Fecha de reporte: 2018-10-15 Página: Revisión:...

Destino Final:

Observaciones:

LA TIJERA, LOS REYES MICH

Aleatorio

EUA Y EU

La muestra se recibió en condiciones para su análisis.

2906-01 SECTOR 1

Estado: Michoacán Código postal: 60330

Ext. 133

60330

[email protected], [email protected],

[email protected]

Información de Facturación

Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab

Fruits-Giddings SA de CV

Km. 1 Carretera los Reyes- Jacona Sn

Michoacán

Razón social:


2018-10-15 Página: 1 de 7 Revisión: AR271-TS-61

Empresa:

Correo electrónico:

Fecha de reporte:

SUN BELLE MÉXICO S.A. DE C.V.

Dirección: Km 1 Carr. los Reyes-Jacona S/N Ciudad o Localidad: Los Reyes

Solicitante: ALFREDO OSEGUERA DÍAZ


[email protected],

[email protected]

Teléfono: 3545427328

Información del Cliente

Domicilio Fiscal:

Estado:

RFC: SBM040520QN6

Ciudad o Localidad: Los Reyes

Código postal:

Analisis Multiresidual de Pesticidas

Nombre común:

Libro de registro:

Rubus Ulmifoli

oct-18P-18-24827No. Reg. de Muestra:

Fecha de recepción:


Nombre científico: Variedad:

Fecha de Término:Fecha de inicio: 2018-10-11

Información de la Muestra

Zarzamora

Ext. SD Correo electrónico:


Telefono: 3545420170

2018-10-15

Menos de 1.5kg

SD

Tupy|Otras

2018-10-11

Parte analizada:

Productor:

Lugar de muestreo:

Uso comercial:

Fruto

NEFTALI ARMANDO GONZALEZ

VAZQUEZ

Fecha de muestreo: 10/09/2018

SD

SD

Estado de la muestra:

Lugar de cosecha:

Método de muestreo:

Destino Comercial:

Cantidad recibida:

Registro SAGARPA:

RFC de Bodega:

Aduana:Mercado Nacional y Extranjero

Congelado

DIRECCION: LOS REYES,

MICHOACÁN

Humano

Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El resultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A. de C.V. , por lo cual no se hace

responsable de la representatividad del resultado para el total del producto. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.

Este formato de interpretación esta protegido y registrado ante el Instituto Mexicano de la Propiedad Intelectual. Se prohibe su reproducción total o parcial sin autorización. El presente informe de resultados no será valido si presenta raspaduras, tachaduras o enmendaduras.

Documento controlado ISO/IEC 17025:2005

Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]

B B

B B

B B

B B

B B

B BB BB B

B B

B BB BB BB BB B

B B

B BB BB BB BB BB BB B

B B

B BB BB BB BB B

B B

B B

B B

B B

B V

B B

B B

B BB BB B

B B

B BB B

B B

B B

B B

B B

B B

B B

B BB BB BB B

B B

B B


1.5 0.5

- - - -

- - - -

- -

- - - -

0.1 0.7

- - - -

0.01 0.1

OXYDEMETON

METHYL

METABOLITE

OXYDEMETON

METHYL

METABOLITE

0.01 - -

- - - -

- -

0.01 0.05

- - - -

0.05 0.1

0.01 - -

0.01 0.01

- - - -

- -

0.01 - -

- - - -

0.01 - -

0.01 0.7

0.01 2

0.01 - -

0.02 1

0.2 0.5

3 1

0.5

0.5 2

0.05 0.1

0.05 0.05

- - - -

- - - -

1

0.01 - -

0.01 - -

0.01 0.05

0.01 0.4

0.01 1

0.05 0.1

- - - -

- - - -

- -

0.01 0.5

0.01 0.05

0.01 0.3

0.1 - -

0.01 1

0.02 0.02

0.01 - -

- - - -

0.5

THIOPHANATE

METHYL/

BENOMYL

METABOLITE

THIOPHANATE

METHYL/ BENOMYL

METABOLITE

0.01 - -

0.01 0.05

0.05

0.01 0.1

0.01 0.05

1 0.7

- - - -

0.01

0.01

0.01

0.02

0.01

- -

- -

5

0.01 0.1

- - - -

0.01 5

0.05 - -

0.01 - -

0.01 - -

- - - -

0.01 - -

0.01 0.02

0.01 - -

0.01 0.5

0.01 0.01

0.01 0.01

0.01 0.01

0.01 0.01

0.05

1 1

2 0.3

0.01 0.02

0.02 1

0.01 0.05

0.02 0.02

0.02 0.02

0.02 0.02

0.05

0.01 0.02

Chlordimeform - - 0.01

- - < LCL

Chloroneb GC/MSMS

0.05 < LCL

SD

CA EU

< LCL

0.01 < LCL

- - < LCL

- - < LCL

0.05

0.01 0.1 - - < LCL

- - - - 0.01 0.1 - - < LCL

Chlorobenzilate GC/MSMS

Fecha de reporte: 2018-10-15

Resultados de AnálisisSe han detectado residuos de pesticidas prohibidos

Analizado

mediante

equipo

Uso autorizado

LMR (ppm)

Reg. Sagarpa:

No. Reg. Lab.:

Cantidad obtenida en mg/kg

(ppm)MX US JP CA CHN

Cantidad obtenida en mg/kg

(ppm)Analito Analito

Analizado

mediante

equipo


AR271-TS-61Revisión:

Cliente:

Productor:

Cromatograma GC:



VAZQUEZ

P-18-24827 10-11-2018.D

P-18-24827

US JP

2, 4-D Methyl ester GC/MSMS 0.2 0.2 0.1

Uso autorizado

LMR (ppm)

