0.01 - -

0.01 - -

0.01 0.3

0.01 0.5

- - - -

0.02 0.05

0.01

- -

0.01 - -

0.7 0.7

- - - -

0.01 0.02

0.01 0.2

- - - -

0.005 0.05

0.01 - -

0.05

5

0.05

0.01 5

- - - -

0.01

0.01

0.01

5

0.3

0.01 - -

0.01 - -

3 0.7

3 6

- -

0.05 5

0.01 0.1

- - - -

- - - -

0.01 1

0.01

0.01 5

0.01

0.01

0.050.01

0.01

- -

0.05

0.01

0.01

0.01

0.5

0.05

0.01

0.03

- -

0.01 - -

- -

0.01 0.05

0.02 0.02

- - - -

0.01 0.01

1 1

0.01

0.05 0.05

0.05 0.05

0.05 0.05

0.01 0.01

0.05 0.5

0.01 - -

0.02 - -

- - - -

0.01 0.05

0.01

0.01 2

1.5 0.5

- - - -

0.01 - -

- - - -

- - - -

0.01 0.2

0.01 0.03

0.01 - -

0.01 0.01

0.01 1

0.05 1

- - - -

0.01 1

0.01 2

0.01

EU KOR

- - - -

- - - -

0.01 0.1

0.01 15

- - - -

0.01 0.05- - - -

- -

- -

15

0.3

0.05

0.50.5

CHN MX US JP CA

0.01

- -

15

Revisión: AR271-TS-70


Resultados de AnálisisSe han detectado residuos de pesticidas prohibidos

Analito

Analizado

mediante

equipo

Uso autorizado

LMR (ppm) Cantidad obtenida en

mg/kg (ppm)Analito

Analizado

mediante

equipo

Uso autorizado

LMR (ppm)

Reg. Sagarpa: SD

No. Reg. Lab.:

CHN

Fecha de reporte:

Cantidad obtenida en

mg/kg (ppm)MX US JP CA

Cliente: P-19-177

Productor:

Cromatograma GC:

SUN BELLE MÉXICO S.A. DE

C.V.

JUAN JAVIER ALVAREZ

ORTEGA

EU

< LCL

Dialifos LC/MSMS - - - - - - - - - - < LCL Fenfuram

GC/MSMS - - - - 0.01 0.1 - -Desmetryn GC/MSMS - - - - - - - - - - < LCL Fenchlorphos

< LCL

Dichlofluanid GC/MSMS - - - - 10 0.1 - - < LCL Fenitrothion

LC/MSMS 20 20 15 20 15

< LCL

Diazinon GC/MSMS 0.75 0.75 0.1 0.1 0.1 < LCL Fenhexamid

LC/MSMS - - - - - - - - - -

< LCL

Dichlorvos GC/MSMS - - - - 0.1 0.1 0.2 < LCL Fenoxycarb

LC/MSMS - - - - 0.1 0.1 - -

< LCL

Dichloran GC/MSMS - - - - - - - - - - < LCL Fenoxaprop-ethyl

GC/MSMS - - - - 0.8 0.1 0.5

< LCL

Diclofop methyl GC/MSMS - - - - 0.01 0.1 - - < LCL Fenpropidin

GC/MSMS 12 12 5 12 5< LCL

Diclobutrazol* LC/MSMS - - - - - - - - - - < LCL Fenpropathrin

LC/MSMS - - - - 0.05 0.1 - -

< LCL

Dieldrin GC/MSMS 0.05 0.05 0.05 0.1 0.02 < LCL Fenpyroximate

LC/MSMS - - - - 0.05 0.1 - -

< LCL

Dicrotophos LC/MSMS - - - - 0.01 0.1 - - < LCL Fenpropimorph

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Difenoconazole LC/MSMS - - - - 0.01 0.1 - - < LCL Fensulfothion

GC/MSMS - - - - - - - - - -

< LCL

Diethofencarb LC/MSMS - - - - 0.01 0.1 - - < LCL Fenson

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Diflufenican LC/MSMS - - - - 0.01 0.1 - - < LCL Fenuron

GC/MSMS - - - - 0.01 0.1 0.05

< LCL

Difenoxuron LC/MSMS - - - - - - - - - - < LCL Fenthion

GC/MSMS - - - - 0.01 0.1 - -

< LCL

Dimepax GC/MSMS - - - - - - - - - - < LCL Flamprop methyl

GC/MSMS - - - - 0.01 0.1 0.02

< LCL

Dimefuron LC/MSMS - - - - - - - - - - < LCL Fipronil

LC/MSMS - - - - - - - - - -

< LCL

Dimethenamid LC/MSMS - - - - 0.01 0.1 - - < LCL Flazasulfuron

LC/MSMS - - - - - - - - - -

< LCLLC/MSMS - - - - 0.01 0.1 - -

Flamprop-isopropyl< LCL- -0.10.01- -- -LC/MSMSDimethachlor

< LCL

Dimethomorph LC/MSMS - - - - 0.01 0.1 - - < LCL Fluazifop-butyl

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Dimethoate GC/MSMS - - - - 1 0.1 - - < LCL Flonicamid

LC/MSMS - - - - 0.1 0.1 - -

< LCL

Dimethylphenol, 2,4- (2,4-xylenol) GC/MSMS - - - - - - - - - - < LCL Flubendiamide

LC/MSMS - - - - 0.01 0.1 - -

- -0.10.01- -- -LC/MSMS < LCL

0.2

1

< LCL

Dinotefuran LC/MSMS - - - - 0.01 0.1 - - < LCL Flucythrinate

GC/MSMS - - - - 0.01 0.1 - -< LCL Fluchloralin - -

0.05

Diniconazole - - 0.01 0.1 - -

< LCL

Diphenamid LC/MSMS - - - - 0.01 0.1 - - < LCL Flufenacet

GC/MSMS 5 5 5 7 - -

< LCL

Dioxathion GC/MSMS - - - - 0.01 0.1 - - < LCL Fludioxonil

GC/MSMS - - - - 0.05 0.1 - -

< LCL

Disulfoton GC/MSMS - - - - 0.05 0.1 - - < LCL Flumiclorac-pentyl

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Diphenylamine GC/MSMS - - - - 0.05 0.1 - - < LCL Flufenoxuron

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Disulfoton sulfoxide GC/MSMS - - - - - - - - - - < LCL Fluopicolide

LC/MSMS - - - - 0.02 0.1 - -

< LCL

Disulfoton sulfone GC/MSMS - - - - - - - - - - < LCL Fluometuron

GC/MSMS - - - - 0.01 0.1 - -

< LCL

Dodemorph LC/MSMS - - - - 0.01 0.1 - - < LCL Fluoroglycofen-ethyl

GC/MSMS 5 5 5 5 - -

< LCL

Diuron (Karmex) LC/MSMS 0.1 0.1 0.05 0.1 - - < LCL Fluopyram

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Edifenphos LC/MSMS - - - - 0.01 0.1 - - < LCL Fluridone

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Dyfonate GC/MSMS - - - - 0.01 0.1 0.01 < LCL Fluoxastrobin

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Endosulfan I (alpha isomer) GC/MSMS - - - - 0.5 0.1 - - < LCL Flusilazole

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Emamectin Benzoate LC/MSMS - - - - 0.1 0.1 - - < LCL Flurtamone

GC/MSMS - - - - 0.01 0.1 - -

< LCL

Endosulfan sulfato GC/MSMS - - - - 0.5 0.1 - - < LCL Flutriafol

GC/MSMS - - - - 0.01 0.1 - -

< LCL

Endosulfan II (beta isomer) GC/MSMS - - - - 0.5 0.1 - - < LCL Flutolanil

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Epoxiconazole LC/MSMS - - - - 0.01 0.1 - - < LCL Fluxapyroxad

GC/MSMS - - - - - - - - - -

< LCL

Endrin GC/MSMS - - - - 0.01 0.1 0.05 < LCL Fluvalinate

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Esfenvalerate + Fenvalerate (**) GC/MSMS 1 1 1 0.1 0.2 < LCL Forchlorfenuron

GC/MSMS - - - - 0.01 25 - -

< LCL

EPTC GC/MSMS - - - - 0.1 0.1 - - < LCL Folpet

LC/MSMS 5 5 5 5 - -

< LCL

Ethalfluralin GC/MSMS - - - - 0.01 0.1 - - < LCL Fosthiazate

LC/MSMS - - - - - - - - - -

< LCL

Etaconazole (Etaconazole I y II) LC/MSMS - - - - - - - - - - < LCL Formetanate

LC/MSMS - - - - 0.1 0.1 - -

< LCL

Ethiofencarb-sulfone LC/MSMS - - - - 0.01 0.1 - - < LCL Furathiocarb

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Ethiofencarb LC/MSMS - - - - 0.01 0.1 - - < LCL Fuberidazole

LC/MSMS - - - - 0.05 0.1 - -

< LCL

Ethoprop GC/MSMS - - - - 0.01 0.1 0.02 < LCL Haloxyfop-methyl

GC/MSMS 0.1 0.1 0.02 0.1 0.02

< LCL

Ethirimol LC/MSMS - - - - - - - - - - < LCL g Chlordan

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Etion GC/MSMS - - - - 0.3 0.1 - - < LCL Heptachlor exo-epoxide (isomer

GC/MSMS 0.05 0.05 0.01 0.1 0.01

< LCL

Ethylan GC/MSMS - - - - - - - - - - < LCL Heptachlor

LC/MSMS - - - - 0.05 0.1 - -

- -

< LCL

Etofenprox GC/MSMS 5 5 0.01 0.1 - - < LCL Heptenophos

GC/MSMS 0.05 0.05 0.01 0.1 0.01

Famoxadone LC/MSMS 10 10 10 10 - - < LCL Hexaconazole

Etoxazole LC/MSMS 1.5 1.5 0.01 1.5 - - < LCL Hexachlorobenzene0.3

0.01 2

- - 0.01 0.1LC/MSMS

Fenamidone GC/MSMS - - - - 0.01 0.1 - - < LCL Hexaflumuron - - 0.01 0.10.01 0.7

- - - - < LCL Hexythiazox

GC/MSMS - - - - 0.1 - -

Fenbuconazol LC/MSMS - -

Fenamiphos Sulfoxide

Fenazaquin LC/MSMS - - - - 0.01 0.1 - - < LCL

- -

- - - -

- - - -

0.02 0.2

0.01 1.5 - -

< LCL

0.05

- - 0.02 0.1

0.01 0.5

< LCL Imazapyr

GC/MSMS - - - - 0.1 0.1 - -

< LCL

Fenbutatin oxide* LC/MSMS - - - - 1 0.1 - - < LCL Imidan

LC/MSMS 2.5 2.5 4 2.5 - -0.05 0.5

5 2 < LCL

- - 0.01 0.1 - -

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LC/MSMS - -LC/MSMS - - - - - - - - - - < LCL Imazalil

LC/MSMS 1

2019-01-07

LC/MSMS - -

LC/MSMS - -

KOR

0.05 0.1

0.01 - -

0.01

CHNKOR

< LCLLC/MSMS - - - - 0.05 0.1 - -

< LCL

- - 0.02 0.1 - -2

0.05

1

US JP CA EUMX

< LCL

LC/MSMS - - - - 0.01 0.1 - -

< LCL- -

< LCL

< LCL

< LCLGC/MSMS 0.05 0.05 0.01 0.1 - -

< LCL

< LCL

Fenarimol LC/MSMS - - - - 1 0.1 - - - -

0.02 < LCL HexazinoneFenamiphos LC/MSMS - - 0.02 0.1

Fenamiphos Sulfone LC/MSMS - - - - - -

0.01

Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El re sultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A. de C.V. , por lo cual no se hace responsable de la representatividad del

resultado para el total del producto. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.

Este formato de interpretación esta protegido y registrado ante el Instituto Mexicano de la Propiedad Intelectual. Se prohibe su reproducción total o parcial sin autorización. El presente informe de resultados no será valido si presenta raspaduras, tacha duras o enmendaduras.



*Analito no declarado en el alcance acreditado y/o autorizado que se obtiene por método acreditado y/o autorizado. Las bandas de colores son de apoyo visual basadas en los LMRs de México y no representan un resultado. 1Límite Máximo de Residuos (LMR) expresados en ppm para cada país indicado en código ISO 3166 -1 alfa-3. LCL = Lowest Calibration Level (Nivel Mínimo de Calibración) ppm = Partes por millón = mg/kg GC/MSMS =Cromatografía de Gases/Masas/Masas LC/MSMS = Cromatografía de Líquidos/MasasMasas Trazas/Traces = < 0.010 ppm.


Director General

B BB BB BB BB BB BB BB BB B

B B

B B

B B

B BB BB BB BB BB B

B B

B B

B B

B B

B B

B B

B B

V B

B B

B B

B BB B

B B

B R

B B


B B

B

B

B

B

B

BBBBBBBBBB

B

B

- - - -

0.02 - -

- - - -

0.01 0.1

0.01 0.02

0.01 1

0.01 - -

0.05 3

0.01 2

0.01 2

- - - -

- - - -

- - - -

0.01 0.05

0.01 0.05

0.01 5

0.01 0.2

0.01 0.05

0.01 - -

0.01 2

- - - -

- - 0.2

0.2

0.1 0.2

0.05 2

0.05 0.05

QUINTOCENE

(PENTACHLORO

NITROBENZENE

)METABOLITE

QUINTOCENE

(PENTACHLORO

NITROBENZENE

)METABOLITE

- - - -

0.02 0.010.01 - -

0.01 0.5

- - - -

0.1 0.05

- - - -

0.01 0.3

0.01 0.2

0.01 - -

0.01 0.1

- - - -

0.01 2

0.01 3

- - - -

DIMETHOATE

METABOLITE

DIMETHOATE

METABOLITE

0.02 1

- - - -

0.05 0.05

0.01 1

0.01 0.5

- - - -

- - - -

0.01 - -

0.01 0.05

0.01 0.2

0.01 - -

0.01 - -

1 1

- -

0.01 0.2

0.05 0.1

0.01 0.05

0.01 - -

- - - -

0.01 5

0.1 0.05

0.01 0.1

- - - -

0.01 0.01

0.01 - -

0.01 0.02

0.01 0.3

0.01 0.05

0.01 - -

0.02 0.02

0.02 1

< LCL

Metrafenone LC/MSMS - - - - 0.01 0.1 - - < LCL

Metolcarb LC/MSMS - - - - 0.01 0.1 - - < LCL

< LCL

Metosulam

Piperophos LC/MSMS - - - - 0.01 0.1 - - < LCL

Pirimicarb LC/MSMS - - - - 0.5

- - - - 0.01 0.1 - - < LCL

Phoxim LC/MSMS - - - - 0.02 0.1 0.05 < LCL

LC/MSMS

LC/MSMS - - - - 0.01 0.1 - -

Picoxystrobin

LC/MSMS

< LCL

Picolinafen

Piperalin LC/MSMS

- - - - 0.01 0.1 - -

Phosphamidon LC/MSMS - - - - 0.01 0.1 0.05 < LCL

op Dicofol*** GC/MSMS - - - - 3 3 - - < LCL

Ovex GC/MSMS - - - - - - - - - - < LCL

Oxadiazon GC/MSMS - - - - 0.01 0.1

Oxadixyl LC/MSMS

Fecha de reporte: 2019-01-07 Revisión: AR271-TS-70


Reg. Sagarpa: SD

No. Reg. Lab.:Cliente:

Productor:

Cromatograma GC:



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Se han detectado residuos de pesticidas prohibidos

Analito

Analizado

mediante

equipo

Uso autorizado

LMR (ppm) Cantidad obtenida en

mg/kg (ppm)Analito

Analizado

mediante

equipo

Uso autorizado

LMR (ppm)

CHN

Cantidad obtenida

en mg/kg (ppm)MX US JP CA CHN MX US JP CAEU KOR EU KOR

Imiprothrin GC/MSMS - - - - - - - - - - < LCL Neburon

Iprodione GC/MSMS 25 25 12 25 - - < LCL Nitrapyrin

Indoxacarb GC/MSMS - - - -

- - - -

0.5 0.5

30 30

< LCL

- -

LC/MSMS - - - - 0.01 0.10.01 0.1 - - < LCL Nicosulfuron

LC/MSMS - - - - - -

0.01 0.1GC/MSMS - - - -

0.01 1

0.1

GC/MSMS - - - - 0.01 0.1

GC/MSMS - - - - - - - -

GC/MSMS

LC/MSMS - - - -

Isazophos LC/MSMS - - - - 0.01 0.1 0.01 < LCL

Isofenphos LC/MSMS

< LCL

Norflurazon-Desmethyl

O Phenylphenol

Nitrothal-isopropyl

Irgarol LC/MSMS

- -

- - - - - - - - - - < LCL Norflurazon

Iprovalicarb LC/MSMS - - - - 0.01 0.1

< LCLNovaluron*

- - - - 0.01 0.1

Isocarbophos GC/MSMS - - - - 0.01 0.1 0.05

- - - - 0.01 0.1 0.01

LC/MSMS

Isoprothiolane GC/MSMS - - - - 0.01 0.1 - - < LCL

< LCL< LCL

Isoprocarb LC/MSMS - - - - 0.01 0.1 - - < LCL Ofurace LC/MSMS - - - - - - - - - - < LCL

Omethoate LC/MSMSDIMETHOATE

METABOLITE

DIMETHOATE

METABOLITE

DIMETHOATE

METABOLITE

DIMETHOATE

METABOLITE

Kelthane*** GC/MSMS - - - - 3 3 - - < LCL

Isoxaflutole LC/MSMS - - - - 0.01 0.1 - - < LCL

Isoproturon LC/MSMS - - - - 0.01 0.1 - - < LCL

Leptophos GC/MSMS - - - - - - - - - - < LCL

Lenacil LC/MSMS - - - - 0.3 0.1 - - < LCL

Kresoxim-methyl LC/MSMS - - - - 0.01 0.1 - - < LCL0.01 2

0.1 - -

- - - -

Malaoxon LC/MSMSMALATHION

METABOLITE

MALATHION

METABOLITE

MALATHION

METABOLITE

MALATHION

METABOLITE

MALATHION

METABOLITE< LCL

Lufenuron LC/MSMS - - - - 0.01 0.1 - - < LCL

Linuron LC/MSMS - - - - 0.2 0.1 - - < LCL0.05 0.05

0.01 0.3

MALATHION

METABOLITE

MALATHION

METABOLITE

Mandipropamid LC/MSMS - - - - 0.01 0.1 - - < LCL

Mancozeb LC/MSMS - - - - 5 0.1 5 < LCL

Malathion GC/MSMS 8 8 8 8 - - < LCL0.02 0.5

0.05 5

0.01 0.1

Mepanipyrim LC/MSMS - - - - 0.01 0.1 - - < LCL

Mecarbam LC/MSMS - - - - 0.01 0.1 - - < LCL

Mebendazole LC/MSMS - - - - - - - - - - < LCL- - - -

0.01 0.05

4 3

Metazachlor LC/MSMS - - - - 0.01 0.1 - - < LCL

Metamitron LC/MSMS - - - - 0.01 0.1 - - < LCL

Metalaxyl-M (Mefenoxam, R-

enantiomero de metalaxyl)GC/MSMS 0.7 0.7 0.2 0.1 - - 0.6750.02 - -

0.1 - -

0.02 - -

Methamidophos LC/MSMS - - - - 0.01 0.1 0.05 < LCL

Methabenzthiazuron LC/MSMS - - - - 0.01 0.1 - - < LCLMetconazole LC/MSMS - - - - 0.01 0.1 - - < LCL0.02 0.4

0.01 0.05

0.01 0.1

Methiocarb sulfone GC/MSMS - - - - 0.05 0.1 - - < LCL

Methiocarb GC/MSMS - - - - 0.05 0.1 - - < LCL

Methidathion LC/MSMS - - - - 0.2 0.1 0.05 < LCL0.02 0.01

0.2 0.05

0.2 0.05

Methoprene GC/MSMS - - - - 0.01 0.1 - - < LCL

Methomyl LC/MSMS - - - - 1 0.01 0.2 < LCL

Methiocarb sulfoxide GC/MSMS - - - - 0.05 0.1 - - < LCL0.2 0.05

0.01 1

0.02 0.2

Methoxyfenozide LC/MSMS 6 6 0.01 6 - - < LCL

Methoxychlor GC/MSMS - - - - 7 0.1 - - < LCL

Methoprotryne LC/MSMS - - - - - - - - - - < LCL- - - -

0.01 14

0.01 1

GC/MSMS - - - - 0.01 0.1 - - < LCL

Methylpentachlophenyl Sulfide GC/MSMS - - - - - - - - - - < LCL

Metolachlor LC/MSMS - - - - 0.01 0.1 - - < LCL

Metobromuron LC/MSMS - - - - 0.01 0.1 - - < LCL

- -

< LCL

Mevinphos GC/MSMS - - - - 0.01 0.1 - - < LCL

Metoxuron LC/MSMS - - - - - - - - - -

Mexacarbate LC/MSMS - - - - - - - - - -

Metsulfuron-methyl LC/MSMS - - - - 0.01 0.1 - - < LCL

Metribuzin

Molinate LC/MSMS - - - - 0.01 0.1 - - < LCL

Mirex GC/MSMS - - - - 0.01 0.1 0.01 < LCL

MGK-264 GC/MSMS - - - - - - - - - - < LCL

- - - - 0.01 0.1 - - < LCL

Monolinuron LC/MSMS - - - - 0.01 0.1 - - < LCL

Monocrotophos LC/MSMS - - - - 0.01 0.1 0.03 < LCL

Napropamide LC/MSMS 0.1 0.1 0.1 0.1 - - < LCL Propamocarb LC/MSMS - - - - 0.01 0.1 - - < LCL

- - - - 1 0.1 - - < LCL

N-2,4-Dimethylphenyl formamide

(2,4-DMPF)LC/MSMS - - - - - - - - - - < LCL

Myclobutanil GC/MSMS 2 2 1 2 - - < LCL

Oxydemeton-methyl LC/MSMS - - - - 0.02 0.1

Monuron LC/MSMS

Oxyfluorfen GC/MSMS 0.05 0.05 0.01 0.1 - - < LCL

Oxamyl LC/MSMS - - - - 0.01 0.1 - - < LCL

Oxamyl Oxime LC/MSMS - - - - - - - - - - < LCL

0.01 0.5

- - - -

0.01 - -

0.05 0.05

- -

< LCL

- -

- -

- -

< LCL

< LCL

Parathion GC/MSMS - - - - 0.5 0.1 0.01 < LCL

Paclobutrazol (Bonzi) LC/MSMS - - - - 0.01 0.1 - - < LCL

Paraoxon LC/MSMS - - - - - - - - - - < LCL

- -

0.01 0.1 - - < LCL

- - < LCL

0.01 0.1 - -

0.1 0.1 0.1

< LCL

< LCL

- -

- -

< LCL- -

< LCL

- - < LCL

DIMETHOATE

METABOLITE< LCL

0.5 0.05

- - - -

- - - -

0.05 0.3

0.01

0.01 0.1 - -

- -

Resultados de análisis

Paraoxon-methyl LC/MSMS - - - - - - - - - - < LCL

< LCL

Parathion methyl GC/MSMS - - - - 0.2 0.1 0.02 < LCL

Penconazol LC/MSMS - - - - 0.2 0.1

Pencycuron LC/MSMS - - - -

- - 0.05 0.024 0.01

Permethrin

Phenmedipham

Phenthoate

Phenyl valerate

Pendimethalin LC/MSMS 0.1 0.1 0.05 0.1 - -

QUINTOCENE

(PENTACHLORO

NITROBENZENE

)METABOLITE

QUINTOCENE

(PENTACHLORO

NITROBENZENE

)METABOLITE

QUINTOCENE

(PENTACHLORO

NITROBENZENE

)METABOLITE

QUINTOCENE

(PENTACHLORO

NITROBENZENE

)METABOLITE

QUINTOCENE

(PENTACHLORO

NITROBENZENE

)METABOLITE

- - - - - - - - - -

- - - - 0.02 0.1 - -- - - -

Phorate

Phorate-sulfone

Phorate-sulfoxide

Phosalone

GC/MSMS

GC/MSMS

GC/MSMS

GC/MSMS

GC/MSMS

GC/MSMS

LC/MSMS

LC/MSMS

GC/MSMS

GC/MSMS

LC/MSMS

LC/MSMS

LC/MSMS

Pentachloroaniline

Pentachloroanisol

Pentachloronitrobenzene

Pentachlorophenol

Penthiopyrad

- - - - 0.05 0.024 0.01

- - - - 1 0.1 1

- - - - 0.01 0.1 - -

- - 0.01 0.1 - -

0.1 - -

0.05 5

0.01 - -

0.01 0.5

0.01 0.05

- - - - 0.01 0.1 - -

< LCL

< LCL

< LCL< LCL

< LCL

0.179

< LCL

< LCL

< LCL

< LCL

< LCL

< LCL

< LCL

- - - - 0.05 0.024 0.01

- -

- - - - 0.01

- - - - - - - - - -

- - - - - - - - - - < LCL

Piperonyl Butoxide LC/MSMS 8 8 8 8 - - < LCL

0.01 0.05

4 1

Pirimiphos-ethyl LC/MSMS - - - - 0.01 0.1 - - < LCL

Pirimiphos-methyl LC/MSMS - - - - 0.1 0.1 - - < LCL

0.1 1 < LCL

Procymidone GC/MSMS - - - - 0.01 0.1 - - < LCL

Profenofos GC/MSMS - - - - 0.01 0.1 - - < LCL

Primisulfuron-methyl LC/MSMS - - - - 0.01 0.1 - - < LCL

Prochloraz LC/MSMS - - - - 0.05 0.1 - - < LCL

< LCL

Profluoralin GC/MSMS - - - - - - - - - - < LCL

Promecarb GC/MSMS - - - - - - - - - - < LCL

0.01 0.05

KOR

Pronamide LC/MSMS - - - - - - - - - - < LCL

Propachlor LC/MSMS - - - - 0.01 0.1 - - < LCL

Prometon GC/MSMS - - - - - - - - - - < LCL

Prometryn GC/MSMS - - - - 0.01 0.1 - -

Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El resultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A. de C.V. , por lo cual no se hace responsable de la representatividad

del resultado para el total del producto. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.






Director General

B BB BB BB BB BB BB BB BB BB BB B

B B

B BB BB BB BB BB BB BB B

B B

B B

B B

B B

B BB B

B B

B B

B B

B B

B B

B

B

B VB VB VB VB VB VB VB VB V

B V

B

B

B

B

B

BBB

B

B

B

B

B

BBBB0.01 0.05 - - < LCLThifensulfuron-methyl LC/MSMS - - - - 0.01 0.1

- - < LCLThidiazuron LC/MSMS - - - - 0.01 0.1 0.01 0.2

0.01 1 - - < LCLThiamethoxam LC/MSMS 0.35 0.35 0.5 0.5

1 < LCLThiacloprid LC/MSMS - - - - 5 0.1 1 0.7

0.01 3 - - < LCLThiabendazole LC/MSMS - - - - 3 0.1

- - < LCLTetramethrin LC/MSMS - - - - 0.01 0.1 0.01 - -

CAPTAN

METABOLITE

CAPTAN

METABOLITE

CAPTAN

METABOLITE < LCLTetrahydrophthalimide, cis-1,2,3,6-

(THPI)GC/MSMS

CAPTAN

METABOLITE

CAPTAN

METABOLITE

CAPTAN

METABOLITE

CAPTAN

METABOLITE

- - < LCLTetradifon GC/MSMS - - - - 1 0.1 0.01 1

0.01 - - - - < LCLTetrachlorvinphos, E-isomer GC/MSMS - - - - 0.01 0.1

- - < LCLTerrazole GC/MSMS - - - - - - - - - - - -

0.01 0.05 - - < LCLTerbutryn GC/MSMS - - - - 0.01 0.1

- - < LCLTerbuthylazine-desethyl LC/MSMS - - - - - - - - - - - -

0.05 0.1 - - < LCLTerbuthylazine GC/MSMS - - - - 0.01 0.1

- - < LCLTerbumeton LC/MSMS - - - - - - - - - - - -

0.01 0.1 - - < LCLTerbacil GC/MSMS 0.2 0.2 0.1 0.1

- - < LCLTeflubenzuron LC/MSMS - - - - 0.01 0.1 0.01 2

0.01 1 - - < LCLTecnazene GC/MSMS - - - - 0.05 0.1

- - < LCLTebuthiuron LC/MSMS - - - - 0.01 0.1 0.01 - -

0.01 - - - - < LCLTebutam LC/MSMS - - - - 0.01 0.1

- - < LCLTebufenpyrad GC/MSMS - - - - 2 0.1 0.05 0.5

0.05 2 - - < LCLTebufenozide LC/MSMS 3 3 3 0.1

- - < LCLTebuconazole GC/MSMS - - - - 0.01 0.1 0.5 0.5

0.02 0.1 - - < LCLSumithrin GC/MSMS - - - - 0.01 0.1

- - < LCLSulfoxaflor LC/MSMS - - - - 0.01 0.1 0.01 0.5

0.01 - - 0.01 < LCLSulfotep LC/MSMS - - - - 0.01 0.1

- - < LCLSulfosulfuron LC/MSMS - - - - 0.01 0.1 0.01 - -

0.01 0.05 - - < LCLSulfentrazone LC/MSMS 0.15 0.15 0.05 0.15

- - < LCLSpiroxamine LC/MSMS - - - - 0.01 0.1 0.01 3

0.1 3 - - < LCLSpirotetramat LC/MSMS - - - - 0.01 2

5 0.1 0.01 5 - - < LCL- - < LCL Vinclozolin GC/MSMS - - - -

- - < LCL

Spiromesifen LC/MSMS - - - - 0.01 0.1 0.02 2

- - - - 0.01 0.1 0.01 0.050.02 1 - - < LCL Vamidothion LC/MSMSSpirodiclofen LC/MSMS - - - - 0.01 0.1

0.01 0.1 0.01 - - - - < LCL1 < LCL Uniconazole GC/MSMS - - - -

- - < LCL

Spinosad A LC/MSMS 1 1 1 0.5 1.5 1

- - - - - - - - - - - -1 0.7 - - < LCL Trimidal LC/MSMSSpinetoram J LC/MSMS 0.8 0.8 0.7 0.5

0.01 0.1 0.01 0.5 - - < LCL- - < LCL Triforine LC/MSMS - - - -

- - < LCL

S-Metolachlor LC/MSMS 0.1 0.1 0.01 0.1 0.05 0.1

- - - - 0.01 0.1 0.01 - -0.01 0.05 - - < LCL Triflusulfuron-methyl LC/MSMSSimetryn LC/MSMS - - - - 0.01 0.1

0.05 0.1 0.01 0.05 - - < LCL- - < LCL Trifluralin GC/MSMS - - - -

- - < LCL

Simazine GC/MSMS 0.2 0.2 0.2 0.1 0.01 0.25

- - - - 0.02 0.1 0.01 0.50.1 1 - - < LCL Triflumuron LC/MSMSSethoxydim* LC/MSMS 5 5 1 5

0.01 0.1 0.02 2 - - < LCL- - < LCL Triflumizole LC/MSMS - - - -

- - < LCL

Sebuthylazine GC/MSMS - - - - - - - - - - - -

- - - - 0.01 0.1 3 10.01 - - - - < LCL Trifloxystrobin LC/MSMSRotenone LC/MSMS - - - - 0.01 0.1

- - - - - - - - - - < LCL- - < LCL Trietazine LC/MSMS - - - -

- - < LCL

Rimsulfuron LC/MSMS 0.01 0.01 0.01 0.01 0.01 - -

- - - - 0.01 0.1 0.01 0.20.05 0.05 - - < LCL Tricyclazole GC/MSMSQuizalofop-ethyl LC/MSMS - - - - 0.05 0.1

- - - - - - - - - - < LCL- - < LCL Triclocarban LC/MSMS - - - -

- - < LCL

Quinoxyfen LC/MSMS - - - - 0.01 0.1 0.02 2

- - - - - - - - - - - -0.01 0.01 - - < LCL Trichloronate GC/MSMSQuinalphos LC/MSMS - - - - 0.02 0.1

0.5 0.1 0.01 0.05 0.2 < LCL- - < LCL Trichlorfon LC/MSMS - - - -

- - < LCL

Pyriproxyfen GC/MSMS 1 1 0.01 0.1 0.05 1

- - - - - - - - - - - -15 15 - - < LCL Tributyl phosphate GC/MSMSPyrimethanil LC/MSMS 15 15 10 15

0.01 0.1 0.01 - - - - < LCL- - < LCL Tribenuron-methyl LC/MSMS - - - -

- - < LCL

Pyridaphenthion GC/MSMS - - - - 0.01 0.1 0.01 0.2

- - - - 0.01 0.1 0.01 0.050.01 1 - - < LCL Triazophos GC/MSMSPyridalyl GC/MSMS - - - - 0.01 0.1

0.01 0.1 0.05 - - - - < LCL- - < LCL Triasulfuron LC/MSMS - - - -

- - < LCL

Pyridaben LC/MSMS - - - - 0.01 0.1 0.5 1

- - - - - - - - - - - -0.01 1 - - < LCL Triallate GC/MSMSPyrazophos LC/MSMS - - - - 0.01 0.1

0.5 0.1 0.01 0.5 - - < LCL- - < LCL Triadimenol GC/MSMS - - - -

- - < LCL

Pyraclostrobin LC/MSMS 4 4 3 3.5 3 3

- - - - 0.1 0.1 0.01 0.053 0.5 - - < LCL Triadimefon GC/MSMSPymetrozine LC/MSMS - - - - 0.01 0.1