MX US JP CA CHN

0.1 0.1 < LCL Chlordane- a GC/MSMS 0.1 0.1 0.02 0.1 0.02

EU KOR EU KOR

0.1 0.05 0.02

3,4 Dichloroaniline GC/MSMSLINURON

METABOLITE

LINURON

METABOLITE

LINURON

METABOLITE

LINURON

METABOLITELINURON METABOLITE < LCL

2,6 Dichlorobenzonitrilo GC/MSMS - - - - - -

2,3 dihydro-2,2dimethylbenzofuran 7-

olGC/MSMS - - - - - - - - - - < LCL- - - -

- - - -

LINURON

METABOLITELINURON METABOLITE

Acetamiprid LC/MSMS 1.6 1.6 2 4 2 < LCL

Acephate LC/MSMS - - - - 0.01

- - - - < LCL

Abamectin LC/MSMS 0.2 0.2 0.01 0.2 - - < LCL

3-Hydroxy carbofuran LC/MSMS - - - - - - - - - -

0.08

Aldicarb LC/MSMS - - - - 0.01 0.1 0.02 < LCL

Alachlor LC/MSMS - - - -

0.1 - - < LCL

Acrinathrin GC/MSMS - - - - 2 0.1 - - < LCL

Acetochlor LC/MSMS - - - - 0.01

Aldrin GC/MSMS 0.05 0.05

- -- -GC/MSMSAmetryn

0.05

0.1 0.02 < LCL

Aldicarb-sulfoxide (Aldoxicarb) LC/MSMS - - - - 0.01 0.1 0.02 < LCL

Aldicarb sulfone LC/MSMS - - - - 0.01

0.01 0.01

0.01 0.05

0.01 - -

Azamethiphos LC/MSMS - - - - 0.01

0.1 - - < LCL

Atrazine-2-hydroxy LC/MSMS - - - - - - - - - - < LCL

Atrazine GC/MSMS - - - - 0.05 - -

- - - -

0.01 - -

Azoxystrobin GC/MSMS 5 5 5 5 - - < LCL

Azinphos-methyl GC/MSMS - - - - 0.01

Azinphos-ethyl LC/MSMS - - - - 0.01 0.1 - - < LCL0.02 - -

0.05 0.3

5 1

Bensulfuron-methyl LC/MSMS - - - - 0.01 0.1 - - < LCL

Bendiocarb LC/MSMS - - - - 0.01

- - - - < LCL

Benalaxyl GC/MSMS - - - - 0.05 0.1 - - < LCL

Baycarb LC/MSMS - - - - - - - - - -

0.05

BHC lindane beta GC/MSMS 0.5 0.5 0.3 0.1 - - < LCL

BHC lindane alpha GC/MSMS 0.5 0.5 0.3

0.1 - - < LCL

Benzoximate LC/MSMS - - - - 0.01 0.1 - - < LCL

Bensulide LC/MSMS - - - - 0.01

Bifenox GC/MSMS - - - - 0.01 0.1 - - < LCL

Bifenazate LC/MSMS 5 5 7

0.1 - - < LCL

BHC lindane gamma GC/MSMS 0.5 0.5 0.3 0.1 - - < LCL

BHC lindane delta GC/MSMS 0.5 0.5 0.3

7 7

0.01

Boscalid LC/MSMS 10 10 10 6 - - < LCL

Bolstar GC/MSMS - - - - - -

< LCL

Bitertanol LC/MSMS - - - - 0.05 0.1 - - < LCL

Bifenthrin GC/MSMS 1 1 1

0.01 1

- - - -

10

Bromopropylate GC/MSMS - - - - 2

Bromophos methyl GC/MSMS - - - - - - - - - - < LCL

Bromacil GC/MSMS - - - - 0.01

Buprofezin GC/MSMS - - - - 0.01 0.1 - - < LCL

Bupirimate LC/MSMS - - - - 0.01

Bromuconazole* LC/MSMS - - - - 0.01 0.1 - - < LCL

1.5 - -

0.05 1

1 1

0.1

Chlorfenvinphos LC/MSMS - - - -

LC/MSMS - - - - 0.01

- - < LCL

5 7 < LCL

0.1 - - < LCL

0.1 - - < LCL

2 1 < LCL

0.1 - - < LCL

0.1

0.05

0.01 1

0.1 - - < LCL

0.1 - - < LCL

0.1 - - < LCL

0.1 - - < LCL

- -

0.1

Chlorfenapyr GC/MSMS - - - -

0.1

0.5 < LCL

- - - - < LCL

Coumaphos GC/MSMS - - - - - - 0.1

GC/MSMS - -

- - - - 0.01

0.1 - - < LCL

Chlormequat LC/MSMS - - - - 0.05 0.1 - - < LCL

Chloridazon (Pyrazon) LC/MSMS - - - - 0.01

0.1

- - 0.01 0.1 - - < LCL

Clomazone* LC/MSMS - - - - 0.02

- - - - < LCL

Chlorthiophos GC/MSMS - - - - - - - - - - < LCL

Chlortal dimethyl GC/MSMS

< LCL- -0.1 3 1

0.01 0.05

- - - -

Cyantraniliprole* LC/MSMS - - - - 0.01 0.1 - - < LCL

0.1 - - < LCL

Cyhalothrin (Isomero Lambda

y gamma)**GC/MSMS - - - - 0.5 0.01 0.2 < LCL

Cyfluthrin GC/MSMS - - - - 0.02

0.02 - - < LCL

Cycloate LC/MSMS - - - - 0.01 0.1 - - < LCL

Cyazofamid LC/MSMS - - - - 0.01

0.1 - - < LCL

Cyprodinil GC/MSMS 10 10 10 10 - - < LCL

Cyproconazole LC/MSMS - - - - 0.5

4 - - < LCL

Cypermethrin a (Zeta-

Cypermethrin)**GC/MSMS 0.8 0.8 0.5 0.1 - - 0.013

Cymoxanil LC/MSMS 4 4 4

- - - - < LCL

DDE-o,p GC/MSMS - - - - - - - - - - < LCL

DDD-p,p GC/MSMS - - - - - -

0.1 - - < LCL

DDD-o,p GC/MSMS - - - - - - - - - - < LCL

Cyromazine LC/MSMS - - - - 0.01

- - - - < LCL

DEET (Diethyl-m-toluamide,

N,N-)GC/MSMS - - - - - - - - - - < LCL

DDT-p,p GC/MSMS - - - - - -

- - - - < LCL

DDT-o,p GC/MSMS - - - - - - - - - - < LCL

DDE-p,p GC/MSMS - - - - - -

OXYDEMETON

METHYL

METABOLITE

OXYDEMETON

METHYL

METABOLITE

OXYDEMETON

METHYL

METABOLITE

OXYDEMETON

METHYL

METABOLITE< LCL

Demeton S GC/MSMS - - - - 0.4

0.1 - - < LCL

Demeton O GC/MSMS - - - - - - - - - - < LCL

Deltamethrin GC/MSMS - - 0.1

0.1 0.02 < LCL

Demeton-s-methyl-sulfone

- - - - < LCLDialifos LC/MSMS - - - - - -

0.1 - - < LCL

Desmetryn GC/MSMS - - - - - - - - - - < LCL

Desmedipham LC/MSMS - - - - 0.01

- - - -

- - < LCL

Captan GC/MSMS 25 25 0.01 0.1 - - < LCL Diazinon GC/MSMS 0.75 0.75 0.1 0.1 0.1 < LCL

Carbaryl GC/MSMS 12 12 10 10 - - - - - -

0.01 0.120 5

0.01

0.2 < LCL

Carbetamide LC/MSMS - - - - 0.01 0.1 - - < LCL Diclobutrazol* LC/MSMS - - - - - - - - - - < LCL

Carbendazim LC/MSMSTHIOPHANATE

METHYL/ BENOMYL

METABOLITE

THIOPHANATE

METHYL/ BENOMYL

METABOLITE

THIOPHANATE

METHYL/ BENOMYL

METABOLITE

THIOPHANATE

METHYL/ BENOMYL

METABOLITE

THIOPHANATE

METHYL/ BENOMYL

METABOLITE

TRAZAS

- - < LCL

Carboxin LC/MSMS - - - - 0.01 0.1 - - < LCL Dicrotophos LC/MSMS - - - - 0.01 0.1 - - < LCL

Carbofuran GC/MSMS - - - - 0.3 0.1 0.02 < LCL Diclofop methyl

0.05

0.02 < LCL

Chinometionate GC/MSMS - - - - 0.01 0.1 - - < LCL Diethofencarb LC/MSMS - - - - 0.01 0.1 - - < LCL

Carfentrazone ethyl LC/MSMS 0.1 0.1 0.1 0.1 - - < LCL Dieldrin

0.01 2

Butocarboxim*

- - 0.01 0.1 - - < LCL

Chlorbromuron LC/MSMS - - - - - - - - - - < LCL Difenoxuron LC/MSMS - - - - - - - - - - < LCL

Chlorantraniliprole LC/MSMS 1.8 1.8 2 0.9 1 < LCL Difenoconazole

Butylate GC/MSMS - - - - 0.01 0.1 - - < LCL

Buturon LC/MSMS - - - - - -

Butocarboxim-sulfoxide LC/MSMS - - - - 0.01

- - - - < LCL

0.1 - - < LCL

0.1

- -- - - -

- -

GC/MSMS 0.05

GC/MSMS - -

GC/MSMS - -

< LCL Dichloran GC/MSMS - -

LC/MSMSOXYDEMETON

METHYL

METABOLITE

LC/MSMS

0.05 0.05 0.1

Dichlorvos

- - 0.01 0.1

- - 0.1 0.1

- - - - - -

- -

- -

0.02

< LCL- -

< LCL- -0.1

0.1 - - < LCL

Chlorsulfuron LC/MSMS - - - - 0.01

- -

0.01

LC/MSMSAminocarb

Chlorfluazuron LC/MSMS - - - - 2

0.01

0.1 0.05 < LCL

Ametoctradin LC/MSMS - - - - 0.01 0.1 Chlorpyrifos methyl GC/MSMS - - - - 0.05

Chlorpyrifos GC/MSMS - - - - 1

Chlorpropham GC/MSMS - - - - 0.01

< LCL

- -- -

0.1 - - < LCL

0.1 - - < LCL

0.1 - - < LCL

0.1 - - < LCL

Chloroxuron LC/MSMS - - - - 0.01 0.1 - - < LCL

Chlorotoluron LC/MSMS - - - - 0.01

- - < LCL

- -- -

LC/MSMS - -

Página:

Muestra:

Huerto:

Cromatograma LC:

2 de 7

Zarzamora


P-18-24827 10-14-2018.d

0.02- -- -LC/MSMSClodinafop-propargyl

- - - - < LCL

Chlorothalonil GC/MSMS - - - - 10 0.1 - - < LCL

Chloropropylate GC/MSMS - - - - - -

KOR CHN

Crimidine LC/MSMS - - - - - - - - - - < LCL

Cyanazine LC/MSMS - - - - 0.01 0.1 - - < LCL

MX

0.01- -- -LC/MSMSClofentezine

- -0.1

- - < LCL

0.1 - - < LCL

Cloquintocet-mexyl

Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El resultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A. de C.V. , por lo cual no se hace responsable de la representatividad del resultado para el total del producto.

Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto. Este formato de interpretación esta protegido y registrado ante el Instituto Mexicano de la Propiedad Intelectual. Se prohibe su reproducción total o parcial sin autorización. El presente informe de resultados no será valido si presenta raspaduras, tachaduras o enmendaduras.