5 0.1 0.02 2 5 < LCL- - < LCL Tolyfluanid GC/MSMS - - - -

- - < LCL

Prosulfuron LC/MSMS - - - - 0.01 0.1 0.01 - -

- - - - - - - - - - - -0.01 0.08 - - < LCL Tolchlofos methyl GC/MSMSProsulfocarb LC/MSMS - - - - 0.01 0.1

- - - - - - - - - - < LCL- - < LCL Tokution GC/MSMS - - - -

- - < LCL

Propyzamide LC/MSMS 0.05 0.05 0.01 0.1 0.01 0.05

- - - - 3 6 0.1 20.05 0.05 - - < LCL Thiophanate-methyl LC/MSMSPropoxur LC/MSMS - - - - 1 0.1

- - - - - - - - - - < LCL- - < LCL Thionazin LC/MSMS - - - -

< LCL

- - < LCL

Propiconazole GC/MSMS 1 1 0.05 1 0.01 0.3

- - - - - - - - - - - -0.01 - - - - < LCL Thiofanox Sulfoxide LC/MSMSPropetamphos LC/MSMS - - - - 0.01 0.1

0.05

1 0.1 0.01 1 - - < LCL- - < LCL Thiodicarb LC/MSMS - - - -

- - < LCL

Propazin GC/MSMS - - - - 0.01 0.1 0.01 - -

- - - - 3 0.1 0.01 10.01 7 - -

Cantidad obtenida en

mg/kg (ppm)Analito

Analizado

mediante

equipo

Uso autorizado

LMR (ppm) Cantidad obtenida

en mg/kg (ppm)

Thiocyclam hydrogen oxalate GC/MSMSPropargite (Omite) LC/MSMS - - - - 0.01 0.1

0.01 0.1 0.01 0.05 - - < LCL- - < LCL Thiobencarb LC/MSMS - - - -Propanil LC/MSMS - - - - 0.1 0.1 0.01

KOR CHN

Productor: JUAN JAVIER ALVAREZ ORTEGA Huerto: ZIRACUARETIRO Reg. Sagarpa: SD

Cliente: SUN BELLE MÉXICO S.A. DE C.V. Muestra: Zarzamora No. Reg. Lab.: P-19-177

CHN MX US JP CA EUMX US JP CA EU KOR

Resultados de análisisSe han detectado residuos de pesticidas prohibidos

Analito

Analizado

mediante

equipo

Uso autorizado

LMR (ppm)

Fecha de reporte: 2019-01-07 Página: 5 de 7 Revisión: AR271-TS-70

JP CA EU KOR CHNAgrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab

Cromatograma GC: P-19-177 01-06-2019.D Cromatograma LC: P-19-177 01-04-2019.d MX US

Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El re sultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A. de C.V. , por lo cual no se hace responsable de la representatividad del

resultado para el total del producto. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.






Director General

0.005

0.010

Vamidothion

Vinclozolin

Heptachlor exo-epoxide (isomer B) 0.020

Heptenophos 0.005

Fuberidazole 0.005

Furathiocarb 0.005

g Chlordan 0.010

Haloxyfop-methyl 0.005

Heptachlor 0.010

Fluxapyroxad 0.005

Folpet 0.010

Forchlorfenuron 0.005

Formetanate 0.005

Fosthiazate 0.005

Flurtamone 0.005

Flusilazole 0.005

Flutolanil 0.010

Flutriafol 0.005

Fluvalinate 0.010

Fluopicolide 0.005

Fluopyram 0.010

Fluoroglycofen-ethyl 0.005

Fluoxastrobin 0.005

Fluridone 0.010

Fludioxonil 0.010

Flufenacet 0.005

Flufenoxuron 0.005

Flumiclorac-pentyl 0.010

Fluometuron 0.005

Flonicamid 0.010

Fluazifop-butyl 0.005

Flubendiamide 0.010

Fluchloralin 0.010

Flucythrinate 0.010

Fenuron 0.005

Fipronil 0.020

Flamprop methyl 0.010

Flamprop-isopropyl 0.010

Flazasulfuron 0.005

Fenpropimorph 0.005

Fenpyroximate 0.005

Fenson 0.020

Fensulfothion 0.010

Fenthion 0.010

Analito LCL (ppm)

Fenoxaprop-ethyl 0.005

Fenoxycarb 0.005

Fenpropathrin 0.010

Fenpropidin 0.005

Methiocarb 0.020 Permethrin 0.010 Spiromesifen 0.005

Methabenzthiazuron 0.005 Pentachloronitrobenzene 0.010 Spinetoram J 0.005

Metconazole 0.005 Pentachloroanisol 0.010 S-Metolachlor 0.005

Metazachlor 0.005 Pentachloroaniline 0.010 Simetryn 0.005 Trifluralin 0.010

Methidathion 0.005 Penthiopyrad 0.010 Spirodiclofen 0.005

Mecarbam 0.005 Parathion methyl 0.010 Rotenone 0.005

Uniconazole 0.010

Triflusulfuron-methyl 0.005

Triforine 0.010

Trimidal 0.005

Methylpentachlophenyl Sulfide 0.010 Phosphamidon 0.005 Tebuconazole 0.010

Methoxyfenozide 0.005 Phosalone 0.010 Sumithrin 0.020

Methiocarb sulfoxide 0.020 Phenthoate 0.005 Spiroxamine 0.005

Methoprene 0.010 Phorate 0.010 Sulfosulfuron 0.005

Methomyl 0.005 Phenyl valerate 0.010 Sulfentrazone 0.005

Analito LCL (ppm)

Dimethylphenol, 2,4- (2,4-xylenol) 0.010

2,6 Dichlorobenzonitrilo 0.010 Bromuconazole* 0.010 Cyanazine 0.005 Diniconazole 0.005

2,3 dihydro-2,2dimethylbenzofuran

7-ol0.020

Methoxychlor 0.010 Phorate-sulfoxide 0.005 Sulfoxaflor 0.005Methoprotryne 0.005 Phorate-sulfone 0.005 Sulfotep 0.005

Methiocarb sulfone 0.010 Phenmedipham 0.005 Spirotetramat 0.005

Piperalin 0.005 Tebuthiuron 0.005

Metolcarb 0.010 Picoxystrobin 0.005 Tebutam 0.005

Metolachlor 0.005 Picolinafen 0.005 Tebufenpyrad 0.010

Metobromuron 0.010 Phoxim 0.010 Tebufenozide 0.005

Fecha de reporte: 2019-01-07 Página: 6 de 7 Revisión:


AR271-TS-70

Analito LCL (ppm)

Dimethoate 0.010

2, 4-D Methyl ester 0.010 Bromophos methyl 0.010 Coumaphos 0.010 Dimethomorph 0.005

1-Naphthol 0.010 Bromacil 0.010 Clothianidin 0.005

Lowest Calibration Level (Nivel Mínimo de Calibración) por analitoAnalito LCL (ppm) Analito LCL (ppm)

Bromopropylate 0.010 Crimidine 0.005

Dinotefuran 0.005

3,4 Dichloroaniline 0.010 Buprofezin 0.010 Cyazofamid 0.005 Dioxathion 0.0102,6-Dichlorobenzamide 0.005 Bupirimate 0.005 Cyantraniliprole 0.005

Diphenamid 0.005

Abamectin 0.005 Butocarboxim* 0.010 Cyflufenamid 0.010 Diphenylamine 0.0103-Hydroxy carbofuran 0.005 Butachlor 0.010 Cycloate 0.005

Disulfoton 0.010

Acetamiprid 0.005 Buturon 0.005 Cyfluthrin 0.010 Disulfoton sulfone 0.010Acephate 0.005 Butocarboxim-sulfoxide 0.005 Cyflumetofen 0.005

Disulfoton sulfoxide 0.010

Aclonifen 0.010 Cadusafos 0.010 Cymoxanil 0.005 Diuron (Karmex) 0.005

Acetochlor 0.005 Butylate 0.020Cyhalothrin (Isomero Lambda y

gamma)**0.010

Dodemorph 0.005

Alachlor 0.005 Carbaryl 0.010 Cyproconazole 0.005 Dyfonate 0.010

Acrinathrin 0.020 Captan 0.010Cypermethrin a (Zeta-

Cypermethrin)**0.010

Edifenphos 0.005

Aldicarb sulfone 0.005 Carbetamide 0.005 Cyromazine 0.005 Emamectin Benzoate 0.005Aldicarb 0.005 Carbendazim 0.005 Cyprodinil 0.010

Endosulfan I (alpha isomer) 0.010

Aldrin 0.010 Carboxin 0.005 DDD-p,p 0.010 Endosulfan II (beta isomer) 0.010Aldicarb-sulfoxide (Aldoxicarb) 0.005 Carbofuran 0.010 DDD-o,p 0.010

Endosulfan sulfato 0.010

Ametryn 0.010 Chinometionate 0.010 DDE-p,p 0.010 Endrin 0.010Ametoctradin 0.005 Carfentrazone ethyl 0.005 DDE-o,p 0.010

Epoxiconazole 0.005

Aminocarb 0.005 Chlorbromuron 0.005 DDT-p,p 0.010 EPTC 0.010Amicarbazone 0.005 Chlorantraniliprole 0.005 DDT-o,p 0.010

Esfenvalerate + Fenvalerate (**) 0.010

Atrazine-2-hydroxy 0.005 Chlordimeform 0.010 Deltamethrin 0.010 Etaconazole (Etaconazole I y II) 0.010Atrazine 0.010 Chlordane- a 0.010 DEET (Diethyl-m-toluamide, N,N-) 0.010

Ethalfluralin 0.010

Azinphos-ethyl 0.005 Chlorfenvinphos 0.005 Demeton S 0.010 Ethiofencarb 0.005Azamethiphos 0.005 Chlorfenapyr 0.010 Demeton O 0.010

Ethiofencarb-sulfone 0.005

Azoxystrobin 0.010 Chloridazon (Pyrazon) 0.005 Desmedipham 0.005 Ethirimol 0.005Azinphos-Methyl 0.005 Chlorfluazuron 0.005 Demeton-s-methyl-sulfone 0.005

Ethoprop 0.010

Benalaxyl 0.010 Chlormequat 0.005 Dialifos 0.005 Ethylan 0.010Baycarb 0.005 Chlorimuron-ethyl 0.005 Desmetryn 0.010

Etion 0.010

Benfluralin 0.010 Chloroneb 0.010 Dichlofluanid 0.010 Etofenprox 0.010Bendiocarb 0.005 Chlorobenzilate 0.010 Diazinon 0.010

Etoxazole 0.005

Bensulide 0.005 Chlorothalonil 0.010 Dichlorvos 0.010 Famoxadone 0.010Bensulfuron-methyl 0.005 Chloropropylate 0.010 Dichloran 0.010

Fenamidone 0.010

Benzoximate 0.005 Chloroxuron 0.005 Diclofop methyl 0.020 Fenamiphos 0.005Benthiavalicarb-isopropyl 0.005 Chlorotoluron 0.005 Diclobutrazol* 0.010

Fenamiphos Sulfone 0.005

BHC lindane beta 0.010 Dieldrin 0.010 Fenamiphos Sulfoxide 0.005BHC lindane alpha 0.010 Chlorpropham 0.010 Dicrotophos 0.005

Fenarimol 0.005Chlorpyrifos 0.010

BHC lindane gamma 0.010 Difenoconazole 0.005 Fenazaquin 0.005BHC lindane delta 0.010 Diethofencarb 0.005Chlorpyrifos methyl 0.010

Chlorsulfuron 0.005

Fenbuconazol 0.005

Bifenox 0.020 Chlorthiophos 0.020 Diflufenican 0.005 Fenbutatin oxide* 0.010Bifenazate 0.005 Chlortal dimethyl 0.010 Difenoxuron 0.005

Fenchlorphos 0.010

Bitertanol 0.005 Clofentezine 0.005 Dimepax 0.010 Fenfuram 0.005Bifenthrin 0.010 Clodinafop-propargyl 0.005 Dimefuron 0.005

Fenhexamid 0.005

Boscalid 0.005 Cloquintocet-mexyl 0.005 Dimethenamid 0.005 Fenitrothion 0.020

Bolstar 0.010 Clomazone 0.005 Dimethachlor 0.005

Analito LCL (ppm)

Hexachlorobenzene 0.010 Mevinphos 0.010 Pirimiphos-methyl 0.005 Terbuthylazine 0.010

Analito LCL (ppm) Analito LCL (ppm) Analito LCL (ppm)

Terbuthylazine-desethyl 0.005

Hexaflumuron 0.005 MGK-264 0.010 Prochloraz 0.005 Terbutryn 0.010

Hexaconazole 0.005 Mexacarbate 0.005 Primisulfuron-methyl 0.005

Terrazole 0.010

Hexythiazox 0.005 Molinate 0.005 Profenofos 0.010 Tetrachlorvinphos, E-isomer 0.010

Hexazinone 0.010 Mirex 0.010 Procymidone 0.010

Tetradifon 0.010

Imazapyr 0.005 Monolinuron 0.005 Promecarb 0.010Tetrahydrophthalimide, cis-1,2,3,6-

(THPI)0.010

Imazalil 0.005 Monocrotophos 0.005 Profluoralin 0.020

Tetramethrin 0.005

Imidacloprid 0.005 Myclobutanil 0.010 Prometryn 0.010 Thiabendazole 0.005

Imazaquin 0.005 Monuron 0.005 Prometon 0.010

Thiacloprid 0.005

Imiprothrin 0.020 Napropamide 0.005 Propachlor 0.005 Thiamethoxam 0.005

Imidan 0.010N-2,4-Dimethylphenyl formamide

(2,4-DMPF)0.010 Pronamide 0.005

Thidiazuron 0.005

Iprodione 0.010 Nicosulfuron 0.005 Propanil 0.005 Thifensulfuron-methyl 0.005

Indoxacarb 0.010 Neburon 0.005 Propamocarb 0.005

0.010

Iprovalicarb 0.005 Nitrapyrin 0.010 Propargite (Omite) 0.005

Thiodicarb 0.005

Thiobencarb 0.010

Irgarol 0.005 Nitrothal-isopropyl 0.010

Isazophos 0.010 Norflurazon 0.005 Propetamphos 0.005

Propazin 0.010 Thiocyclam hydrogen oxalate

Prosulfocarb 0.005

Isoprocarb 0.005 O Phenylphenol 0.010

Isocarbophos 0.010 Norflurazon-Desmethyl 0.010 Propiconazole 0.010

Isofenphos 0.005 Novaluron* 0.010 Propoxur

Propyzamide

0.005

0.005

Isoprothiolane 0.010 Ofurace 0.005

Isoxaflutole 0.010 op Dicofol*** 0.010 Pymetrozine 0.005

Isoproturon 0.005 Omethoate 0.005 Prosulfuron 0.005

Kresoxim-methyl 0.005 Oxadiazon 0.010 Pyrazophos 0.005

Kelthane*** 0.010 Ovex 0.010 Pyraclostrobin 0.005

Leptophos 0.010 Oxamyl 0.005 Pyridalyl 0.010

Lenacil 0.005 Oxadixyl 0.005 Pyridaben 0.005

Lufenuron 0.005 Oxydemeton-methyl 0.005 Pyrimethanil 0.005

Linuron 0.005 Oxamyl Oxime 0.005 Pyridaphenthion 0.010

Malathion 0.010 Paclobutrazol (Bonzi) 0.005 Quinalphos 0.005

Malaoxon 0.005 Oxyfluorfen 0.010 Pyriproxyfen 0.010

Mandipropamid 0.005 Paraoxon-methyl 0.005 Quizalofop-ethyl 0.005

Mancozeb 0.005 Paraoxon 0.005 Quinoxyfen 0.005

Mebendazole 0.005 Parathion 0.010 Rimsulfuron 0.005

Simazine 0.010


enantiomero de metalaxyl)0.010 Pencycuron 0.005 Sethoxydim* 0.010

Mepanipyrim 0.010 Penconazol 0.005 Sebuthylazine 0.010

Metamitron 0.005 Pendimethalin 0.005

Metsulfuron-methyl 0.005 Pirimiphos-ethyl 0.005 Terbumeton 0.005

Methamidophos 0.005 Pentachlorophenol 0.010 Spinosad A 0.005

Metribuzin 0.010 Pirimicarb 0.005 Terbacil 0.010

Metrafenone 0.005 Piperophos 0.005 Teflubenzuron 0.010

Metoxuron 0.005 Piperonyl Butoxide 0.005 Tecnazene 0.010

Metosulam 0.005

Thiofanox Sulfoxide

Thionazin

Thiophanate-methyl

Tokution

Tolchlofos methyl

Tolyfluanid

Triadimefon

Triadimenol

Triallate

0.005

0.005

0.005

0.010

0.010

0.010

0.010

0.010

0.010

Triasulfuron

Triazophos

Tribenuron-methyl

Tributyl phosphate

0.005

0.010

0.005

0.010

Tricyclazole 0.010

Triclocarban 0.010

Trichloronate 0.010

Trichlorfon 0.005

Triflumuron 0.010

Trietazine 0.005

Trifloxystrobin 0.005

Triflumizole 0.005

Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El re sultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A.

de C.V. , por lo cual no se hace responsable de la representatividad del resultado para el total del producto. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.




ppm = Partes por millón = mg/kg Incertidumbre = 50 % según "Method validation and quality control procedures for pesticide residues analysis in food and feed". No. de Documento SANCO/10684/2009. Punto 91

International Maximum Residue Level Database

http://www.mrldatabase.com/

EU Pesticides Database

http://ec.europa.eu/sanco_pesticides/public/index.cfm

Electronic Code of Federal Regulation

http://ecfr.gpoaccess.gov/cgi/t/text/text-idx?