*Analito no declarado en el alcance acreditado y/o autorizado que se obtiene por método acreditado y/o autorizado. Las bandas de colores son de apoyo visual basadas en los LMRs de México y no representan un resultado. 1Límite Máximo de Residuos (LMR) expresados en ppm para cada país indicado en código ISO 3166-1 alfa-3. LCL = Lowest Calibration Level (Nivel Mínimo de Calibración) ppm = Partes por millón = mg/kg GC/MSMS =Cromatografía de Gases/Masas/Masas LC/MSMS = Cromatografía de Líquidos/MasasMasas

Autoriza Lic. Carlos Sepúlveda Ibarra

Director General

B BB BB BB BB BR BB BB BB BB BB BB BB BB B

B B

B BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB B

B B

B B

B B

B B

B B

B BB B

B B

B BB B

B B

B B

B B

B B

B B

B BB B

0.05

0.5 0.5

30 30

0.02

0.01 0.3

- -

0.02 0.02

0.01 1

- -

0.01 0.01

0.01

- -

0.01 0.05

0.01

0.05

0.01 0.3MALATHION

METABOLITE

MALATHION

METABOLITE

0.02 0.5

0.05 5

0.01 0.1

- - - -

0.01 0.05

4 3

0.02 1

0.01 1

0.1 - -

- -

- -

5 0.04

0.05

0.05

0.5 1

0.05 2

0.01 3

0.05 - -

- -

0.01 - -

0.01 - -

0.01 0.3

0.01 - -

- - - -

0.03 3

0.01 0.05

- - - -

- -

0.01 0.05

0.01 0.02

0.01

0.01 0.2

0.01

0.01

5

0.05

0.05

0.013

0.01

0.01

0.01

- -

0.05

0.02

0.1

0.02

0.02

0.01

0.01

0.01

0.02

0.01 0.3

0.01 0.05

0.05 0.5

0.01

0.01

0.01

0.01

0.01 0.5

0.01 - -

0.01 - -

0.7 0.5

- - - -

0.01 0.02

0.01 2

0.02 0.1

0.02 0.2

0.01 0.5

0.05 0.5

5 2

0.01 - -

- - - -

15 15

0.01 0.05

0.01 5

0.01 5

- - - -

0.02 0.02

- - - -

0.01 0.01

1 1

0.01 0.3

0.01 0.2

0.01 0.03

0.05 0.2

0.05 0.2

0.05 0.2

0.01 0.01

0.05 0.5

0.02 - -

- - - -

0.01 1

0.01 1

0.01 - -

0.01 0.05

0.01 0.1

0.01 0.1

0.01 1

0.01 - -

0.01 - -

KOR EU KOR

0.01 - -

- - - -

- - - -

0.01 - -

0.01 0.01

0.01 1

0.05 1

1

- -

5

0.05

0.3

- -0.7

CHN MX US JP CA

Revisión: AR271-TS-61


Resultados de AnálisisSe han detectado residuos de pesticidas prohibidos

Analito

Analizado

mediante

equipo

Uso autorizado

LMR (ppm) Cantidad obtenida en

mg/kg (ppm)Analito

Analizado

mediante

equipo

Uso autorizado

LMR (ppm)

Reg. Sagarpa: SD

No. Reg. Lab.:

CHN

Fecha de reporte:

Cantidad obtenida en

mg/kg (ppm)MX US JP CA

Cliente: P-18-24827

Productor:

Cromatograma GC:

SUN BELLE MÉXICO S.A. DE

C.V.

NEFTALI ARMANDO

GONZALEZ VAZQUEZ

EU

< LCL

Dimefuron LC/MSMS - - - - - - - - - - < LCL Fluchloralin

LC/MSMS - - - - 0.01 0.1 - -Diflufenican LC/MSMS - - - - 0.01 0.1 - - < LCL Flubendiamide

< LCL

Dimethachlor LC/MSMS - - - - 0.01 0.1 - - < LCL Flufenacet

GC/MSMS 5 5 5 7 - -

< LCL

Dimepax GC/MSMS - - - - - - - - - - < LCL Fludioxonil

GC/MSMS - - - - 0.01 0.1 - -

< LCL

Dimethoate GC/MSMS - - - - 1 0.1 - - 0.251 Fluometuron

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Dimethenamid LC/MSMS - - - - 0.01 0.1 - - < LCL Flufenoxuron

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Diniconazole LC/MSMS - - - - 0.01 0.1 - - < LCL Fluoroglycofen-ethyl

LC/MSMS - - - - 0.01 0.1 - -< LCL

Dimethomorph LC/MSMS - - - - 0.01 0.1 - - < LCL Fluopicolide

LC/MSMS - - - - 0.02 0.1 - -

< LCL

Dioxathion GC/MSMS - - - - 0.01 0.1 - - < LCL Flurtamone

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Dinotefuran LC/MSMS - - - - 0.01 0.1 - - < LCL Fluoxastrobin

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Disulfoton GC/MSMS - - - - 0.05 0.1 - - < LCL Flutriafol

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Diphenamid LC/MSMS - - - - 0.01 0.1 - - < LCL Flusilazole

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Diuron (Karmex)* LC/MSMS 0.1 0.1 0.05 0.1 - - < LCL Folpet

GC/MSMS - - - - - - - - - -

< LCL

Disulfoton-sulfone LC/MSMS - - - - 0.05 0.1 - - < LCL Fluvalinate

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Dyfonate GC/MSMS - - - - 0.01 0.1 0.01 < LCL Formetanate

LC/MSMS - - - - 0.1 0.1 - -

< LCL

Dodemorph LC/MSMS - - - - 0.01 0.1 - - < LCL Forchlorfenuron

GC/MSMS - - - - 0.01 25 - -

< LCL

Emamectin Benzoate LC/MSMS - - - - 0.1 0.1 - - < LCL Furathiocarb

LC/MSMS - - - - 0.01 0.1 - -

< LCLLC/MSMS - - - - - - - - - -

Fuberidazole< LCL- -0.10.01- -- -LC/MSMSEdifenphos

< LCL

Endosulfan II (beta isomer) GC/MSMS - - - - 0.5 0.1 - - < LCL Haloxyfop-methyl

GC/MSMS 0.1 0.1 0.02 0.1 0.02

< LCL

Endosulfan I (alpha isomer) GC/MSMS - - - - 0.5 0.1 - - < LCL g Chlordan

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Endosulfan sulfate GC/MSMS - - - - 0.5 0.1 - - < LCL Heptachlor

LC/MSMS - - - - 0.05 0.1 - -

0.010.10.010.050.05GC/MSMS < LCL

0.05

0.01

< LCL

Epoxiconazole LC/MSMS - - - - 0.01 0.1 - - < LCL Heptenophos

GC/MSMS 0.05 0.05 0.01 0.1 0.01< LCL Heptachlor exo-epoxide (isomer 0.01

- -

< LCL

Etaconazole (Etaconazole I y II) LC/MSMS - - - - - - - - - - < LCL Hexaconazole

GC/MSMS 0.05 0.05 0.01 0.1 - -

< LCL

Esfenvalerate + Fenvalerate* (**) GC/MSMS 1 1 1 0.1 0.2 < LCL Hexachlorobenzene

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Ethiofencarb LC/MSMS - - - - 0.01 0.1 - - < LCL Hexythiazox

GC/MSMS - - - - 0.01 0.1 - -

< LCL

Ethalfluralin GC/MSMS - - - - 0.01 0.1 - - < LCL Hexazinone

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Ethirimol LC/MSMS - - - - - - - - - - < LCL Imazapyr

LC/MSMS - - - - 0.02 0.1 - -

< LCL

Ethiofencarb-sulfone LC/MSMS - - - - 0.01 0.1 - - < LCL Imazalil

LC/MSMS 1 1 0.01 1.5 - -

< LCL

Ethylan GC/MSMS - - - - - - - - - - < LCL Imidacloprid

LC/MSMS - - - - 0.05 0.1 - -

< LCL

Ethoprop GC/MSMS - - - - 0.01 0.1 0.02 < LCL Imazaquin

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Etofenprox GC/MSMS 5 5 0.01 0.1 - - < LCL Indoxacarb

GC/MSMS - - - - 0.1 0.1 - -

< LCL

Etion GC/MSMS - - - - 0.3 0.1 - - < LCL Imidan

LC/MSMS 2.5 2.5 4 2.5 - -

< LCL

Famoxadone LC/MSMS 10 10 10 10 - - < LCL Iprovalicarb

GC/MSMS 25 25 12 25 - -

< LCL

Etoxazole LC/MSMS 1.5 1.5 0.01 1.5 - - < LCL Iprodione

GC/MSMS - - - - 0.01 0.1 - -

< LCL

Fenarimol LC/MSMS - - - - 1 0.1 - - < LCL Isazophos

LC/MSMS - - - - - - - - - -

< LCL

Fenamiphos LC/MSMS - - - - 0.02 0.1 0.02 < LCL Irgarol

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Fenbuconazol LC/MSMS - - - - 0.01 0.1 - - < LCL Isoprocarb

LC/MSMS - - - - 0.01 0.1 0.01

< LCL

Fenazaquin LC/MSMS - - - - 0.01 0.1 - - < LCL Isofenphos

LC/MSMS - - - - 0.01 0.1 0.01

< LCL

Fenchlorphos GC/MSMS - - - - 0.01 0.1 - - < LCL Isoxaflutole

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Fenbutatin oxide* LC/MSMS - - - - 1 0.1 - - < LCL Isoproturon

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Fenhexamid LC/MSMS 20 20 15 20 15 < LCL Kresoxim-methyl

GC/MSMS - - - - 3 3 - -

< LCL

Fenfuram LC/MSMS - - - - - - - - - - < LCL Kelthane***

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Fenoxaprop-ethyl LC/MSMS - - - - 0.1 0.1 - - < LCL Linuron

LC/MSMS - - - - 0.3 0.1 - -

< LCL

Fenitrothion GC/MSMS - - - - 0.8 0.1 0.5 < LCL Lenacil

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Fenpropathrin GC/MSMS 12 12 5 12 5 < LCL Malaoxon

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Fenoxycarb LC/MSMS - - - - 0.05 0.1 - - < LCL Lufenuron

LC/MSMS - - - - 0.2 0.1 - -

< LCL

Fenpropimorph LC/MSMS - - - - 0.05 0.1 - - < LCL Mancozeb

GC/MSMS 8 8 8 8 - -

< LCL

Fenpropidin LC/MSMS - - - - 0.01 0.1 - - < LCL Malathion

LC/MSMSMALATHION

METABOLITE

MALATHION

METABOLITE

MALATHION

METABOLITE

MALATHION

METABOLITE

MALATHION

METABOLITE

Fenson GC/MSMS - - - - - - - - - - < LCL Mebendazole

LC/MSMS - - - - 0.01 0.1 - -

< LCL

Fenpyroximate LC/MSMS - - - - 0.01 0.1 - - < LCL Mandipropamid

LC/MSMS - - - - 5 0.1 5

Fenthion GC/MSMS - - - - 0.01 0.1 0.05 < LCL Mepanipyrim

LC/MSMS - - - - 0.01 0.1 - -

< LCL- - 0.01 0.1 - -0.01 0.2

Fensulfothion GC/MSMS - - - - 0.01 0.1 - - < LCL Mecarbam

0.1Methamidophos

Methabenzthiazuron

0.005 0.05

0.01 - -

- - - -

0.01 0.1 - -

- - - - - -

0.01 - -

< LCL Metconazole - - 0.01 0.1LC/MSMS

0.03 0.5

Fipronil GC/MSMS - - - - 0.01 0.1 0.02 < LCL Metamitron

GC/MSMS 0.7 0.7 0.2 0.1 - -

< LCL

- - < LCLMetalaxyl-M (Mefenoxam, R-

enantiomero de metalaxyl)Fenuron LC/MSMS - - - - - -

LC/MSMS - - - - 0.2 0.1 0.05

< LCL

Fluazifop-butyl LC/MSMS - - - - 0.01 0.1 - - < LCL Methidathion

LC/MSMS - - - - 0.01 0.1 0.05Flonicamid LC/MSMS - -

< LCL

- - 0.01 0.1 - - < LCL

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LC/MSMS - -Flamprop methyl LC/MSMS - - - - 0.01 0.1 - - < LCL Metazachlor

LC/MSMS - -

2018-10-15

LC/MSMS - -

Endrin GC/MSMS - - - - 0.01 0.1 0.05

Flazasulfuron LC/MSMS - - - - 0.1 0.1 - - < LCL

- -

< LCL

Flamprop-isopropyl LC/MSMS - - - - - - - - - - - -

0.05

CHNKOR

< LCLLC/MSMS - - - - 0.01 0.1 - -

< LCL

- - 0.01 0.1 - -- -

0.4

- -

US JP CA EUMX

< LCL

< LCL

< LCLLC/MSMS - - - - - - - - - -

< LCL

Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El re sultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A. de C.V. , por lo cual no se hace responsable de la representatividad del

resultado para el total del producto. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.

Este formato de interpretación esta protegido y registrado ante el Instituto Mexicano de la Propiedad Intelectual. Se prohibe su reproducción total o parcial sin autorización. El presente informe de resultados no será valido si presenta raspaduras, tacha duras o enmendaduras.



*Analito no declarado en el alcance acreditado y/o autorizado que se obtiene por método acreditado y/o autorizado. Las bandas de colores son de apoyo visual basadas en los LMRs de México y no representan un resultado. 1Límite Máximo de Residuos (LMR) expresados en ppm para cada país indicado en código ISO 3166 -1 alfa-3. LCL = Lowest Calibration Level (Nivel Mínimo de Calibración) ppm = Partes por millón = mg/kg GC/MSMS =Cromatografía de Gases/Masas/Masas LC/MSMS = Cromatografía de Líquidos/MasasMasas Trazas/Traces = < 0.010 ppm.


Director General

B BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB B

B B

B B

B BB B

B B

B B

B B

B B

R B

B B

B B

B BB BB BB BB BB BB BB BB B

B B

B

B

B

B

B

BBBBBBBBBBBB

0.02 - -

0.01 - -

0.01 - -

- - - -

0.1 1

0.01 0.25

0.01 0.05

0.05 0.1

0.5

0.05 0.05

0.01 - -

0.01 - -

0.01 - -

3 0.5

3 3

0.01 1

0.5 1

0.01 0.05

0.01 - -

0.01 2

- - - -

- - 0.05

0.01 0.05

4 1

0.01 0.02

0.01 1

0.01 - -

0.05 1

0.01 2

0.01 2

- - - -

- - - -

- - - -

0.05 5

0.01 - -

0.01 0.5

- - - -

0.01 0.05

0.01 0.05

0.01 0.05

0.01 5

0.01 0.2

0.3

0.01 0.2

0.1 0.2

0.05 2

0.05 0.05

QUINTOCENE

(PENTACHLORONIT

ROBENZENE)META

BOLITE

QUINTOCENE

(PENTACHLORO

NITROBENZENE

)METABOLITE

- - - -

0.02 0.01

0.01 - -

- - - -

0.01 14

0.01 0.5

0.01 0.2

0.05 0.1

0.01 0.05

0.01 - -

- - - -

0.01 5

< LCL

Pentachloroanisol GC/MSMS - - - - - - - - - - < LCL

Pencycuron LC/MSMS - - - - 0.01 0.1 - - < LCL

< LCL

Pendimethalin

- - - - 0.01 0.1 - - < LCL

Simazine GC/MSMS 0.2 0.2 0.2 0.1 - - < LCL

LC/MSMS

LC/MSMS 0.1 0.1 0.05 0.1 - -

S-Metolachlor

LC/MSMS

< LCL

Simetryn

0.1 0.1 0.01 0.1 - -

Sethoxydim* LC/MSMS 5 5 1 5 - - < LCL

Profenofos GC/MSMS - - - - 0.01 0.1 - - < LCL

Profluoralin GC/MSMS - - - - - - - - - - < LCL

Promecarb GC/MSMS - - - - - - - -

Prometon GC/MSMS

Fecha de reporte: 2018-10-15 Revisión: AR271-TS-61


Reg. Sagarpa: SD

No. Reg. Lab.:Cliente:

Productor:

Cromatograma GC:



VAZQUEZ

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US JP CA EUMX CHN

Se han detectado residuos de pesticidas prohibidos

Analito

Analizado

mediante

equipo

Uso autorizado

LMR (ppm) Cantidad obtenida en

mg/kg (ppm)Analito

Analizado

mediante

equipo

Uso autorizado

LMR (ppm)