Health Canada

http://pr-rp.hc-sc.gc.ca/mrl-lrm/index-eng.php

Normas Alimentarias FAO/OMS

http://www.codexalimentarius.net/pestres/data/pesticides/search.html

Positive List System for Agricultural Chemical Residues in Foods (Japón)

http://m5.ws001.squarestart.ne.jp/foundation/search.html

Información correspondiente a la página 2, página 3, página 4 y página 5

Información correspondiente a la página 5 y 6


Referencias

Glosario

Trazas = < 0.010 ppm.

MX= México

US= Estados Unidos

JP= Japón

CA= Canadá

EU= Union Europea

KOR=Corea

CHN= China

GC/MSMS = Gases/Masas/Masas AGILENT 225/MS, 240/MS

LC/MSMS = Líquidos/Masas/Masas QQQ (AGILENT 6460)

LCL = Lowest Calibration Level (Nivel Mínimo de Calibración)

LMR = Límite Máximo de Residuos

ppm = Partes por millón = mg/Kg

SD = Sin dato

1. El laboratorio Análisis Técnicos S.A. de C.V. se encuentra acreditado ante la EMA, en el Ensayo de determinación de residuos de pesticidas en frutas, legumbres, alimentos agrícolas y

semillas (incorporando extracción QuEChERS), por cromatografia de GASES/MASAS/MASAS ante el sistema ISO/IEC 17015:2005. 7890

2. El laboratorio Análisis Técnicos S.A. de C.V. se encuentra acreditado ante la EMA, en el Ensayo de determinación de residuos de pesticidas en frutas, legumbres, alimentos agrícolas y

semillas (incorporando extracción QuEChERS), por cromatografia de LÍQUIDOS/MASAS/MASAS ante el sistema ISO/IEC 17015:2005.

3. * = Analito no declarado en el alcance acreditado y/o autorizado que se obtiene por método acreditado y/o autorizado.

4. Uso autorizado del plaguicida en el país correspondiente indicado en código ISO 3166-1 alfa-2. Los LMR de cada país se indican en la misma tabla de resultados.

5. En caso de no haber sido detectado algun pesticida se observa una banda verde fuerte. En caso de haber detectado algun pesticida dentro de los límites permitidos se observa una banda

amarilla. En caso de haber detectado algun pesticida fuera de los límites permitidos se observará una banda roja. En caso de haber detectado algún pesticida prohibido se observará una

banda roja.

6. Las bandas de colores son de apoyo visual basadas en los LMRs de cada país y no representan un resultado.

7. ** = Se toma el LMR de Isomero Lambda para la molécula Cyhalothrin (Isomero Gamma y Lambda) , para Cypermethrin a (Zeta-Cypermethrin) se toma el LMR de Zeta-Cypermethrin y

para el LMR de Esfenvalerate + Fenvalerate se toma el de Esfenvalerate.

8. 2 = Para Canadá se considera el default LMR de 0.1 ppm según el punto 5.2.1.4.2 Food and Drug Regulations de Canada Food Inspection Agency http://www.inspection.gc.ca/food/meat-

and-poultry-products/manual-of-procedures/chapter-5/eng/1395150894222/1395150895519?chap=2.

9. Las bandas de colores de cada molécula son de apoyo visual basadas en los LMRs de cada país y no representan un resultado.

10. **El LMR de Dicofol es la suma de Kelthane(Dicofol) y op Dicofol

1. En las tablas correspondientes se presenta el punto más bajo de la calibración (LCL).

2. Las tablas correspondientes NO REPRESENTAN UN RESULTADO. Son datos informativos de calidad.

3.Incertidumbre = 50 % según "Method validation and quality control procedures for pesticide residues analysis in food and feed". No. de Documento SANCO/10684/2009. Punto 91

Límites Máximos de Residuos (LMR) para Zarzamora indicados en El Catálogo Oficial

de Plaguicidas de México 2004.

Límites Máximos de Residuos (LMR) para Zarzamora indicados en Enviromental

Protection Agency (EPA) Estados Unidos.

Límites Máximos de Residuos (LMR) para Zarzamora indicados en Electronic Code of

Federal Regulations, (e-CFR TM) Estados Unidos.

1. El cliente tiene cinco días naturales posteriores a la emisión de resultados**** para poder hacer alguna observación o reclamación al respecto, ya que en caso de no hacerlo en este

periodo de tiempo se considerará este informe como aceptado.

2. Las muestras podrán ser desechadas a los 5 días después de la emisión de resultados****, únicamente las muestras para análisis microbiológico serán desechadas 24 h después de ser

recibidas.

3. La información inscrita en el presente "Informe de resultados de análisis" se trata con estricto apego al aviso de privacidad de Análisis Técnicos S.A. de C.V. acatando a los artículos

tercero transitorio, 16 y 17 de la Ley Federa de Protección de Datos Personales en Posesión de los Particulares, con la finalidad de regular su tratamiento legítimo, controlado e informado, a

efecto de garantizar la privacidad y el derecho a la autodeterminación informativa de las personas.

4. Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas.

5. Análisis Técnicos S.A. de C.V. no se encuentra acreditado en muestreo.

6. Los LMR de los paises son un dato de referencia, solicitando revisar los sitios oficiales de cada país ya que pueden cambiar o modificarse.

7. El resultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A. de C.V., por lo cual no se hace responsable de la representatividad del resultado para el

total del producto

8. Este formato de interpretación está protegido y registrado ante el Instituto Nacional del Derecho de Autor (INDAUTOR), así mismo, los logotipos y nombre de Agrolab y sus filiales se

encuentran registrados ante el Instituto Mexicano de la propiedad Industrial (IMPI). Se prohibe su reproducción total o parcial, para otro fin que no sea la interpretación de resultados, sin

previa autorización.

9. El presente informe de resultados no será válido si presenta raspaduras, tachaduras o enmendaduras.

10. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.

11. El laboratorio Análisis Técnicos S.A. de C.V. no es responsable de la actualización de los LMR's ya que son considerados como un dato informativo. Es responsabilidad del usuario del

Informe revisar los sitios oficiales para LMR de cada país ya que la información puede cambiar o modificarse.

12. La detección del residuo del plaguicida por arriba del límite de cuantificación se reporta como ppm (mg//Kg) , por debajo del límite de cuantificación se reportar como <LCL ppm (mg/Kg)

y por debajo del LD se considera como no determinado.

****La emisión del resultados, contempla el informe final destinado a ser enviado al cliente (PDF). La entrega de resultados al cliente, se encuentra sujeta a confirmación de pago.


Información adicional y complementaria

Información general

Fecha de reporte: 2019-01-07 7 de 7 Revisión:Página:

Final del informe

AR271-TS-70

Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El resultado representa la muestra que fue recibida en las instalaciones de

Análisis Técnicos S.A. de C.V. , por lo cual no se hace responsable de la representatividad del resultado para el total del producto. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.




Report Date: 2019-01-07 Page: 1 of 7 Revision AR272-TS-70


Client Information

Applicant: ALFREDO OSEGUERA DÍAZ Company: SUN BELLE MÉXICO S.A. DE C.V.


[email protected],

[email protected]

Address: Km 1 Carr. los Reyes-Jacona S/N City or Town: Los Reyes

State: Michoacán ZIP Code: 60330

Telephone: 3545427328 Ext. 133 E-mail:


Billing Information

Corporate name: Fruits-Giddings SA de CV RFC SBM040520QN6

Address: Km. 1 Carretera los Reyes- Jacona Sn City or Town: Los Reyes

State: Michoacán ZIP Code: 60330

Sample Reg. No. P-19-177 Registry Book: ene-19

Receipt Date: 2019-01-04 Start Date: Termination Day: 2019-01-072019-01-04

Sample Information

Telephone: 3545420170 Ext. SD E-mail:[email protected], [email protected],

[email protected], [email protected]


Pesticides Multiresidual Analysis


Tupy|Otras

Analyzed part: Fruit Sample status: Frozen Less Than 1.5Kg

Variety:

Amount recieved:

Common Name: Blackberry Scientific Name: Rubus Ulmifoli

Sampling Place: DIRECCION: ZIRACUARETIRO,

MICHOACÁNSampling Method: Random SDWarehouse RFC:

Producer: JUAN JAVIER ALVAREZ ORTEGA Harvest Place: ZIRACUARETIRO SDSAGARPA Reg.:

Commercial use: Human Commercial Destination: National And Foreign Market

Sampling date:03 DE ENERO DEL 2018 Hora:

11:00 AM

Sample received in conditions for analysis.

2303-01(SECTOR 01)

Final Destination:

Observations:

SDCustoms House:

USA,EUROPE AND JAPAN

Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued result only affects the sample received at the facility of Análisis Técnicos S.A. de C.V, therefore it́ s not responsible for the

representation of the result for the total product. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.

This form of interpretation is protected and registered with the Instituto Mexicano de la Propiedad IntelectualIts total or partial reproduction without authorization is prohibited. This report will not be valid if you have scratches, erasures or amendments.

Controlled document ISO/IEC 17025:2005


B B

B B

B B

B B

B B

B B

B BB B

B B

B BB BB BB BB B

B B

B BB BB BB BB BB BB B

B B

B BB BB BB BB B

B B

B B

B B

B B

B B

B B

B B

B BB BB B

B B

B BB B

B B

V B

B B

B B

B B

B B

B BB BB BB B

B B

B B

B B

B B

B B

B B

B B

B B

B B

KOR CHN

OXYDEMETON

METHYL

METABOLITE

0.02

- - - -

0.01 - -

- - - -

- - - -

- - - -

- - - -

- - - -

- - - -

0.1 0.2

- - - -

0.01 0.1

0.01 1

0.02 1

0.2 0.5

0.5

0.02 - -

3 1

0.5 2

0.05 0.1

3 1

0.05 0.05

- - - -

0.01 0.05

- - - -

0.01 1

0.01 - -

0.01 - -

0.9 0.7

0.01 0.2

0.01 - -

- -

0.01 0.5

0.01 0.05

0.01 1

0.1 0.1

0.02 0.5

0.01 0.05

0.01 1

0.02 0.02

0.01 - -

- - - -

0.01 1

0.01 - -

0.01 - -

0.01 0.05

THIOPHANATE

METHYL/ BENOMYL

METABOLITE

0.01 - -

0.01 0.05

0.05 0.05

0.01 0.1

0.01 0.05

1 1

- - - -

0.01 0.02

1.5 - -

0.05 1

0.01 0.1

0.01 - -

0.01 - -

- - - -

20 5

0.01 0.5

THIOPHANATE

METHYL/

BENOMYL

METABOLITE

0.01

0.01

0.01 0.01

0.01 0.01

7 7

0.01 0.05

1 0.3

0.01 1

- - - -

10 9

0.01 0.1

0.05 0.3

0.01 0.02

0.02 - -

0.01 0.02

0.01 - -

0.01 0.1

0.01 0.5

0.01 0.01

0.01 0.01

0.01 - -

0.01 - -

- - - -

0.05 - -

- - - -

0.01 - -

0.02 - -

0.05 0.3

5 3

0.01 0.02

0.01 - -

0.02 1

0.01 0.05

0.02 0.02

0.02 0.02

0.02 0.02

0.01 0.01

0.01 0.05

0.1 0.05

- - - -

- - - -

- - - -

LINURON

METABOLITELINURON METABOLITE

- - - -

0.08 0.05

0.01 1

2 1

Report Date: 2019-01-07 Page: 2 of 7 Revision: AR272-TS-70

Chromatogram GC: P-19-177 01-06-2019.D Chromatogram LC: P-19-177 01-04-2019.d


Analysis Results

Producer: JUAN JAVIER ALVAREZ ORTEGA Orchard: ZIRACUARETIRO SAGARPA Reg.: SD

Client: SUN BELLE MÉXICO S.A. DE C.V. Sample: Blackberry Lab Reg. No.: P-19-177

US JPMX CA EU

JP CA CHN

1-Naphthol GC/MSMSCARBARYL

METABOLITE

CARBARYL

METABOLITE

CARBARYL

METABOLITE

CARBARYL

METABOLITECARBARYL METABOLITE

US JP CA CHN MX US

Banned pesticides residues have been detected

Analyte Analyzed by

Authorized use

MRL (ppm) Obtained amount in mg/kg

(ppm)Analyte Analyzed by

Authorized use

MRL (ppm) Obtained amount in mg/kg

(ppm)MX EU KOR EU KOR

CARBARYL

METABOLITE

CARBARYL

METABOLITE

0.1 - - < LCL

2,3 dihydro-2,2dimethylbenzofuran 7-ol GC/MSMS - - - - - - - - - -

< LCL Carbetamide LC/MSMS - - - - 0.01

THIOPHANATE

METHYL/

BENOMYL

METABOLITE

THIOPHANATE

METHYL/ BENOMYL

METABOLITE

< LCL

2, 4-D Methyl ester GC/MSMS 0.2 0.2 0.1 0.1 0.1

< LCL Carbendazim LC/MSMSTHIOPHANATE

METHYL/ BENOMYL

METABOLITE

THIOPHANATE

METHYL/ BENOMYL

METABOLITE

THIOPHANATE

METHYL/ BENOMYL

METABOLITE

0.1 - - < LCL

2,6-Dichlorobenzamide LC/MSMS - - - - - - - - - -

< LCL Carboxin LC/MSMS - - - - 0.01

0.1 0.02 < LCL

2,6 Dichlorobenzonitrilo GC/MSMS - - - - - - - - - -

< LCL Carbofuran GC/MSMS - - - - 0.3

0.1 - - < LCL

3-Hydroxy carbofuran LC/MSMS - - - - - - - - - -

< LCL Chinometionate GC/MSMS - - - - 0.01

0.1 - - < LCL

3,4 Dichloroaniline GC/MSMS LINURON METABOLITELINURON

METABOLITE

LINURON

METABOLITE

LINURON

METABOLITELINURON METABOLITE

< LCL Carfentrazone ethyl LC/MSMS 0.1 0.1 0.1

- - - - < LCL

Acephate LC/MSMS - - - - 0.01 0.1 0.50

< LCL Chlorbromuron LC/MSMS - - - - - -

0.9 1 < LCL

Abamectin LC/MSMS 0.2 0.2 0.05 0.2 - -

< LCL Chlorantraniliprole LC/MSMS 1.8 1.8 2

0.1 0.01 < LCL

Acetochlor LC/MSMS - - - - 0.01 0.1 - -

< LCL Chlordimeform GC/MSMS - - - - 0.01

0.1 0.02 < LCL

Acetamiprid LC/MSMS 1.6 1.6 2 4 2

< LCL Chlordane- a GC/MSMS 0.1 0.1 0.02

0.1 - - < LCL

Acrinathrin GC/MSMS - - - - 2 0.1 - -

< LCL Chlorfenvinphos LC/MSMS - - - - 0.05

0.1 - - < LCL

Aclonifen GC/MSMS - - - - 0.01 0.1 - -

< LCL Chlorfenapyr GC/MSMS - - - - 0.01

0.1 - - < LCL

Aldicarb LC/MSMS - - - - 0.01 0.1 0.02

< LCL Chloridazon (Pyrazon) LC/MSMS - - - - 0.01

0.1 - - < LCL

Alachlor LC/MSMS - - - - 0.01 0.1 - -

< LCL Chlorfluazuron LC/MSMS - - - - 2

0.1 - - < LCL

Aldicarb-sulfoxide (Aldoxicarb) LC/MSMS - - - - 0.01 0.1 0.02

< LCL Chlormequat LC/MSMS - - - - 0.05

0.1 - - < LCL

Aldicarb sulfone LC/MSMS - - - - 0.01 0.1 0.02

< LCL Chlorimuron-ethyl LC/MSMS - - - - 0.01

0.1 - - < LCL

Ametoctradin LC/MSMS - - - - 0.01 0.1 - -

< LCL Chloroneb GC/MSMS - - - - 0.01

0.1 - - < LCL

Aldrin GC/MSMS 0.05 0.05 0.05 0.1 0.05

< LCL Chlorobenzilate GC/MSMS - - - - 0.01

0.1 - - < LCL

Amicarbazone LC/MSMS - - - - 0.01 0.1 - -

< LCL Chlorothalonil GC/MSMS - - - - 10

- - - - < LCL

Ametryn GC/MSMS - - - - 0.01 0.1 - -

< LCL Chloropropylate GC/MSMS - - - - - -

0.1 - - < LCL

Atrazine GC/MSMS - - - - 0.02 0.1 - -

< LCL Chloroxuron LC/MSMS - - - - 0.01

0.1 - - < LCL

Aminocarb LC/MSMS - - - - - - - - - -

< LCL Chlorotoluron LC/MSMS - - - - 0.01

< LCL

0.1 - - < LCL

Atrazine-2-hydroxy LC/MSMS - - - - - - - - - -

< LCL Chlorpropham GC/MSMS - - - - 0.01

Chlorpyrifos GC/MSMS - - - - 1 0.1 - - < LCL0.01 0.3

< LCLAzinphos-ethyl LC/MSMS - - - - 0.01 0.1 - -

- - - -

Azamethiphos LC/MSMS - - - - 0.01 0.1 - - < LCL Chlorpyrifos methyl GC/MSMS - - - - 0.05 0.1 - -

- - - -

0.01 1

0.05 0.1

- - < LCL

Azoxystrobin GC/MSMS 5 5 5 5 - -

< LCL Chlortal dimethyl GC/MSMS - - - - - -Azinphos-Methyl LC/MSMS - - - - 0.01 2 1 - -

- - - -

0.1 - - < LCL

Benalaxyl GC/MSMS - - - - 0.05 0.1 - -

< LCL Clodinafop-propargyl LC/MSMS - - - - 0.02

< LCL

Baycarb LC/MSMS - - - - - - - - - -

< LCL Chlorthiophos GC/MSMS - - - - - -

- - - -

0.1 - - < LCL

Benfluralin GC/MSMS - - - - 0.01 0.1 - -

< LCL Clomazone LC/MSMS - - - - 0.02

0.1 - - < LCL

Bendiocarb LC/MSMS - - - - 0.01 0.1 - -

< LCL Clofentezine LC/MSMS - - - - 0.01

0.1 - - < LCL

Bensulide LC/MSMS - - - - 0.01 0.1 - -

< LCL Clothianidin LC/MSMS - - - - 0.2

0.1 - - < LCL

Bensulfuron-methyl LC/MSMS - - - - 0.01 0.1 - -

< LCL Cloquintocet-mexyl LC/MSMS - - - - 0.01

- - - - < LCL

Benzoximate LC/MSMS - - - - 0.01 0.1 - -

< LCL Crimidine LC/MSMS - - - - - -

0.1 0.05 < LCL

Benthiavalicarb-isopropyl LC/MSMS - - - - 0.01 0.1 - -

< LCL Coumaphos GC/MSMS - - - - - -

0.1 - - < LCL

BHC lindane beta GC/MSMS 0.5 0.5 0.3 0.1 - -

< LCL Cyantraniliprole LC/MSMS 4 4 0.01

0.1 - - < LCL

BHC lindane alpha GC/MSMS 0.5 0.5 0.3 0.1 - -

< LCL Cyanazine LC/MSMS - - - - 0.01

0.1 - - < LCL

BHC lindane gamma GC/MSMS 0.5 0.5 0.3 0.1 - -

< LCL Cycloate LC/MSMS - - - - 0.01

0.02 - - < LCL

BHC lindane delta GC/MSMS 0.5 0.5 0.3 0.1 - -

< LCL Cyazofamid LC/MSMS - - - - 0.01

0.1 - - < LCL

Bifenox GC/MSMS - - - - 0.01 0.1 - -

< LCL Cyflumetofen LC/MSMS - - - - 0.01

0.1 - - < LCL

Bifenazate LC/MSMS 5 5 7 5 7

< LCL Cyflufenamid GC/MSMS - - - - 0.01

0.01 0.2 < LCL

Bitertanol LC/MSMS - - - - 0.05 0.1 - -

0.011Cyhalothrin (Isomero Lambda

y gamma)**GC/MSMS - - - - 0.5

0.1 - - < LCL

Bifenthrin GC/MSMS 1 1 1 1 1

< LCL Cyfluthrin GC/MSMS - - - - 0.02

0.1 - - < LCL

Boscalid LC/MSMS 10 10 10 6 - -

< LCLCypermethrin a (Zeta-

Cypermethrin)**GC/MSMS 0.8 0.8 0.5

4 - - < LCL

Bolstar GC/MSMS - - - - - - - - - -

< LCL Cymoxanil LC/MSMS 4 4 4

- - < LCL

Bromophos methyl GC/MSMS - - - - - - - - - -

< LCL Cyprodinil GC/MSMS 10 10 10

0.1 - - < LCL

Bromacil GC/MSMS - - - - 0.01 0.1 - -

< LCL Cyproconazole LC/MSMS - - - - 0.5

- -

0.1 - -

< LCL DDD-o,p GC/MSMS - - - - - -

0.1 - - < LCL

Bromopropylate GC/MSMS - - - - 2 0.1 - -

< LCL Cyromazine LC/MSMS - - - - 0.01- -

0.01 5

0.05 - -

- - - - 0.01 0.1 - -

< LCL DDE-o,p GC/MSMS - - - - - -

- - - - < LCL

Bupirimate LC/MSMS - - - - 0.01 0.1 - -

< LCL DDD-p,p GC/MSMS - - - - - -Bromuconazole* LC/MSMS - - - - 0.01

Butocarboxim* LC/MSMS - - - - 0.01 0.1 - -

< LCL DDT-o,p GC/MSMS - - - - - -

- - - - < LCL

Butachlor GC/MSMS - - - - 0.01 0.1 - -

< LCL DDE-p,p GC/MSMS - - - - - -

< LCL

Buprofezin GC/MSMS

- - 0.01 0.1 0.02

- - < LCL

Buturon LC/MSMS - - - - - - - - - -

< LCLDEET (Diethyl-m-toluamide,

N,N-)GC/MSMS - - - - - -Butocarboxim-sulfoxide LC/MSMS - - - - 0.01 0.1 - - - -

- - - - < LCL< LCL Demeton O

25 0.01 0.1 - -

- - - -

0.1 0.02 < LCL

0.1 - - < LCL

Butylate GC/MSMS - - - - 0.01 0.1 - -

< LCL Deltamethrin GC/MSMS - - - - 0.1

0.01 - -

0.01 0.05Cadusafos GC/MSMS - -

< LCL Desmedipham LC/MSMS - - - - 0.01

OXYDEMETON

METHYL

METABOLITE

OXYDEMETON

METHYL

METABOLITE

< LCL

< LCL Demeton S GC/MSMS - - - - 0.4

Carbaryl GC/MSMS 12 12 10 10 - -

< LCL Demeton-s-methyl-sulfone LC/MSMSOXYDEMETON

METHYL

METABOLITE

OXYDEMETON

METHYL

METABOLITE

OXYDEMETON

METHYL

METABOLITECaptan GC/MSMS 25

GC/MSMS - -

< LCL

Chlorsulfuron LC/MSMS - - - - 0.01 0.1 - - < LCL

0.1 - - < LCL

- - - - < LCLDDT-p,p GC/MSMS - - - - - -

- - - - < LCL

- - - - < LCL

- - - - < LCL

10

* Analyte not declared in the scope accredited and / or licensed accredited obtained by method and / or authorized. The colored bands are visual aids based on MRLs of Mexico and are not a result. 1Maximum Resuide Limits (MRL) expressed in ppm for every country using ISO 3166 -1 alfa-2. LCL = Lowest Calibration Level ppm = Parts per million = mg/kg GC/MSMS = Gass Chromatography /Mass/Mass LC/MSMS = Liquid Chromatography /MassMass

Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued res ult only affects the sample received at the facility of Análisis Técnicos S.A. de C.V, therefore it ´s not responsible for the representation of the result for the total product.

Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product. This form of interpretation is protected and registered with the Instituto Mexicano de la Propiedad Intelectual. Its total or partial reproduction without authorization is prohibited. This report will not be valid if you have scratches, erasures or ame ndments.