CHN

Cantidad obtenida

en mg/kg (ppm)MX US JP CA CHN MX US JP CAEU KOR EU KOR

Methiocarb GC/MSMS - - - - 0.05 0.1 - - < LCL Picoxystrobin

Methiocarb sulfoxide GC/MSMS - - - - 0.05 0.1 - - < LCL Piperonyl Butoxide

Methiocarb sulfone GC/MSMS - - - -

0.2 0.05

0.2 0.05

0.2 0.05

< LCL

0.1

LC/MSMS - - - - - - - -0.05 0.1 - - < LCL Piperalin

LC/MSMS - - - - 0.01

8 8LC/MSMS 8 8

0.01 1

- -

LC/MSMS - - - - 0.01 0.1

LC/MSMS - - - - 0.01 0.1

LC/MSMS

LC/MSMS - - - -

Methoxychlor GC/MSMS - - - - 7 0.1 - - < LCL

Metobromuron LC/MSMS

< LCL

Pirimiphos-ethyl

Primisulfuron-methyl

Piperophos

Methoprotryne LC/MSMS

0.2

- - - - - - - - - - < LCL Pirimicarb

Methomyl LC/MSMS - - - - 1 0.1

< LCLPirimiphos-methyl

- - - - 0.01 0.1

Methoxyfenozide LC/MSMS 6 6 0.01 6 - -

- - - - 0.01 0.1 - -

LC/MSMS

Metolcarb LC/MSMS - - - - 0.01 0.1 - - < LCL

< LCL< LCL

Metolachlor LC/MSMS - - - - 0.01 0.1 - - < LCL Prochloraz LC/MSMS - - - - 0.05 0.1 - - < LCL

Procymidone GC/MSMS - - - - 1.5 0.1

Metrafenone LC/MSMS - - - - 0.01 0.1 - - < LCL

Metoxuron LC/MSMS - - - - - - - - - - < LCL

Metosulam LC/MSMS - - - - 0.01 0.1 - - < LCL

Mevinphos GC/MSMS - - - - 0.01 0.1 - - < LCL

Metsulfuron-methyl* LC/MSMS - - - - 0.01 0.1 - - < LCL

Metribuzin GC/MSMS - - - - 0.01 0.1 - - < LCL0.1 0.05

0.01 - -

0.01 0.5

Monocrotophos LC/MSMS - - - - 0.01 0.1 0.03 < LCL

Mirex GC/MSMS - - - - 0.01 0.1 0.01 < LCL

Mexacarbate LC/MSMS - - - - - - - - - - < LCL- - - -

0.01 - -

0.01 0.2

Myclobutanil GC/MSMS 2 2 1 2 - - < LCL

Monuron LC/MSMS - - - - 0.01 0.1 - - < LCL

Monolinuron LC/MSMS - - - - 0.01 0.1 - - < LCL0.01 - -

0.01 - -

1 1

Neburon LC/MSMS - - - - - - - - - - < LCL

Napropamide LC/MSMS 0.1 0.1 0.1 0.1 - - < LCL

N-2,4-Dimethylphenyl formamide

(2,4-DMPF)LC/MSMS - - - - - - - - - - < LCL- - - -

0.1 0.05

- - - -

Norflurazon LC/MSMS 0.1 0.1 0.1 0.1 - - < LCL

Nitrapyrin GC/MSMS - - - - 0.01 0.1 - - < LCL

Nicosulfuron LC/MSMS - - - - 0.01 0.1 - - < LCL0.01 0.3

0.01 0.2

0.01 0.1

Omethoate LC/MSMSDIMETHOATE

METABOLITE

DIMETHOATE

METABOLITE

DIMETHOATE

METABOLITE

DIMETHOATE

METABOLITE

DIMETHOATE

METABOLITE0.226

Ofurace LC/MSMS - - - - - - - - - - < LCL

Novaluron* LC/MSMS - - - - 0.01 0.1 - - < LCL0.01 1

- - - -

DIMETHOATE

METABOLITE

DIMETHOATE

METABOLITE

Oxadixyl LC/MSMS - - - - 1 0.1 - - < LCL

Ovex GC/MSMS - - - - - - - - - - < LCL

op Dicofol*** GC/MSMS - - - - 3 3 - - < LCL0.02 1

- - - -

0.01 1

Oxyfluorfen GC/MSMS 0.05 0.05 0.01 0.1 - - < LCL

Oxydemeton-methyl LC/MSMS - - - - 0.02 0.1 - - < LCL

Oxamyl LC/MSMS - - - - 0.01 0.1 - - < LCL0.01 0.5

0.01 - -

0.05 0.05

Paraoxon-methyl LC/MSMS - - - - - - - - - - < LCL

Paraoxon LC/MSMS - - - - - - - - - - < LCL

Paclobutrazol (Bonzi) LC/MSMS - - - - 0.01 0.1 - - < LCL0.5 0.05

- - - -

- - - -

GC/MSMS - - - - 0.02 0.1 - - < LCL

Parathion GC/MSMS - - - - 0.5 0.1 0.01 < LCL

Penconazol LC/MSMS - - - - 0.2 0.1 - - < LCL

Parathion methyl GC/MSMS - - - - 0.2 0.1 0.02 < LCL

0.05

< LCL

Permethrin GC/MSMS - - - - 1 0.1 1 < LCL

Pentachloroaniline GC/MSMS

QUINTOCENE

(PENTACHLORO

NITROBENZENE

)METABOLITE

QUINTOCENE

(PENTACHLORON

ITROBENZENE)M

ETABOLITE

QUINTOCENE

(PENTACHLORO

NITROBENZENE)

METABOLITE

QUINTOCENE

(PENTACHLORO

NITROBENZENE)

METABOLITE

QUINTOCENE

(PENTACHLORON

ITROBENZENE)M

ETABOLITE

Phenmedipham LC/MSMS - - - - 0.01 0.1 - -

Pentachlorophenol GC/MSMS - - - - 0.01 0.1 - - < LCL

Pentachloronitrobenzene

Phorate GC/MSMS - - - - 0.05 0.024 0.01 < LCL

Phenyl valerate GC/MSMS - - - - - - - - - - < LCL

Phenthoate LC/MSMS - - - - 0.01 0.1 - - < LCL

- - - - 0.01 0.1 - - < LCL

Phorate-sulfoxide LC/MSMS - - - - 0.05 0.024 0.01 < LCL

Phorate-sulfone LC/MSMS - - - - 0.05 0.024 0.01 < LCL

Picolinafen LC/MSMS - - - - 0.01 0.1 - - < LCL

- - - - - - - - - - < LCL

Phoxim LC/MSMS - - - - 0.02 0.1 0.05 < LCL

Phosphamidon LC/MSMS - - - - 0.01 0.1 0.05 < LCL

Propachlor LC/MSMS - - - - 0.01 0.1

Phosalone LC/MSMS

Propamocarb LC/MSMS - - - - 0.05 0.1 - - < LCL

Prometryn GC/MSMS - - - - 0.01 0.1 - - < LCL

Pronamide LC/MSMS - - - - - - - - - - < LCL

0.01 0.05

- - - -

0.02 - -

0.01 0.1

- -

< LCL

- -

- -

- -

< LCL

< LCL

Propetamphos LC/MSMS - - - - 0.01 0.1 - - < LCL

Propanil LC/MSMS - - - - 0.1 0.1 - - < LCL

Propargite (Omite) LC/MSMS - - - - 0.01 0.1 - - < LCL

- -

0.01 0.1 - - < LCL

- - < LCL

0.1 0.1 - -

- - 0.5 0.1

< LCL

< LCL

- -

1

< LCL- -

< LCL

- - < LCL

- - < LCL

0.01 0.05

0.01 7

0.01 - -

0.01 - -

0.01

0.01 0.1 - -

- -

Resultados de análisis

Propazin GC/MSMS - - - - 0.01 0.1 - - < LCL

< LCL

Propiconazole GC/MSMS 1 1 0.05 1 - - < LCL

Propoxur LC/MSMS - - - - 1 0.1

Propyzamide LC/MSMS 0.05 0.05

- - 0.01 0.1 - -

Pyrimethanil

Pyriproxyfen

Quinalphos

Quinoxyfen

Prosulfocarb LC/MSMS - - - - 0.01 0.1 - -

- - - - 0.01 0.1 - -

- - - - 0.01 0.1 - -

4 4 3 3.5 - -

- - - -

Quizalofop-ethyl

Rimsulfuron

Rotenone

Sebuthylazine

LC/MSMS

LC/MSMS

LC/MSMS

LC/MSMS

LC/MSMS

LC/MSMS

GC/MSMS

LC/MSMS

LC/MSMS

LC/MSMS

LC/MSMS

LC/MSMS

GC/MSMS

Prosulfuron

Pymetrozine

Pyraclostrobin

Pyrazophos

Pyridaben

- - - - 0.05 0.1 - -

15 15 10 15 - -

1 1 0.01 0.1 - -

- - 0.01 0.1 - -

0.1 - -

15 15

0.05 1

0.01 0.01

0.05 0.05

- - - - - - - - - -

< LCL

< LCL

< LCL

< LCL

< LCL

< LCL

< LCL

< LCL

< LCL

< LCL

< LCL

< LCL

< LCL

0.01 0.01 0.01 0.01 - -

- -

- - - - 0.02

- - - - 0.01 0.1 - -

KOR

Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El re sultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A. de C.V. , por lo cual no se hace responsable de la representatividad del

resultado para el total del producto. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.




*Analito no declarado en el alcance acreditado y/o autorizado que se obtiene por método acreditado y/o autorizado. Las bandas de colores son de apoyo visual basadas en los LMRs de México y no representan un resultado. 1Límite Máximo de Residuos (LMR) expresados en ppm para cada país indicado en código ISO 3166 -1 alfa-3. LCL = Lowest Calibration Level (Nivel Mínimo de Calibración) ppm = Partes por millón = mg/kg GC/MSMS =Cromatografía de Gases/Masas/Masas LC/MSMS = Cromatografía de Líquidos/MasasMasas Trazas/Traces = < 0.010 ppm.


Director General

BB BBBBBBBBBBBBBBBBBBBBBBBB

B

BBBBBBBBBBBBBBBBBBBBBBBBBBB

BB- - < LCLVinclozolin GC/MSMS - - - - 5 0.1 0.01 5

Vamidothion LC/MSMS - - - - 0.01 0.1 0.01 0.05 - -

< LCL

Trimidal LC/MSMS - - - - - - - - - - - - - - < LCL

< LCL

Terbumeton LC/MSMS

Terbacil GC/MSMS

Teflubenzuron LC/MSMS

Thiacloprid LC/MSMS

Tetramethrin LC/MSMS

Thiabendazole LC/MSMS

0.35 0.35

- -

Thidiazuron

Tetrahydrophthalimide, cis-1,2,3,6-(THPI) GC/MSMS

GC/MSMS

LC/MSMS

GC/MSMS

< LCL

Terbuthylazine

GC/MSMS

GC/MSMS

GC/MSMS

Terrazole

Tetradifon

Tetrachlorvinphos, E-isomer

Terbutryn

Terbuthylazine-desethyl

LC/MSMS

Thiamethoxam LC/MSMS

< LCL

- -

- - - - 0.01 - -0.1

0.1

0.01

0.01

- -

- - < LCL0.20.01

1

0.01

1 < LCL

3 - -

< LCL

- - - - - - < LCL

- - - - - - - -- -

< LCL- -

0.1

- - - - 0.01 0.05 - - < LCL

- - - -

0.01

Tebuthiuron LC/MSMS

1 1 1

- -

- -

< LCL

- - < LCL

- - - - 0.01 0.1

- -

0.05 - - < LCL

- -

- -

- - - -

- -

Spirodiclofen

Productor: NEFTALI ARMANDO GONZALEZ VAZQUEZ Huerto: LA TIJERA, LOS REYES MICH Reg. Sagarpa: SD

Cliente:


US JP KOR CHNCA

Cantidad obtenida

en mg/kg (ppm)

Cromatograma LC:

EU

Fecha de reporte: 2018-10-15 Página: 5 de 7 Revisión:

SUN BELLE MÉXICO S.A. DE C.V. Muestra: Zarzamora No. Reg. Lab.: P-18-24827

AR271-TS-61

LC/MSMS

- - - - 0.01 0.2

- - - - 0.01 1

0.8 0.8 0.7 0.05

Spinosad A LC/MSMS

MX

1

0.5

0.5

Sumithrin GC/MSMS

- - < LCL

Sulfentrazone LC/MSMS

Spiroxamine LC/MSMS - - < LCL

0.15 0.15 0.05 - - - - < LCL

- - - - 0.01

Spirotetramat LC/MSMS

Spiromesifen LC/MSMS

0.1

Sulfotep LC/MSMS

Sulfosulfuron LC/MSMS

< LCL

- - < LCL

- - - - 0.01 - - 0.01 < LCL

- - - - 0.01 - -

Sulfoxaflor LC/MSMS

0.1

0.1

Tebufenozide LC/MSMS

Tebuconazole GC/MSMS

- -

- - - - 0.01 0.1 - -

0.5

0.053 3 3 1 - -

- - - - 0.01 0.5

- - - - 0.01

- - - - 0.01 - - - - < LCL

- - - - 2 0.5

0.1

0.05

0.01

< LCL

- - - - 0.01 1 - - < LCL

- - - -

CAPTAN METABOLITE

0.01

0.01

- -

0.1

0.1

- -

- -

0.2 0.2 0.1

- - - -

- -

0.01

- -

< LCL

- - 1 10.01

CAPTAN

METABOLITE

CAPTAN

METABOLITE

< LCL

< LCL

- -

0.01 0.05 - - < LCL0.1LC/MSMSThifensulfuron-methyl 0.01- -

- - - -

Triforine LC/MSMS - - - - 0.01 0.1 0.01 0.5

Triflusulfuron-methyl LC/MSMS - - - - 0.01 0.1 0.01

- -

- - - - 0.01 0.1

- - 3

- - 0.01

CAPTAN METABOLITE CAPTAN METABOLITE

0.5 1 - - < LCL

- - - - 5 0.70.1

0.5

- -

Tebutam LC/MSMS

Tebufenpyrad GC/MSMS

0.1

CAPTAN METABOLITECAPTAN

METABOLITE

< LCL

- -

- -

0.1

0.1

0.1

< LCL

0.1

0.1

0.1

0.1

< LCL- - - - 0.01 - - - -

< LCL1

1.5 1 < LCL

Se han detectado residuos de pesticidas prohibidos

US JP CA EU KOR

- -

P-18-24827 10-14-2018.d MX

Resultados de análisis

CHNCromatograma GC: P-18-24827 10-11-2018.D

Spinetoram J LC/MSMS

Analito

Analizado

mediante

equipo

Uso autorizado

LMR (ppm)

< LCL

< LCL

< LCL

- -

0.02

0.02

0.1

0.01

0.01

0.01

0.01

0.01

0.1 0.01

0.15

0.1

- -

0.5

0.01 1

0.02

- -

0.1

2

0.01 0.05 - - < LCL

Thiocyclam hydrogen oxalate GC/MSMS - - - - 3 0.1 0.01 1 - - < LCL

Thiobencarb LC/MSMS - - - - 0.01 0.1

< LCL

Thionazin LC/MSMS - - - - - - - - - - - - - - < LCL

Thiodicarb LC/MSMS - - - - 1 0.1 0.01 1 - -

< LCL

Tokution GC/MSMS - - - - - - - - - - - - - - < LCL

Thiophanate-methyl LC/MSMS - - - - 3 6 0.1 2 - -

< LCL

Triadimefon GC/MSMS - - - - 0.1 0.1 0.01 0.05 - - < LCL

Tolyfluanid GC/MSMS - - - - 5 0.1 0.02 2 5

< LCL

Triasulfuron LC/MSMS - - - - 0.01 0.1 0.05 - - - - < LCL

Triadimenol GC/MSMS - - - - 0.5 0.1 0.01 0.5 - -

< LCL

Tribenuron-methyl LC/MSMS - - - - 0.01 0.1 0.01 - - - - < LCL

Triazophos GC/MSMS - - - - 0.01 0.1 0.01 0.05 - -

0.05 0.2 < LCL

Trichloronate GC/MSMS - - - - - - - - - - - - - - < LCL

Trichlorfon LC/MSMS - - 0.5 0.1 0.01

< LCL

Tricyclazole GC/MSMS - - - - 0.02 0.1 0.01 0.05 - - < LCL

Triclocarban LC/MSMS - - - - - - - - - - - - - -

< LCL

Trifloxystrobin LC/MSMS - - - - 0.01 0.1 3 0.7 - - < LCL

Trietazine LC/MSMS - - - - - - - - - - - - - -

< LCL

Triflumuron LC/MSMS - - - - 0.02 0.1 0.05 0.5 - - < LCL

Triflumizole LC/MSMS - - - - 0.01 0.1 0.1 2 - -

< LCLTrifluralin GC/MSMS - - - - 0.05 0.1 0.01 0.05 - -

Atención: Análisis Técnicos S.A. de C.V no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El resultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A. de C.V, por lo cual no se hace responsable de la representatividad del resultado para el total del producto.

Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto. Este formato de interpretación esta protegido y registrado ante el Instituto Mexicano de la Propiedad Intelectual. Se prohibe su reproducción total o parcial sin autorización. El presente informe de resultados no será valido si presenta raspaduras, tachaduras o enmendaduras.




Director General

*Analito no declarado en el alcance acreditado y/o autorizado que se obtiene por método acreditado y/o autorizado. Las bandas de colores son de apoyo visual basadas en los LMRs de México y no representan un resultado. 1Límite Máximo de Residuos (LMR) expresados en ppm para cada país indicado en código ISO 3166-1 alfa-3. LCL = Lowest Calibration Level (Nivel Mínimo de Calibración) ppm = Partes por millón = mg/kg GC/MSMS =Cromatografía de Gases/Masas/Masas LC/MSMS = Cromatografía de Líquidos/MasasMasas Trazas/Traces = < 0.010 ppm.