Authorizes Lic. Carlos Sepúlveda Ibarra

General Director

B BB BB BB BB BB BB BB BB BB BB BB BB BB B

B B

B BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB B

B B

B B

B B

B B

B B

B BB B

B B

B BB B

B B

B B

B B

B B

B B

B BB B

0.01 0.02

0.01 0.05

0.01 0.01

0.05 3

0.01 0.01

0.01 - -

0.01 - -

0.01 0.3

0.01 0.5

0.01 0.05

0.5 1

0.05 2

0.01 0.05

0.1

0.1

0.1

0.1

- - - -

0.01 0.5

0.01 0.5

0.02 0.05

0.01 - -

0.01 0.05

0.03 3

0.01 0.05

- - - -

5 5

0.05 0.05

0.05 0.3

0.01 - -

0.01 - -

3 0.7

0.01 - -

0.01 5

0.01 5

3 6

0.01 - -

0.01 - -

0.01 - -

0.01 0.02

0.01 0.2

- - - -

0.005 0.05

0.01 - -

- - - -

0.01 - -

0.03 0.5

0.01 0.2

0.01 1

0.01 - -

0.01 0.05

- - - -

0.02 0.2

0.01 0.5

0.05 0.5

5 2

0.01 - -

- - - -

15 15

0.01 0.3

0.01 0.05

0.05 0.50.01 0.5

0.01 - -

0.01 - -

0.7 0.7

- - - -

0.02 0.02

- - - -

0.01 0.01

1 1

0.01 0.3

0.01 2

- - - -

0.01 1

0.01 - -

0.01 - -

0.01 0.2

0.01 0.03

0.05 0.05

0.7

0.02 0.1

- - - -

0.01 0.01

0.05 0.5

0.01 - -

0.02 - -

- - - -

0.01 0.05

0.01 5

0.01 5

- - - -

0.05 0.05

0.05 0.05

0.05 1

- - - -

0.01 1

0.01 2

0.01 - -

0.01 0.05

0.05 5

0.01 0.1

- - - -

0.01 2

1.5 0.5

- - - -

0.01 - -

- - - -

- - - -

0.01 - -

0.01 0.01

0.01 1

- - - -

0.01 0.1

0.01 15

- - - -

0.01 0.05- - - -

0.05 0.1

0.01 - -

0.01 0.01


Chromatogram GC: P-19-177 01-06-2019.D Chromatogram LC: P-19-177 01-04-2019.d


Analysis Results

Producer:JUAN JAVIER ALVAREZ

ORTEGAOrchard: ZIRACUARETIRO SAGARPA Reg.: SD

Client:SUN BELLE MÉXICO S.A. DE

C.V.Sample: Blackberry Lab Reg. No.: P-19-177

US JP CA EUMX

JP CA CHN

Desmetryn GC/MSMS - - - - - - - - - -

US JP CA CHN MX US


AnalyteAnalyzed

by

Authorized use

MRL (ppm) Obtained amount in

mg/kg (ppm)Analyte

Analyzed

by

Authorized use


mg/kg (ppm)MX EU KOR EU KOR

- - - -

- - - - < LCL

Diazinon GC/MSMS 0.75 0.75 0.1 0.1 0.1

< LCL Fenfuram LC/MSMS - - - - - -

0.1 - - < LCL

Dialifos LC/MSMS - - - - - - - - - -

< LCL Fenchlorphos GC/MSMS - - - - 0.01

0.1 0.5 < LCL

Dichloran GC/MSMS - - - - - - - - - -

< LCL Fenitrothion GC/MSMS - - - - 0.8

20 15 < LCL

Dichlofluanid GC/MSMS - - - - 10 0.1 - -

< LCL Fenhexamid LC/MSMS 20 20 15

0.1 - - < LCL

Diclobutrazol* LC/MSMS - - - - - - - - - -< LCL Fenoxycarb LC/MSMS - - - - 0.05

0.1 - - < LCL

Dichlorvos GC/MSMS - - - - 0.1 0.1 0.2

< LCL Fenoxaprop-ethyl LC/MSMS - - - - 0.1

0.1 - - < LCL

Dicrotophos LC/MSMS - - - - 0.01 0.1 - -

< LCL Fenpropidin LC/MSMS - - - - 0.01

12 5 < LCL

Diclofop methyl GC/MSMS - - - - 0.01 0.1 - -

< LCL Fenpropathrin GC/MSMS 12 12 5

0.1 - - < LCL

Diethofencarb LC/MSMS - - - - 0.01 0.1 - -

< LCL Fenpyroximate LC/MSMS - - - - 0.01

0.1 - - < LCL

Dieldrin GC/MSMS 0.05 0.05 0.05 0.1 0.02

< LCL Fenpropimorph LC/MSMS - - - - 0.05

0.1 - - < LCL

Difenoxuron LC/MSMS - - - - - - - - - -

< LCL Fensulfothion GC/MSMS - - - - 0.01

- - - - < LCL

Difenoconazole LC/MSMS - - - - 0.01 0.1 - -

< LCL Fenson GC/MSMS - - - - - -

- - - - < LCL

Dimefuron LC/MSMS - - - - - - - - - -

< LCL Fenuron LC/MSMS - - - - - -

0.1 0.05 < LCL

Diflufenican LC/MSMS - - - - 0.01 0.1 - -

< LCL Fenthion GC/MSMS - - - - 0.01

0.1 - - < LCL

Dimethachlor LC/MSMS - - - - 0.01 0.1 - -

< LCL Flamprop methyl LC/MSMS - - - - 0.01

0.1 0.02 < LCL

Dimepax GC/MSMS - - - - - - - - - -

< LCL Fipronil GC/MSMS - - - - 0.01

0.1 - - < LCL

Dimethoate GC/MSMS - - - - 1 0.1 - -

< LCL Flazasulfuron LC/MSMS - - - - 0.1

- - - - < LCL

Dimethenamid LC/MSMS - - - - 0.01 0.1 - -

< LCL Flamprop-isopropyl LC/MSMS - - - - - -

0.1 - - < LCL

Dimethylphenol, 2,4- (2,4-xylenol) GC/MSMS - - - - - - - - - -

< LCL Fluazifop-butyl LC/MSMS - - - - 0.01

0.1 - - < LCL

Dimethomorph LC/MSMS - - - - 0.01 0.1 - -

< LCL Flonicamid LC/MSMS - - - - 0.01

0.1 - - < LCL

Dinotefuran LC/MSMS - - - - 0.01 0.1 - -

< LCL Fluchloralin GC/MSMS - - - - 0.01

0.1 - - < LCL

Diniconazole LC/MSMS - - - - 0.01 0.1 - -

< LCL Flubendiamide LC/MSMS - - - - 0.01

7 - - < LCL

Diphenamid LC/MSMS - - - - 0.01 0.1 - -

< LCL Fludioxonil GC/MSMS 5 5 5

0.1 - - < LCL

Dioxathion GC/MSMS - - - - 0.01 0.1 - -

< LCL Flucythrinate GC/MSMS - - - - 0.05

0.1 - - < LCL

Disulfoton GC/MSMS - - - - 0.05 0.1 - -

< LCL Flufenoxuron LC/MSMS - - - - 0.01

0.1 - - < LCL

Diphenylamine GC/MSMS - - - - 0.05 0.1 - -

< LCL Flufenacet LC/MSMS - - - - 0.01

0.1 - - < LCL

Disulfoton sulfoxide GC/MSMS - - - - - - - - - -

< LCL Fluometuron LC/MSMS - - - - 0.02

0.1 - - < LCL

Disulfoton sulfone GC/MSMS - - - - - - - - - -

< LCL Flumiclorac-pentyl GC/MSMS - - - - 0.01

5 - - < LCL

Dodemorph LC/MSMS - - - - 0.01 0.1 - -

< LCL Fluopyram GC/MSMS 5 5 5

0.1 - - < LCL

Diuron (Karmex) LC/MSMS 0.1 0.1 0.05 0.1 - -

< LCL Fluopicolide LC/MSMS - - - - 0.01

0.1 - - < LCL

Edifenphos LC/MSMS - - - - 0.01 0.1 - -

< LCL Fluoxastrobin LC/MSMS - - - - 0.01

0.1 - - < LCL

Dyfonate GC/MSMS - - - - 0.01 0.1 0.01

< LCL Fluoroglycofen-ethyl LC/MSMS - - - - 0.01

0.1 - - < LCL

Endosulfan I (alpha isomer) GC/MSMS - - - - 0.5 0.1 - -

< LCL Flurtamone LC/MSMS - - - - 0.01

0.1 - - < LCL

Emamectin Benzoate LC/MSMS - - - - 0.1 0.1 - -

< LCL Fluridone GC/MSMS - - - - 0.01

0.1 - - < LCL

Endosulfan sulfato GC/MSMS - - - - 0.5 0.1 - -

< LCL Flutolanil GC/MSMS - - - - 0.01

0.1 - - < LCL

Endosulfan II (beta isomer) GC/MSMS - - - - 0.5 0.1 - -

< LCL Flusilazole LC/MSMS - - - - 0.01

- - - - < LCL

Epoxiconazole LC/MSMS - - - - 0.01 0.1 - -

< LCL Fluvalinate GC/MSMS - - - - - -

0.1 - - < LCL

Endrin GC/MSMS - - - - 0.01 0.1 0.05

< LCL Flutriafol LC/MSMS - - - - 0.01

25 - - < LCL

Esfenvalerate + Fenvalerate (**) GC/MSMS 1 1 1 0.1 0.2

< LCL Folpet GC/MSMS - - - - 0.01

5 - - < LCL

EPTC GC/MSMS - - - - 0.1 0.1 - -

< LCL Fluxapyroxad LC/MSMS 5 5 5

- - - - < LCL

Ethalfluralin GC/MSMS - - - - 0.01 0.1 - -

< LCL Formetanate LC/MSMS - - - - - -

0.1 - - < LCL

Etaconazole (Etaconazole I y II) LC/MSMS - - - - - - - - - -

< LCL Forchlorfenuron LC/MSMS - - - - 0.1

0.1 - - < LCL

Ethiofencarb-sulfone LC/MSMS - - - - 0.01 0.1 - -

< LCL Fuberidazole LC/MSMS - - - - 0.01

0.1 - - < LCL

Ethiofencarb LC/MSMS - - - - 0.01 0.1 - -

< LCL Fosthiazate LC/MSMS - - - - 0.05

0.02 < LCL

Ethoprop GC/MSMS - - - - 0.01 0.1 0.02

< LCL g Chlordan GC/MSMS 0.1 0.1 0.02

0.1 - - < LCL

Ethirimol LC/MSMS - - - - - - - - - -

< LCL Furathiocarb LC/MSMS - - - - 0.01

0.01 < LCL

Etion GC/MSMS - - - - 0.3 0.1 - -

< LCL Heptachlor GC/MSMS 0.05 0.05 0.01

0.1 - - < LCL

Ethylan GC/MSMS - - - - - - - - - -

< LCL Haloxyfop-methyl LC/MSMS - - - - 0.05

- - < LCL

Etoxazole LC/MSMS 1.5 1.5 0.01 1.5 - -

< LCL Heptenophos LC/MSMS - - - - 0.01

0.1 0.01 < LCL

Etofenprox GC/MSMS 5 5 0.01 0.1 - -

< LCL Heptachlor exo-epoxide (isomer GC/MSMS 0.05 0.05 0.01

- - < LCL

Fenamidone GC/MSMS - - - - 0.01 0.1 - -

< LCL Hexaconazole LC/MSMS - - - - 0.01

0.1 - - < LCL

Famoxadone LC/MSMS 10 10 10 10 - -

< LCL Hexachlorobenzene GC/MSMS 0.05 0.05 0.01

0.01

0.1 - - < LCL

Fenamiphos Sulfone LC/MSMS - - - - - - - - - -

< LCL Hexazinone GC/MSMS - - - - 0.01

0.1 - - < LCL

Fenamiphos LC/MSMS - - - - 0.02 0.1 0.02

< LCL Hexaflumuron LC/MSMS - - - - 0.01

0.1 - - < LCL

Fenarimol LC/MSMS - - - - 1 0.1 - -

< LCL Imazalil LC/MSMS - - - - 0.02

1.5 - - < LCL

Fenamiphos Sulfoxide LC/MSMS - - - - - - - - - -

< LCL Hexythiazox LC/MSMS 1 1 0.01

LC/MSMS - - - - 0.01 0.1 - -

< LCL Imazaquin LC/MSMS - - - - 0.05

0.1 - - < LCL

Fenazaquin LC/MSMS - - - - 0.01 0.1 - -

< LCL Imazapyr LC/MSMS - - - - 0.01

0.05 0.05

5 1.5

CHNKOR

0.1 - - < LCL< LCL Imidan GC/MSMS - - - - 0.1

2.5 - - < LCL

Fenbutatin oxide* LC/MSMS - - - - 1 0.1 - -

< LCL Imidacloprid LC/MSMS 2.5 2.5 4

0.1 - - < LCL

Fenbuconazol

*Analyte not declared in the scope accredited and / or licensed accredited obtained by method and / or authorized. The colored bands are visual aids based on MRLs of Mexico and are not a result. 1Maximum Resuide Limits (MRL) expressed in ppm for every country using ISO 3166-1 alfa-2. LCL = Lowest Calibration Level ppm = Parts per million = mg/kg GC/MSMS = Gass Chromatography /Mass/Mass LC/MSMS = Liquid Chromatography /MassMass

Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued result only affects the sample received at the facility of Análisis Técnicos S.A. de C.V, therefore it´s not responsible for the

representation of the result for the total product. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.

This form of interpretation is protected and registered with the Instituto Mexicano de la Propiedad Intelectual. Its total or partial reproduction without authorization is prohibited. This report will not be valid if you have scratches, erasures or amendments.




General Director


B B

B B

B B

B BB BB BB BB BB B

B B

B B

B B

B B

B B

B B

B B

V B

B B

B B

B BB B

B B

B R

B B


B B

B

B

B

B

B

BBBBBBBBBB

B

B

0.01 2

0.01 2

- - - -

- - - -

- - - -

0.01 0.05

- - - -

0.02 - -

- - - -

0.01 2

- - - -

- - 0.2

0.01 0.05

4 1

0.01 0.02

0.01 1

0.01 - -

0.05 3

0.01 - -

0.01 0.5

0.01 0.05

0.01 0.05

0.01 0.05

0.01 5

0.01 0.2

0.01 0.05

0.01 - -

0.5 0.05

- - - -

- - - -

0.05 0.3

0.01 0.2

0.1 0.2

0.05 2

0.05 0.05

QUINTOCENE

(PENTACHLORO

NITROBENZENE

)METABOLITE

QUINTOCENE

(PENTACHLORO

NITROBENZENE

)METABOLITE

DIMETHOATE

METABOLITE

DIMETHOATE

METABOLITE

0.02 1

- - - -

0.05 0.05

0.01 1

0.01 0.5

- - - -

0.01 - -

0.05 0.05

0.01 0.1

0.01 0.5

- - - -

- - - -

0.01 - -

0.01 0.05

0.01 0.2

0.01 - -

0.01 - -

0.01 1

- - - -

0.01 0.2

0.05 0.1

0.01 0.05

0.01 - -

- - - -

0.01 5

0.1 0.05

0.01 0.05

0.01 0.1

0.02 0.01

0.2 0.05

0.2 0.05

0.2 0.05

0.01 1

0.02 0.2

- - - -

0.05 5

0.01 0.1

- - - -

0.01 0.05

4 3

0.02 - -

0.1 - -

0.02 - -

0.02 0.4

0.01 0.05

0.01 - -

0.02 0.02

0.02 1

0.01 2

0.1 - -

- - - -

0.05 0.05

0.01 0.3

EU KOR EU KOR

- - - -

0.5 0.5

30 30

0.01 1

- - - -

0.01 0.01

0.01 - -

- - - -

0.01 0.3

0.01 0.2

0.01 - -

0.01 0.1

- - - -

0.01 2

Metolcarb LC/MSMS - - - - 0.01 0.1 - - < LCL

Metolachlor LC/MSMS - - - - 0.01

ZIRACUARETIRO SAGARPA Reg.: SD

US JP CA EU

Nicosulfuron


AnalyteAnalyzed

by

Authorized use

MRL (ppm)

MX JP CA CHN

- -

0.01 0.1 0.01

- - - -

0.02 0.1 0.05

- -< LCL Norflurazon-Desmethyl

0.1< LCL Norflurazon - -

0.05

< LCL O Phenylphenol

- -

- -

- - < LCL

MALATHION

METABOLITE

Phosphamidon LC/MSMS - - - - 0.01 0.1 0.05

Phoxim LC/MSMS

0.1 - -

Analysis Results

AnalyteAnalyzed

by

Authorized use


mg/kg (ppm)CA CHN

GC/MSMS - - - - 0.01

Indoxacarb GC/MSMS - - - - 0.01

Irgarol LC/MSMS - - - - - -

Iprovalicarb LC/MSMS - - - -

Iprodione GC/MSMS

Isocarbophos

Isazophos LC/MSMS - - - -

- -

< LCL Neburon


P-19-177SUN BELLE MÉXICO S.A. DE C.V. Sample: Blackberry Lab Reg. No.:Client:

Producer: JUAN JAVIER ALVAREZ ORTEGA Orchard:

US JP MX US

Chromatogram GC: P-19-177 01-06-2019.D Chromatogram LC:

Obtained amount in

mg/kg (ppm)

P-19-177 01-04-2019.d MXAgrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab

- - 0.01

LC/MSMS - - - - - - < LCL

0.01 < LCL

0.1

- -GC/MSMS - - - - 0.1

- -

Imiprothrin GC/MSMS - - - - - - - - - -

- - < LCL0.1< LCL

- - - -

LC/MSMS - -0.1

25 25 12 25 - -

0.010.01 GC/MSMS - - - -0.1 - -

< LCL Nitrapyrin

< LCL Nitrothal-isopropyl < LCL

< LCLLC/MSMS - - - - 0.01< LCL Novaluron*0.1

0.1 - - < LCLGC/MSMS - - - - 0.01

Isoprocarb LC/MSMS - -- - - - 0.01 0.1 - -

0.01 0.02

0.01 0.3

0.01 3

- - - -

Isoprothiolane GC/MSMS - - - - 0.01 0.1 - -

< LCL Ofurace < LCLLC/MSMS - -

< LCLLC/MSMS 0.1 0.1 0.1

Isofenphos LC/MSMS - - - - 0.01 0.1 0.01

- - - - < LCLGC/MSMS - - - -

< LCL Omethoate

3

DIMETHOATE

METABOLITE

- - - -

DIMETHOATE

METABOLITE< LCLLC/MSMS

DIMETHOATE

METABOLITE

DIMETHOATE

METABOLITE

DIMETHOATE

METABOLITE

< LCL Ovex

< LCL Oxadiazon

< LCL

Isoxaflutole LC/MSMS - - - - 0.01 0.1 - -

< LCL op Dicofol*** GC/MSMS - - - - 3

- - - - < LCLGC/MSMS - - - - - -

Isoproturon LC/MSMS - - - - 0.01 0.1 - -

Kresoxim-methyl LC/MSMS - - - - 0.01 0.1 - - < LCL

GC/MSMS - - - - 0.01

- - < LCL

Kelthane*** GC/MSMS - - - - 3 3 - -

Linuron LC/MSMS - - - - 0.2 0.1

Leptophos GC/MSMS - - - - - - - - - - < LCL

Lenacil LC/MSMS - - - - 0.3 0.1

< LCL

Malathion GC/MSMS 8 8 8 8 - - < LCL

Malaoxon LC/MSMSMALATHION

METABOLITE

MALATHION

METABOLITE

MALATHION

METABOLITE

MALATHION

METABOLITE

Lufenuron LC/MSMS - - - - 0.01 0.1 - - < LCL

MALATHION

METABOLITE

MALATHION

METABOLITE

0.02 0.5

- - < LCL

Mecarbam LC/MSMS - - - - 0.01 0.1 - - < LCL

Mebendazole LC/MSMS - - - - - - - -

5 < LCL

Mandipropamid LC/MSMS - - - - 0.01 0.1 - - < LCL

Mancozeb LC/MSMS - - - - 5 0.1

- - < LCL

Metazachlor LC/MSMS - - - - 0.01 0.1 - - < LCL

Metamitron LC/MSMS - - - - 0.01 0.1

- - < LCL


enantiomero de metalaxyl)GC/MSMS 0.7 0.7 0.2 0.1 - - 0.675

Mepanipyrim LC/MSMS - - - - 0.01 0.1

0.05 < LCL

Methidathion LC/MSMS - - - - 0.2 0.1 0.05 < LCL

Methamidophos LC/MSMS - - - - 0.01 0.1

- - < LCL

Methabenzthiazuron LC/MSMS - - - - 0.01 0.1 - - < LCLMetconazole LC/MSMS - - - - 0.01 0.1

< LCL

Methomyl LC/MSMS - - - - 1 0.01 0.2 < LCL

Methiocarb sulfoxide GC/MSMS - - - - 0.05 0.1

- - < LCL

Methiocarb sulfone GC/MSMS - - - - 0.05 0.1 - - < LCL

Methiocarb GC/MSMS - - - - 0.05 0.1

Methoxyfenozide LC/MSMS 6 6 0.01 6 - - < LCL

Methoxychlor GC/MSMS - - - - 7 0.1

- - < LCL

Methoprotryne LC/MSMS - - - - - - - - - - < LCL

Methoprene GC/MSMS - - - - 0.01 0.1

0.01 14

LC/MSMS - - - - 0.01 0.1 - -

- - < LCL

Metobromuron LC/MSMS - - - - 0.01 0.1 - - < LCL

Methylpentachlophenyl Sulfide GC/MSMS - - - - - - - -

- - < LCLMetosulam LC/MSMS - - - - 0.01 0.1

- - < LCL

Mevinphos GC/MSMS - - - - 0.01 0.1 - - < LCL

Metsulfuron-methyl LC/MSMS - - - - 0.01 0.1

0.1

Metribuzin GC/MSMS - - - - 0.01 0.1 - - < LCL

Metoxuron LC/MSMS - - - - - - - - - - < LCL

Metrafenone

Molinate LC/MSMS - - - - 0.01 0.1 - - < LCL

Mirex GC/MSMS - - - - 0.01 0.1

- - < LCL

MGK-264 GC/MSMS - - - - - - - - - - < LCL

Mexacarbate LC/MSMS - - - - - - - -

Myclobutanil GC/MSMS 2 2 1 2 - - < LCL

Monuron LC/MSMS - - - - 0.01 0.1

0.03 < LCL

Monolinuron LC/MSMS - - - - 0.01 0.1 - - < LCL

Monocrotophos LC/MSMS - - - - 0.01 0.1

1 1

Napropamide LC/MSMS 0.1 0.1 0.1 0.1 - - < LCL

N-2,4-Dimethylphenyl formamide

(2,4-DMPF)LC/MSMS - - - - - - - - Propachlor LC/MSMS - -- - - -

0.1 0.05

0.1 - - < LCL

Oxadixyl LC/MSMS - - - - 1 0.1 - - < LCL

- - < LCL - - 0.01 0.1 - -

- - < LCL

0.01 < LCL

< LCL

- - < LCL

- - < LCL

- -

Oxydemeton-methyl LC/MSMS - - - - 0.02 0.1 - - < LCL

Oxyfluorfen GC/MSMS 0.05 0.05 0.01 0.1 - - < LCL

Oxamyl LC/MSMS - - - - 0.01 0.1 - - < LCL

Oxamyl Oxime LC/MSMS - - - - - - - - - - < LCL

Paraoxon-methyl LC/MSMS - - - - - - - - - - < LCL

Parathion GC/MSMS - - - - 0.5 0.1 0.01 < LCL

Paclobutrazol (Bonzi) LC/MSMS - - - - 0.01 0.1 - - < LCL

Paraoxon LC/MSMS - - - - - - - - - - < LCL

Parathion methyl GC/MSMS - - - - 0.2 0.1 0.02 < LCL

Penconazol LC/MSMS - - - - 0.2 0.1 - - < LCL

Pencycuron LC/MSMS - - - - 0.01 0.1 - -

- - - - 0.01 0.1 - -

- - - - 0.01 0.1

< LCL

Pendimethalin LC/MSMS 0.1 0.1 0.05 0.1 - - < LCL

- -

- - - - 0.01 0.1 - -

< LCL

< LCL

< LCL< LCL

< LCL

0.179

< LCL

- -

Phorate-sulfoxide

Phosalone

GC/MSMS

GC/MSMS

GC/MSMS

GC/MSMS

GC/MSMS

GC/MSMS

LC/MSMS

LC/MSMS

GC/MSMS

GC/MSMS

LC/MSMS

LC/MSMS

LC/MSMS

Pentachloroaniline

Pentachloroanisol

Pentachloronitrobenzene

Pentachlorophenol

Penthiopyrad

Permethrin

Phenmedipham

Phenthoate

Phenyl valerate

Phorate

Phorate-sulfone

- - 0.02 0.1 - -

QUINTOCENE

(PENTACHLORO

NITROBENZENE

)METABOLITE

QUINTOCENE

(PENTACHLORO

NITROBENZENE

)METABOLITE

QUINTOCENE

(PENTACHLORO

NITROBENZENE

)METABOLITE

QUINTOCENE

(PENTACHLORO

NITROBENZENE

)METABOLITE

QUINTOCENE

(PENTACHLORO

NITROBENZENE

)METABOLITE

- - - - - - - - - -

- - - - 1 0.1 1

- - - -

0.02 0.010.01 - -

0.01 0.5

0.05 5

< LCL

< LCL

< LCL

< LCL

< LCL

< LCL

- - - - 0.05 0.024 0.01

- -

- - - - 0.01 0.1 - -

- - 0.05 0.024 0.01

- - - - - - - - - -

- - - - 0.05 0.024 0.01

Picoxystrobin LC/MSMS - - - - 0.01 0.1 - - < LCL

Piperalin LC/MSMS - - - - - - - - - - < LCL

- - - - 0.01 0.1 - -

< LCL

< LCL

- -

LC/MSMS - - - - 0.01 0.1 - - < LCLPicolinafen

Pirimicarb LC/MSMS - - - - 0.5 0.1 1 < LCL

Pirimiphos-ethyl LC/MSMS - - - - 0.01 0.1 - - < LCL

Piperonyl Butoxide LC/MSMS 8 8 8 8 - - < LCL

Piperophos LC/MSMS - - - - 0.01 0.1 - - < LCL

Prochloraz LC/MSMS - - - - 0.05 0.1 - - < LCL

Procymidone GC/MSMS - - - - 0.01 0.1 - - < LCL

Pirimiphos-methyl LC/MSMS - - - - 0.1 0.1 - - < LCL

Primisulfuron-methyl LC/MSMS - - - - 0.01 0.1 - - < LCL

- - - - - - - - < LCL

Prometon GC/MSMS - - - - - - - - - - < LCL

Profenofos GC/MSMS - - - - 0.01 0.1 - - < LCL

Profluoralin GC/MSMS - - - - - - - - - - < LCL

CHNKOR

< LCL

Propamocarb LC/MSMS - - - - 0.01 0.1 - - < LCL

Prometryn GC/MSMS - - - - 0.01 0.1 - - < LCL

Pronamide LC/MSMS - - - - - - - - - - < LCL

0.01 0.1

Promecarb GC/MSMS - -

* Analyte not declared in the scope accredited and / or licensed accredited obtained by method and / or authorized. The colored bands are visual aids based on MRLs of Mexico and are not a result. 1Maximum Resuide Limits (MRL) expressed in ppm for every country using ISO 3166-1 alfa-2. LCL = Lowest Calibration Level ppm = Parts per million = mg/kg GC/MSMS = Gass Chromatography /Mass/Mass LC/MSMS = Liquid Chromatography /MassMass

Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued result only affects the sample received at the facility of Análisis Técnicos S.A. de C.V, therefore it́ s not responsible for the representation of the result for the total

product. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.





General Director

B BB BB BB BB BB BB BB BB BB BB B

B B

B BB BB BB BB BB BB BB B

B B

B B

B B

B B

B BB B

B B

B B

B B

B B

B B

B

B

B VB VB VB VB VB VB VB VB V

B V

B

B

B

B

B

BBB

B

B

B

B

B

BBBB0.01 0.05 - - < LCLThifensulfuron-methyl LC/MSMS - - - - 0.01 0.1

- - < LCLThidiazuron LC/MSMS - - - - 0.01 0.1 0.01 0.2

0.01 1 - - < LCLThiamethoxam LC/MSMS 0.35 0.35 0.5 0.5

1 < LCLThiacloprid LC/MSMS - - - - 5 0.1 1 0.7

0.01 3 - - < LCLThiabendazole LC/MSMS - - - - 3 0.1

- - < LCLTetramethrin LC/MSMS - - - - 0.01 0.1 0.01 - -

CAPTAN

METABOLITE

CAPTAN

METABOLITE

CAPTAN

METABOLITE< LCL

Tetrahydrophthalimide, cis-1,2,3,6-

(THPI)GC/MSMS

CAPTAN

METABOLITE

CAPTAN

METABOLITE

CAPTAN

METABOLITE

CAPTAN

METABOLITE

- - < LCLTetradifon GC/MSMS - - - - 1 0.1 0.01 1

0.01 - - - - < LCLTetrachlorvinphos, E-isomer GC/MSMS - - - - 0.01 0.1

- - < LCLTerrazole GC/MSMS - - - - - - - - - - - -

0.01 0.05 - - < LCLTerbutryn GC/MSMS - - - - 0.01 0.1

- - < LCLTerbuthylazine-desethyl LC/MSMS - - - - - - - - - - - -

0.05 0.1 - - < LCLTerbuthylazine GC/MSMS - - - - 0.01 0.1

- - < LCLTerbumeton LC/MSMS - - - - - - - - - - - -

0.01 0.1 - - < LCLTerbacil GC/MSMS 0.2 0.2 0.1 0.1

- - < LCLTeflubenzuron LC/MSMS - - - - 0.01 0.1 0.01 2

0.01 1 - - < LCLTecnazene GC/MSMS - - - - 0.05 0.1

- - < LCLTebuthiuron LC/MSMS - - - - 0.01 0.1 0.01 - -

0.01 - - - - < LCLTebutam LC/MSMS - - - - 0.01 0.1

- - < LCLTebufenpyrad GC/MSMS - - - - 2 0.1 0.05 0.5

0.05 2 - - < LCLTebufenozide LC/MSMS 3 3 3 0.1

- - < LCLTebuconazole GC/MSMS - - - - 0.01 0.1 0.5 0.5

0.02 0.1 - - < LCLSumithrin GC/MSMS - - - - 0.01 0.1

- - < LCLSulfoxaflor LC/MSMS - - - - 0.01 0.1 0.01 0.5

0.01 - - 0.01 < LCLSulfotep LC/MSMS - - - - 0.01 0.1

- - < LCLSulfosulfuron LC/MSMS - - - - 0.01 0.1 0.01 - -

0.01 0.05 - - < LCLSulfentrazone LC/MSMS 0.15 0.15 0.05 0.15

- - < LCLSpiroxamine LC/MSMS - - - - 0.01 0.1 0.01 3

0.1 3 - - < LCLSpirotetramat LC/MSMS - - - - 0.01 2

5 0.1 0.01 5 - - < LCL- - < LCL Vinclozolin GC/MSMS - - - -

- - < LCL

Spiromesifen LC/MSMS - - - - 0.01 0.1 0.02 2

- - - - 0.01 0.1 0.01 0.050.02 1 - - < LCL Vamidothion LC/MSMSSpirodiclofen LC/MSMS - - - - 0.01 0.1

0.01 0.1 0.01 - - - - < LCL1 < LCL Uniconazole GC/MSMS - - - -

- - < LCL

Spinosad A LC/MSMS 1 1 1 0.5 1.5 1

- - - - - - - - - - - -1 0.7 - - < LCL Trimidal LC/MSMSSpinetoram J LC/MSMS 0.8 0.8 0.7 0.5

0.01 0.1 0.01 0.5 - - < LCL- - < LCL Triforine LC/MSMS - - - -

- - < LCL

S-Metolachlor LC/MSMS 0.1 0.1 0.01 0.1 0.05 0.1

- - - - 0.01 0.1 0.01 - -0.01 0.05 - - < LCL Triflusulfuron-methyl LC/MSMSSimetryn LC/MSMS - - - - 0.01 0.1

0.05 0.1 0.01 0.05 - - < LCL- - < LCL Trifluralin GC/MSMS - - - -

- - < LCL

Simazine GC/MSMS 0.2 0.2 0.2 0.1 0.01 0.25

- - - - 0.02 0.1 0.01 0.50.1 1 - - < LCL Triflumuron LC/MSMSSethoxydim* LC/MSMS 5 5 1 5

0.01 0.1 0.02 2 - - < LCL- - < LCL Triflumizole LC/MSMS - - - -

- - < LCL

Sebuthylazine GC/MSMS - - - - - - - - - - - -

- - - - 0.01 0.1 3 10.01 - - - - < LCL Trifloxystrobin LC/MSMSRotenone LC/MSMS - - - - 0.01 0.1

- - - - - - - - - - < LCL- - < LCL Trietazine LC/MSMS - - - -

- - < LCL

Rimsulfuron LC/MSMS 0.01 0.01 0.01 0.01 0.01 - -

- - - - 0.01 0.1 0.01 0.20.05 0.05 - - < LCL Tricyclazole GC/MSMSQuizalofop-ethyl LC/MSMS - - - - 0.05 0.1

- - - - - - - - - - < LCL- - < LCL Triclocarban LC/MSMS - - - -

- - < LCL

Quinoxyfen LC/MSMS - - - - 0.01 0.1 0.02 2

- - - - - - - - - - - -0.01 0.01 - - < LCL Trichloronate GC/MSMSQuinalphos LC/MSMS - - - - 0.02 0.1

0.5 0.1 0.01 0.05 0.2 < LCL- - < LCL Trichlorfon LC/MSMS - - - -

- - < LCL

Pyriproxyfen GC/MSMS 1 1 0.01 0.1 0.05 1

- - - - - - - - - - - -15 15 - - < LCL Tributyl phosphate GC/MSMSPyrimethanil LC/MSMS 15 15 10 15

0.01 0.1 0.01 - - - - < LCL- - < LCL Tribenuron-methyl LC/MSMS - - - -

- - < LCL

Pyridaphenthion GC/MSMS - - - - 0.01 0.1 0.01 0.2

- - - - 0.01 0.1 0.01 0.050.01 1 - - < LCL Triazophos GC/MSMSPyridalyl GC/MSMS - - - - 0.01 0.1

0.01 0.1 0.05 - - - - < LCL- - < LCL Triasulfuron LC/MSMS - - - -

- - < LCL

Pyridaben LC/MSMS - - - - 0.01 0.1 0.5 1

- - - - - - - - - - - -0.01 1 - - < LCL Triallate GC/MSMSPyrazophos LC/MSMS - - - - 0.01 0.1

0.5 0.1 0.01 0.5 - - < LCL- - < LCL Triadimenol GC/MSMS - - - -

- - < LCL

Pyraclostrobin LC/MSMS 4 4 3 3.5 3 3

- - - - 0.1 0.1 0.01 0.053 0.5 - - < LCL Triadimefon GC/MSMSPymetrozine LC/MSMS - - - - 0.01 0.1

5 0.1 0.02 2 5 < LCL- - < LCL Tolyfluanid GC/MSMS - - - -

- - < LCL

Prosulfuron LC/MSMS - - - - 0.01 0.1 0.01 - -

- - - - - - - - - - - -0.01 0.08 - - < LCL Tolchlofos methyl GC/MSMSProsulfocarb LC/MSMS - - - - 0.01 0.1

- - - - - - - - - - < LCL- - < LCL Tokution GC/MSMS - - - -

- - < LCL

Propyzamide LC/MSMS 0.05 0.05 0.01 0.1 0.01 0.05

- - - - 3 6 0.1 20.05 0.05 - - < LCL Thiophanate-methyl LC/MSMSPropoxur LC/MSMS - - - - 1 0.1

- - - - - - - - - - < LCL- - < LCL Thionazin LC/MSMS - - - -

< LCL

- - < LCL

Propiconazole GC/MSMS 1 1 0.05 1 0.01 0.3

- - - - - - - - - - - -0.01 - - - - < LCL Thiofanox Sulfoxide LC/MSMSPropetamphos LC/MSMS - - - - 0.01 0.1

0.05

1 0.1 0.01 1 - - < LCL- - < LCL Thiodicarb LC/MSMS - - - -

- - < LCL

Propazin GC/MSMS - - - - 0.01 0.1 0.01 - -

- - - - 3 0.1 0.01 10.01 7 - -

Obtained amount in

mg/kg (ppm)Analyte

Analyzed

by

Authorized use


mg/kg (ppm)

Thiocyclam hydrogen oxalate GC/MSMSPropargite (Omite) LC/MSMS - - - - 0.01 0.1

0.01 0.1 0.01 0.05 - - < LCL- - < LCL Thiobencarb LC/MSMS - - - -Propanil LC/MSMS - - - - 0.1 0.1 0.01

KOR CHN

Producer: JUAN JAVIER ALVAREZ ORTEGA Orchard: ZIRACUARETIRO SAGARPA Reg.: SD

Client: SUN BELLE MÉXICO S.A. DE C.V. Sample: Blackberry Lab Reg. No.: P-19-177

CHN MX US JP CA EUMX US JP CA EU KOR

Analysis ResultsBanned pesticides residues have been detected

AnalyteAnalyzed

by

Authorized use

MRL (ppm)


JP CA EU KOR CHNAgrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab

Chromatogram GC: P-19-177 01-06-2019.D Chromatogram LC: P-19-177 01-04-2019.d MX US

* Analyte not declared in the scope accredited and / or licensed accredited obtained by method and / or authorized. The colored bands are visual aids based on MRLs of Mexico and are not a result. 1Maximum Resuide Limits (MRL) expressed in ppm for every country using ISO 3166-1 alfa-2. LCL = Lowest Calibration Level ppm = Parts per million = mg/kg GC/MSMS = Gass Chromatography /Mass/Mass LC/MSMS = Liquid Chromatography /MassMass

Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued result only affects the sample received at the facility of Análisis Técnicos S.A. de C.V, therefore it́ s not responsible for the representation of the result for the total

product. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.





General Director

Vamidothion

Vinclozolin

Triflumuron 0.010

Heptachlor 0.010

Heptachlor exo-epoxide (isomer B) 0.020

Heptenophos 0.005

Fosthiazate 0.005

Fuberidazole 0.005Furathiocarb 0.005g Chlordan 0.010Haloxyfop-methyl 0.005

Fluvalinate 0.010

Fluxapyroxad 0.005

Folpet 0.010

Forchlorfenuron 0.005

Formetanate 0.005

Fluridone 0.010

Flurtamone 0.005

Flusilazole 0.005

Flutolanil 0.010

Flutriafol 0.005

Fluometuron 0.005

Fluopicolide 0.005

Fluopyram 0.010

Fluoroglycofen-ethyl 0.005

Fluoxastrobin 0.005

Flucythrinate 0.010

Fludioxonil 0.010

Flufenacet 0.005

Flufenoxuron 0.005

Flumiclorac-pentyl 0.010

Flazasulfuron 0.005

Flonicamid 0.010

Fluazifop-butyl 0.005

Flubendiamide 0.010

Fluchloralin 0.010

Fenthion 0.010

Fenuron 0.005

Fipronil 0.020

Flamprop methyl 0.010

Flamprop-isopropyl 0.010

Fenpropidin 0.005

Fenpropimorph 0.005

Fenpyroximate 0.005

Fenson 0.020

Fensulfothion 0.010

Analyte LCL (ppm)

Fenoxaprop-ethyl 0.005

Fenoxycarb 0.005

Fenpropathrin 0.010

Trietazine 0.005

Trifloxystrobin 0.005

Methidathion 0.005 Penthiopyrad 0.010 Spirodiclofen 0.005

0.010 Pencycuron 0.005 Sethoxydim* 0.010

Mecarbam 0.005 Parathion methyl 0.010 Rotenone 0.005

Triflumizole 0.005

Methiocarb sulfone 0.010 Phenmedipham 0.005 Spirotetramat 0.005

Methiocarb 0.020 Permethrin 0.010 Spiromesifen 0.005

Trifluralin 0.010

Triflusulfuron-methyl 0.005

Triforine 0.010

Trimidal 0.005

Uniconazole 0.010

0.005

0.010

Methomyl 0.005 Phenyl valerate 0.010 Sulfentrazone 0.005

Methiocarb sulfoxide 0.020 Phenthoate 0.005 Spiroxamine 0.005

Methoprotryne 0.005 Phorate-sulfone 0.005 Sulfotep 0.005

Methoprene 0.010 Phorate 0.010 Sulfosulfuron 0.005

Methoxyfenozide 0.005 Phosalone 0.010 Sumithrin 0.020

Methoxychlor 0.010 Phorate-sulfoxide 0.005 Sulfoxaflor 0.005

Metobromuron 0.010 Phoxim 0.010 Tebufenozide 0.005

Methylpentachlophenyl Sulfide 0.010 Phosphamidon 0.005 Tebuconazole 0.010

0.005 Tebutam 0.005

Metolachlor 0.005 Picolinafen 0.005 Tebufenpyrad 0.010

Metoxuron 0.005 Piperonyl Butoxide 0.005 Tecnazene 0.010

Metosulam 0.005 Piperalin 0.005 Tebuthiuron 0.005

Tricyclazole 0.010

Triclocarban 0.010

Trichloronate 0.010

Trichlorfon 0.005

Report Date 2019-01-07 Page 6 of 7 Revision: AR272-TS-70


Lowest Calibration Level per analyteAnalyte LCL (ppm) Analyte LCL (ppm) Analyte LCL (ppm) Analyte LCL (ppm)

Dimethoate 0.010

2, 4-D Methyl ester 0.010 Bromophos methyl 0.010 Coumaphos 0.010 Dimethomorph 0.0051-Naphthol 0.010 Bromacil 0.010 Clothianidin 0.005