Vamidothion 0.005

Malaoxon 0.005 Pentachloroaniline 0.010 Spinosad A 0.005

Lenacil 0.005 Penconazol 0.005 Simetryn 0.005

Kresoxim-methyl 0.005 Parathion methyl 0.010 Simazine 0.010

Vinclozolin 0.010

Triflusulfuron-methyl 0.005

Kelthane*** 0.010 Parathion 0.010 Sethoxydim* 0.010 Trimidal 0.005

Lufenuron 0.005 Pendimethalin 0.005 Spinetoram J 0.005

Isofenphos 0.005 Oxyfluorfen 0.010 Quizalofop-ethyl 0.005

Mancozeb 0.005 Pentachloronitrobenzene 0.010 Spiromesifen 0.005

Malathion 0.010 Pentachloroanisol 0.010 Spirodiclofen 0.005

Mebendazole 0.005 Permethrin 0.010 Spiroxamine 0.005

Mandipropamid 0.005 Pentachlorophenol 0.010 Spirotetramat 0.005

Mepanipyrim 0.010 Phenthoate 0.005 Sulfosulfuron 0.005Mecarbam 0.005 Phenmedipham 0.005 Sulfentrazone 0.005

Metamitron 0.005 Phorate 0.010 Sulfoxaflor 0.005

Metalaxyl-M (Mefenoxam, R-

enantiomero de metalaxyl)0.010 Phenyl valerate 0.010 Sulfotep 0.005

0.005

Metconazole 0.005 Phorate-sulfoxide 0.005 Tebuconazole 0.010

Metazachlor 0.005 Phorate-sulfone 0.005 Sumithrin 0.020

Lowest Calibration Level (Nivel Mínimo de Calibración) por analitoAnalito LCL (ppm) Analito LCL (ppm) Analito LCL (ppm)

Methidathion 0.005 Phoxim 0.010 Tebutam 0.005

Methamidophos 0.005 Phosphamidon 0.005 Tebufenpyrad 0.010

Methabenzthiazuron 0.005 Phosalone 0.010 Tebufenozide

Fecha de reporte: 2018-10-15 Página: 6 de 7 Revisión:


AR271-TS-61

Analito LCL (ppm)

Endosulfan I (alpha isomer) 0.010

2,3 dihydro-2,2dimethylbenzofuran 0.020 Butocarboxim-sulfoxide 0.005 Cyproconazole 0.005 Endosulfan II (beta isomer) 0.010

2, 4-D Methyl ester 0.010 Butocarboxim* 0.010Cypermethrin a (Zeta-

Cypermethrin)**0.010

Endosulfan sulfate 0.010

3,4 Dichloroaniline 0.010 Butylate 0.020 Cyromazine 0.005 Endrin 0.0102,6 Dichlorobenzonitrilo 0.010 Buturon 0.005 Cyprodinil 0.010

Epoxiconazole 0.005

Abamectin 0.005 Carbaryl 0.010 DDD-p,p 0.010 Esfenvalerate + Fenvalerate* (**) 0.0103-Hydroxy carbofuran 0.005 Captan 0.010 DDD-o,p 0.010

Etaconazole (Etaconazole I y II) 0.010

Acetamiprid 0.005 Carbetamide 0.005 DDE-p,p 0.010 Ethalfluralin 0.010Acephate 0.005 Carbendazim 0.005 DDE-o,p 0.010

Ethiofencarb 0.005

Acrinathrin 0.020 Carboxin 0.005 DDT-p,p 0.010 Ethiofencarb-sulfone 0.005Acetochlor 0.005 Carbofuran 0.010 DDT-o,p 0.010

Ethirimol 0.005

Aldicarb 0.005 Chinometionate 0.010 Deltamethrin 0.010 Ethoprop 0.010Alachlor 0.005 Carfentrazone ethyl 0.005 DEET (Diethyl-m-toluamide, N,N-) 0.010

Ethylan 0.010

Aldicarb-sulfoxide (Aldoxicarb) 0.005 Chlorbromuron 0.005 Demeton S 0.010 Etion 0.010Aldicarb sulfone 0.005 Chlorantraniliprole 0.005 Demeton O 0.010

Etofenprox 0.010

Ametoctradin 0.005 Chlordimeform 0.010 Desmedipham 0.005 Etoxazole 0.005Aldrin 0.010 Chlordane- a 0.010 Demeton-s-methyl-sulfone 0.005

Famoxadone 0.010

Aminocarb 0.005 Chlorfenvinphos 0.005 Dialifos 0.005 Fenamiphos 0.005Ametryn 0.010 Chlorfenapyr 0.010 Desmetryn 0.010

Fenarimol 0.005

Atrazine-2-hydroxy 0.005 Chloridazon (Pyrazon) 0.005 Dichloran 0.010 Fenazaquin 0.005Atrazine 0.010 Chlorfluazuron 0.005 Diazinon 0.010

Fenbuconazol 0.005

Azinphos-ethyl 0.005 Chlorobenzilate 0.010 Diclobutrazol* 0.010 Fenbutatin oxide* 0.010Azamethiphos 0.005 Chlormequat 0.005 Dichlorvos 0.010

Fenchlorphos 0.010

Azoxystrobin 0.010 Chloropropylate 0.010 Dicrotophos 0.005 Fenfuram 0.005Azinphos-methyl 0.010 Chloroneb 0.010 Diclofop methyl 0.020

Fenhexamid 0.005

Benalaxyl 0.010 Chlorotoluron 0.005 Diethofencarb 0.005 Fenitrothion 0.020Baycarb 0.005 Chlorothalonil 0.010 Dieldrin 0.010

Fenoxaprop-ethyl 0.005

Bensulfuron-methyl 0.005 Chlorpropham 0.010 Difenoxuron 0.005 Fenoxycarb 0.005Bendiocarb 0.005 Chloroxuron 0.005 Difenoconazole 0.005

Fenpropathrin 0.010

Benzoximate 0.005 Chlorpyrifos methyl 0.010 Dimefuron 0.005 Fenpropidin 0.005Bensulide 0.005 Chlorpyrifos 0.010 Diflufenican 0.005

Fenpropimorph 0.005

BHC lindane beta 0.010 Chlortal dimethyl 0.010 Dimethachlor 0.005 Fenpyroximate 0.005BHC lindane alpha 0.010 Chlorsulfuron 0.005 Dimepax 0.010

Fenson 0.020

BHC lindane gamma 0.010 Clodinafop-propargyl 0.005 Dimethoate 0.010 Fensulfothion 0.010BHC lindane delta 0.010 Chlorthiophos 0.020 Dimethenamid 0.005

Fenthion 0.010

Bifenox 0.020 Clomazone* 0.005 Diniconazole 0.005 Fenuron 0.005Bifenazate 0.005 Clofentezine 0.005 Dimethomorph 0.005

Fipronil 0.020

Bitertanol 0.005 Dioxathion 0.010 Flamprop methyl 0.010Bifenthrin 0.010 Cloquintocet-mexyl 0.005 Dinotefuran 0.005

Flamprop-isopropyl 0.010Coumaphos 0.010

Boscalid 0.005 Disulfoton 0.010 Flazasulfuron 0.005Bolstar 0.010 Diphenamid 0.005Crimidine 0.005

Cyanazine 0.005

Flonicamid 0.010

Bromophos methyl 0.010 Cyazofamid 0.005 Diuron (Karmex)* 0.010 Fluazifop-butyl 0.005Bromacil 0.010 Cyantraniliprole* 0.010 Disulfoton-sulfone 0.005

Flubendiamide 0.010

Bromuconazole* 0.010 Cyfluthrin 0.010 Dyfonate 0.010 Fluchloralin 0.020Bromopropylate 0.010 Cycloate 0.005 Dodemorph 0.005

Fludioxonil 0.010

Buprofezin 0.010 Cymoxanil 0.005 Emamectin Benzoate 0.005 Flufenacet 0.005

Bupirimate 0.005Cyhalothrin (Isomero Lambda y

gamma)**0.010 Edifenphos 0.005

Analito LCL (ppm)

Flufenoxuron 0.005 Methomyl 0.005 Piperonyl Butoxide 0.005 Terbumeton 0.005

Analito LCL (ppm) Analito LCL (ppm) Analito LCL (ppm)

Terbuthylazine 0.010

Fluopicolide 0.005 Methoxychlor 0.010 Pirimicarb 0.005 Terbuthylazine-desethyl 0.005