Dimethylphenol, 2,4- (2,4-xylenol) 0.010

2,6 Dichlorobenzonitrilo 0.010 Bromuconazole* 0.010 Cyanazine 0.005 Diniconazole 0.005

2,3 dihydro-2,2dimethylbenzofuran

7-ol0.020 Bromopropylate 0.010 Crimidine 0.005

Dinotefuran 0.005

3,4 Dichloroaniline 0.010 Buprofezin 0.010 Cyazofamid 0.005 Dioxathion 0.0102,6-Dichlorobenzamide 0.005 Bupirimate 0.005 Cyantraniliprole 0.005

Diphenamid 0.005

Abamectin 0.005 Butocarboxim* 0.010 Cyflufenamid 0.010 Diphenylamine 0.0103-Hydroxy carbofuran 0.005 Butachlor 0.010 Cycloate 0.005

Disulfoton 0.010

Acetamiprid 0.005 Buturon 0.005 Cyfluthrin 0.010 Disulfoton sulfone 0.010Acephate 0.005 Butocarboxim-sulfoxide 0.005 Cyflumetofen 0.005

Disulfoton sulfoxide 0.010

Aclonifen 0.010 Cadusafos 0.010 Cymoxanil 0.005 Diuron (Karmex) 0.005

Acetochlor 0.005 Butylate 0.020Cyhalothrin (Isomero Lambda y

gamma)**0.010

Dodemorph 0.005

Alachlor 0.005 Carbaryl 0.010 Cyproconazole 0.005 Dyfonate 0.010

Acrinathrin 0.020 Captan 0.010Cypermethrin a (Zeta-

Cypermethrin)**0.010

Edifenphos 0.005

Aldicarb sulfone 0.005 Carbetamide 0.005 Cyromazine 0.005 Emamectin Benzoate 0.005Aldicarb 0.005 Carbendazim 0.005 Cyprodinil 0.010

Endosulfan I (alpha isomer) 0.010

Aldrin 0.010 Carboxin 0.005 DDD-p,p 0.010 Endosulfan II (beta isomer) 0.010Aldicarb-sulfoxide (Aldoxicarb) 0.005 Carbofuran 0.010 DDD-o,p 0.010

Endosulfan sulfato 0.010

Ametryn 0.010 Chinometionate 0.010 DDE-p,p 0.010 Endrin 0.010Ametoctradin 0.005 Carfentrazone ethyl 0.005 DDE-o,p 0.010

Epoxiconazole 0.005

Aminocarb 0.005 Chlorbromuron 0.005 DDT-p,p 0.010 EPTC 0.010Amicarbazone 0.005 Chlorantraniliprole 0.005 DDT-o,p 0.010

Esfenvalerate + Fenvalerate (**) 0.010

Atrazine-2-hydroxy 0.005 Chlordimeform 0.010 Deltamethrin 0.010 Etaconazole (Etaconazole I y II) 0.010Atrazine 0.010 Chlordane- a 0.010 DEET (Diethyl-m-toluamide, N,N-) 0.010

Ethalfluralin 0.010

Azinphos-ethyl 0.005 Chlorfenvinphos 0.005 Demeton S 0.010 Ethiofencarb 0.005Azamethiphos 0.005 Chlorfenapyr 0.010 Demeton O 0.010

Ethiofencarb-sulfone 0.005

Azoxystrobin 0.010 Chloridazon (Pyrazon) 0.005 Desmedipham 0.005 Ethirimol 0.005Azinphos-Methyl 0.005 Chlorfluazuron 0.005 Demeton-s-methyl-sulfone 0.005

Ethoprop 0.010

Benalaxyl 0.010 Chlormequat 0.005 Dialifos 0.005 Ethylan 0.010Baycarb 0.005 Chlorimuron-ethyl 0.005 Desmetryn 0.010

Etion 0.010

Benfluralin 0.010 Chloroneb 0.010 Dichlofluanid 0.010 Etofenprox 0.010Bendiocarb 0.005 Chlorobenzilate 0.010 Diazinon 0.010

Etoxazole 0.005

Bensulide 0.005 Chlorothalonil 0.010 Dichlorvos 0.010 Famoxadone 0.010Bensulfuron-methyl 0.005 Chloropropylate 0.010 Dichloran 0.010

Fenamidone 0.010

Benzoximate 0.005 Chloroxuron 0.005 Diclofop methyl 0.020 Fenamiphos 0.005Benthiavalicarb-isopropyl 0.005 Chlorotoluron 0.005 Diclobutrazol* 0.010

Fenamiphos Sulfone 0.005

BHC lindane beta 0.010 Dieldrin 0.010 Fenamiphos Sulfoxide 0.005BHC lindane alpha 0.010 Chlorpropham 0.010 Dicrotophos 0.005

Fenarimol 0.005Chlorpyrifos 0.010

BHC lindane gamma 0.010 Difenoconazole 0.005 Fenazaquin 0.005BHC lindane delta 0.010 Diethofencarb 0.005Chlorpyrifos methyl 0.010

Chlorsulfuron 0.005Fenbuconazol 0.005

Bifenox 0.020 Chlorthiophos 0.020 Diflufenican 0.005 Fenbutatin oxide* 0.010Bifenazate 0.005 Chlortal dimethyl 0.010 Difenoxuron 0.005

Fenchlorphos 0.010Bitertanol 0.005 Clofentezine 0.005 Dimepax 0.010 Fenfuram 0.005Bifenthrin 0.010 Clodinafop-propargyl 0.005 Dimefuron 0.005

Fenhexamid 0.005

Boscalid 0.005 Cloquintocet-mexyl 0.005 Dimethenamid 0.005 Fenitrothion 0.020

Bolstar 0.010 Clomazone 0.005 Dimethachlor 0.005

Analyte LCL (ppm)

Hexachlorobenzene 0.010 Mevinphos 0.010 Pirimiphos-methyl 0.005 Terbuthylazine 0.010

Analyte LCL (ppm) Analyte LCL (ppm) Analyte LCL (ppm)

Terbuthylazine-desethyl 0.005

Hexaflumuron 0.005 MGK-264 0.010 Prochloraz 0.005 Terbutryn 0.010

Hexaconazole 0.005 Mexacarbate 0.005 Primisulfuron-methyl 0.005

Terrazole 0.010

Hexythiazox 0.005 Molinate 0.005 Profenofos 0.010 Tetrachlorvinphos, E-isomer 0.010

Hexazinone 0.010 Mirex 0.010 Procymidone 0.010

Tetradifon 0.010

Imazapyr 0.005 Monolinuron 0.005 Promecarb 0.010Tetrahydrophthalimide, cis-1,2,3,6-

(THPI)0.010

Imazalil 0.005 Monocrotophos 0.005 Profluoralin 0.020

Tetramethrin 0.005

Imidacloprid 0.005 Myclobutanil 0.010 Prometryn 0.010 Thiabendazole 0.005

Imazaquin 0.005 Monuron 0.005 Prometon 0.010

Thiacloprid 0.005

Imiprothrin 0.020 Napropamide 0.005 Propachlor 0.005 Thiamethoxam 0.005

Imidan 0.010N-2,4-Dimethylphenyl formamide

(2,4-DMPF)0.010 Pronamide 0.005

Thiodicarb 0.005

Thidiazuron 0.005

Iprodione 0.010 Nicosulfuron 0.005 Propanil 0.005 Thifensulfuron-methyl 0.005

Indoxacarb 0.010 Neburon 0.005 Propamocarb 0.005

Thiobencarb 0.010

Irgarol 0.005 Nitrothal-isopropyl 0.010 Propazin 0.010 Thiocyclam hydrogen oxalate 0.010

Iprovalicarb 0.005 Nitrapyrin 0.010 Propargite (Omite) 0.005

Isocarbophos 0.010 Norflurazon-Desmethyl 0.010 Propiconazole 0.010Isazophos 0.010 Norflurazon 0.005 Propetamphos 0.005

0.005

0.005

Isoproturon 0.005 Omethoate 0.005 Prosulfuron 0.005

Isoprothiolane 0.010 Ofurace 0.005 Prosulfocarb 0.005

Isoprocarb 0.005 O Phenylphenol 0.010

Isofenphos 0.005 Novaluron* 0.010 Propoxur

Propyzamide

Kelthane*** 0.010 Ovex 0.010 Pyraclostrobin 0.005

Isoxaflutole 0.010 op Dicofol*** 0.010 Pymetrozine 0.005

Lenacil 0.005 Oxadixyl 0.005 Pyridaben 0.005

Kresoxim-methyl 0.005 Oxadiazon 0.010 Pyrazophos 0.005

Linuron 0.005 Oxamyl Oxime 0.005 Pyridaphenthion 0.010

Leptophos 0.010 Oxamyl 0.005 Pyridalyl 0.010

Malaoxon 0.005 Oxyfluorfen 0.010 Pyriproxyfen 0.010

Lufenuron 0.005 Oxydemeton-methyl 0.005 Pyrimethanil 0.005

Mancozeb 0.005 Paraoxon 0.005 Quinoxyfen 0.005

Malathion 0.010 Paclobutrazol (Bonzi) 0.005 Quinalphos 0.005

0.010 Rimsulfuron 0.005

Mandipropamid 0.005 Paraoxon-methyl 0.005 Quizalofop-ethyl 0.005

Metsulfuron-methyl 0.005 Pirimiphos-ethyl 0.005 Terbumeton 0.005

Methamidophos 0.005 Pentachlorophenol 0.010 Spinosad A 0.005

Metribuzin 0.010 Pirimicarb 0.005 Terbacil 0.010

Metrafenone 0.005

Metolcarb 0.010 Picoxystrobin

Piperophos 0.005 Teflubenzuron 0.010

0.005

0.010

0.005

0.010

Thiofanox Sulfoxide

Thionazin

Thiophanate-methyl

Tokution

Methabenzthiazuron 0.005 Pentachloronitrobenzene 0.010 Spinetoram J 0.005

0.010

Metazachlor 0.005 Pentachloroaniline 0.010 Simetryn 0.005

Triadimenol

Triallate

Metconazole

0.005

0.005

0.005

0.010

0.010

0.010

0.010

0.010

0.010

Tolchlofos methyl

Tolyfluanid

Triadimefon

0.005

Metamitron 0.005

Triasulfuron

Triazophos

Tribenuron-methyl

Tributyl phosphate

0.005 Pentachloroanisol 0.010

Mepanipyrim 0.010 Penconazol 0.005 Sebuthylazine

Pendimethalin 0.005 Simazine

S-Metolachlor

0.010


enantiomero de metalaxyl)

Mebendazole 0.005 Parathion

Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued result only affects the sample received at the facility of Análisis Técnicos S.A. de C.V, therefore it́ s

not responsible for the representation of the result for the total product. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.



ppm = Parts per million = mg/kg Uncertainty = 50 % according to "Method validation and quality control procedures for pesticide residues analysis in food and feed". No. de Documento SANCO/10684/2009. Punto 91

Data corresponding to page 2, page 3, page 4 and page 5

Report Date: 2019-01-07 Page: 7 of 7 Revision AR272-TS-70

End of Report


Additional and complementary information

General Information

1. The customer has five calendar days of issuance of the results**** in order to make any comment or complaint about it, because if not done within this time period will be considered this

report has been accepted.

2. Samples may be disposed within 5 days after the issue of results**** only samples for microbiological analysis shall be discarded 24 hours after being received

3. The information recorded in this "Report test results" is treated with strict adherence to privacy notice Análisis Técnicos S.A. de C.V complying with Articles third transient, 16 and 17 of Law

Protection Federation Personal Data Held by Private Parties, in order to regulate their treatment legitimate, controlled and reported, in order to ensure privacy and the right to self-determination

informative individuals.

4.Análisis Técnicos S.A. de C.V not have the authority, or the right to deny, accept or approve cuts or harvests.

5. Análisis Técnicos S.A. de C.V. is not accredited in sampling.

6. MRLs of the countries are a reference data, requesting check the official sites of each country and that can be changed or modified.

7. The result represents the sample that was received on the premises of Análisis Técnicos S.A. de C.V , which is not responsible for the representation of the result for the total product

8. This form of interpretation is protected and registered with the Instituto Nacional del Derecho de Autor (INDAUTOR), likewise, logos and Agrolab name and its subsidiaries are registered with

the Instituto Mexicano de la Propiedad Intelectual (IMPI). Reproduction is prohibited in whole or in part, for any purpose other than the interpretation of results, without permission.

9. This report is not valid if you have scratches, erasures or amendments.

10. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.

11. Análisis Técnicos S.A. de C.V. It is not responsible for updating the MRL's because they are considered as a piece of information. It is your responsibility to review the report LMR official

sites for each country since the information can be changed or modified.

12. The detection of the pesticide residue above the quantification limit is reported as ppm (mg / kg), below the limit of quantification reported as <LCL ppm (mg / kg) and below the LD is

considered as undetermined.

**** The issuance of the results includes the final report in PDF format. Delivering results to the client, is subject to confirmation of payment.


References

International Maximum Residue Level Database

http://www.mrldatabase.com/

EU Pesticides Database

http://ec.europa.eu/sanco_pesticides/public/index.cfm

Electronic Code of Federal Regulation

http://ecfr.gpoaccess.gov/cgi/t/text/text-idx?

Health Canada

http://pr-rp.hc-sc.gc.ca/mrl-lrm/index-eng.php

Normas Alimentarias FAO/OMS

http://www.codexalimentarius.net/pestres/data/pesticides/search.html

Positive List System for Agricultural Chemical Residues in Foods (Japón)

http://m5.ws001.squarestart.ne.jp/foundation/search.html

1. The laboratory Análisis Técnicos S.A. de C.V. is accredited before EMA, in the test of determination of residues of pesticides in fruits, vegetables, agricultural food and seeds (incorporating

QuEChERS extraction), by GASS CHROMATOGRAPHY / MASS / MASS to the ISO / IEC 17015:2005.

2. The laboratory Análisis Técnicos S.A. de C.V. is accredited before EMA, in the test of determination of residues of pesticides in fruits, vegetables, agricultural food and seeds (incorporating

QuEChERS extraction), by LIQUID CHROMATOGRAPHY / MASS / MASS to the ISO / IEC 17015:2005.

3. * = Analyte not declared in the scope accredited and / or licensed accredited obtained by method and / or authorized.

4.Authorized use of the pesticide in the relevant country code specified in ISO 3166-1 alpha-2. RML for each country are indicated in the same results table.

5. If no pesticide was detected a green band is shown. If a pesticide was detected within the allowed limits a yellow band is shown. If a pesticide was detected outside of the allowed limits a red

band is shown. If a forbidden pesticide was detected a red band is shown.

6. The colored bands are visual aids based on MRLs of each country and are not a result.

7. ** = The MRL of Isomero Lambda is taken for the molecule Cyhalothrin (Isomero Gamma and Lambda), for Cypermethrin a (Zeta-Cypermethrin) the MRL for Zeta-Cypermethrin is taken and

for the MRL for Esfenvalerate + Fenvalerate, the one for Esfenvalerate is taken.

8. 2 =For Canada the MRL of 0.1 ppm default is considered according to the point 5.2.1.4.2 Food and Drug Regulations of the Canada Food Inspection Agency

http://www.inspection.gc.ca/food/meat-and-poultry-products/manual-of-procedures/chapter-5/eng/1395150894222/1395150895519?chap=2.

9. *** = Dicofol MRL is the sum of p, p-dicofol and o, p-dicofol.

10. The color bands of each molecule are visual support based on the MRLs of each country and do not represent a result.

Information corresponding to page 5 and 6

1. In the corresponding table it´s represented the lower calibration poing (LCL).

2.The correspondig table is NOT A RESULT. It represents quality information data.

3. Uncertainty = 50 % according to "Method validation and quality control procedures for pesticide residues analysis in food and feed". No. de Documento SANCO/10684/2009. point 91

Glosario

GC/MSMS = Gass/Mass/Mass AGILENT 225/MS, 240/MS

LC/MSMS = Liquid/Mass/Mass QQQ (AGILENT 6460)

LCL = Lowest Calibration Level

MRL = Maximum Resuide Limits

ppm = Parts per million = mg/Kg

SD = No Data

Traces = < 0.010 ppm.

MX= Mexico

US= United States

JP= Japan

CA= Canada

EU= European Union

KOR= Korea

CHN= China

Maximum Residue Limits (MRLs) for Blackberry listed in The Official Catalog of Mexico

Pesticide 2004.

Maximum Residue Limits (MRLs) for Blackberry indicated in Environmental Protection

Agency (EPA) United States.

Maximum Residue Limits (MRLs) for Blackberry indicated in Electronic Code of Federal

Regulations (e-CFR TM) United States.

Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued result only affects the sample received at the facility of Análisis Técnicos S.A.

de C.V, therefore it´s not responsible for the representation of the result for the total product. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.

This form of interpretation is protected and registered with the Instituto Mexicano de la Propiedad. Its total or partial reproduction without authorization is prohibited. This report will not be valid if you have scratches, erasures or amendments.



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