Fluometuron 0.005 Methoprotryne 0.005 Piperophos 0.005

Terbutryn 0.010

Fluoxastrobin 0.005 Metobromuron 0.010 Pirimiphos-methyl 0.005 Terrazole 0.010

Fluoroglycofen-ethyl 0.005 Methoxyfenozide 0.005 Pirimiphos-ethyl 0.005

Tetrachlorvinphos, E-isomer 0.010

Flusilazole 0.005 Metolcarb 0.010 Prochloraz 0.005 Tetradifon 0.010

Flurtamone 0.005 Metolachlor 0.005 Primisulfuron-methyl 0.005

Tetrahydrophthalimide, cis-1,2,3,6-

(THPI)0.010

Fluvalinate 0.010 Metoxuron 0.005 Profenofos 0.010 Tetramethrin 0.005

Flutriafol 0.005 Metosulam 0.005 Procymidone 0.010

Thiabendazole 0.005

Forchlorfenuron 0.005 Metribuzin 0.010 Promecarb 0.010 Thiacloprid 0.005

Folpet 0.010 Metrafenone 0.005 Profluoralin 0.020

Thiamethoxam 0.005

Fuberidazole 0.005 Mevinphos 0.010 Prometryn 0.010 Thidiazuron 0.005

Formetanate 0.005 Metsulfuron-methyl* 0.005 Prometon 0.010

0.010

Furathiocarb 0.005 Mexacarbate 0.005 Pronamide 0.005

Thiocyclam hydrogen oxalate 0.010

Thifensulfuron-methyl 0.005

g Chlordan 0.010 Mirex 0.010

Haloxyfop-methyl 0.005 Monocrotophos 0.005 Propamocarb 0.005

Propachlor 0.005 Thiobencarb

Propetamphos 0.005

Heptenophos 0.005 Myclobutanil 0.010

Heptachlor 0.010 Monolinuron 0.005 Propanil 0.005

Heptachlor exo-epoxide (isomer B) 0.010 Monuron 0.005 Propargite (Omite)

Propazin

0.005

0.010

Hexachlorobenzene 0.010N-2,4-Dimethylphenyl formamide

(2,4-DMPF)0.010

Hexazinone 0.010 Neburon 0.005 Propoxur 0.005

Hexaconazole 0.005 Napropamide 0.005 Propiconazole 0.010

Imazalil 0.005 Nitrapyrin 0.010 Prosulfocarb 0.005

Hexythiazox 0.005 Nicosulfuron 0.005 Propyzamide 0.005

Imazaquin 0.005 Novaluron* 0.010 Pymetrozine 0.005

Imazapyr 0.005 Norflurazon 0.005 Prosulfuron 0.005

Imidan 0.010 Omethoate 0.005 Pyrazophos 0.005

Imidacloprid 0.005 Ofurace 0.005 Pyraclostrobin 0.005

Iprodione 0.010 Ovex 0.010 Pyrimethanil 0.005

Indoxacarb 0.010 op Dicofol*** 0.010 Pyridaben 0.005

Irgarol 0.005 Oxamyl 0.005 Quinalphos 0.005

Iprovalicarb 0.005 Oxadixyl 0.005 Pyriproxyfen 0.010

Isazophos 0.010 Oxydemeton-methyl 0.005 Quinoxyfen 0.005

Sebuthylazine 0.010

Isoproturon 0.005 Paraoxon 0.005 Rotenone 0.005

Isoprocarb 0.005 Paclobutrazol (Bonzi) 0.005 Rimsulfuron 0.005

Isoxaflutole 0.010 Paraoxon-methyl 0.005

Methiocarb sulfoxide 0.020 Piperalin 0.005 Terbacil 0.010

Linuron 0.005 Pencycuron 0.005 S-Metolachlor 0.005

Methiocarb sulfone 0.020 Picoxystrobin 0.005 Teflubenzuron 0.010

Methiocarb 0.010 Picolinafen 0.005 Tebuthiuron 0.005

Thiodicarb

Thionazin

Thiophanate-methyl

Tokution

Tolyfluanid

Triadimefon

Triadimenol

Triasulfuron

Triazophos

0.005

0.005

0.005

0.010

0.010

0.010

0.010

0.005

0.010

Tribenuron-methyl

Trichlorfon

Trichloronate

Triclocarban

0.005

0.005

0.010

0.010

Triflumizole 0.005

Trifloxystrobin 0.005

Trietazine 0.005

Tricyclazole 0.010

Triforine 0.010

Triflumuron 0.010

Trifluralin 0.010

Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El resultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A.

de C.V. , por lo cual no se hace responsable de la representatividad del resultado para el total del producto. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.




ppm = Partes por millón = mg/kg Incertidumbre = 50 % según "Method validation and quality control procedures for pesticide residues analysis in food and feed ". No. de Documento SANCO/10684/2009. Punto 91

International Maximum Residue Level Database

http://www.mrldatabase.com/

EU Pesticides Database

http://ec.europa.eu/sanco_pesticides/public/index.cfm

Electronic Code of Federal Regulation

http://ecfr.gpoaccess.gov/cgi/t/text/text-idx?

Health Canada

http://pr-rp.hc-sc.gc.ca/mrl-lrm/index-eng.php

Normas Alimentarias FAO/OMS

http://www.codexalimentarius.net/pestres/data/pesticides/search.html

Positive List System for Agricultural Chemical Residues in Foods (Japón)

http://m5.ws001.squarestart.ne.jp/foundation/search.html

Información correspondiente a la página 2, página 3, página 4 y página 5

Información correspondiente a la página 5 y 6


Referencias

Glosario

Trazas = < 0.010 ppm.

MX= México

US= Estados Unidos

JP= Japón

CA= Canadá

EU= Union Europea

KOR=Corea

CHN= China

GC/MSMS = Gases/Masas/Masas AGILENT 225/MS, 240/MS

LC/MSMS = Líquidos/Masas/Masas QQQ (AGILENT 6460)

LCL = Lowest Calibration Level (Nivel Mínimo de Calibración)

LMR = Límite Máximo de Residuos

ppm = Partes por millón = mg/Kg

SD = Sin dato

1. El laboratorio Análisis Técnicos S.A. de C.V. se encuentra acreditado ante la EMA, en el Ensayo de determinación de residuos de pesticidas en frutas, legumbres, alimentos agrícolas y

semillas (incorporando extracción QuEChERS), por cromatografia de GASES/MASAS/MASAS ante el sistema ISO/IEC 17015:2005. 7890

2. El laboratorio Análisis Técnicos S.A. de C.V. se encuentra acreditado ante la EMA, en el Ensayo de determinación de residuos de pesticidas en frutas, legumbres, alimentos agrícolas y

semillas (incorporando extracción QuEChERS), por cromatografia de LÍQUIDOS/MASAS/MASAS ante el sistema ISO/IEC 17015:2005.

3. * = Analito no declarado en el alcance acreditado y/o autorizado que se obtiene por método acreditado y/o autorizado.

4. Uso autorizado del plaguicida en el país correspondiente indicado en código ISO 3166-1 alfa-2. Los LMR de cada país se indican en la misma tabla de resultados.

5. En caso de no haber sido detectado algun pesticida se observa una banda verde fuerte. En caso de haber detectado algun pesticida dentro de los límites permitidos se observa una banda

amarilla. En caso de haber detectado algun pesticida fuera de los límites permitidos se observará una banda roja. En caso de haber detectado algún pesticida prohibido se observará una

banda roja.

6. Las bandas de colores son de apoyo visual basadas en los LMRs de cada país y no representan un resultado.

7. ** = Se toma el LMR de Isomero Lambda para la molécula Cyhalothrin (Isomero Gamma y Lambda) , para Cypermethrin a (Zeta-Cypermethrin) se toma el LMR de Zeta-Cypermethrin y

para el LMR de Esfenvalerate + Fenvalerate se toma el de Esfenvalerate.

8. 2 = Para Canadá se considera el default LMR de 0.1 ppm según el punto 5.2.1.4.2 Food and Drug Regulations de Canada Food Inspection Agency http://www.inspection.gc.ca/food/meat-

and-poultry-products/manual-of-procedures/chapter-5/eng/1395150894222/1395150895519?chap=2.

9. Las bandas de colores de cada molécula son de apoyo visual basadas en los LMRs de cada país y no representan un resultado.

10. **El LMR de Dicofol es la suma de Kelthane(Dicofol) y op Dicofol

1. En las tablas correspondientes se presenta el punto más bajo de la calibración (LCL).

2. Las tablas correspondientes NO REPRESENTAN UN RESULTADO. Son datos informativos de calidad.

3.Incertidumbre = 50 % según "Method validation and quality control procedures for pesticide residues analysis in food and feed". No. de Documento SANCO/10684/2009. Punto 91

Límites Máximos de Residuos (LMR) para Zarzamora indicados en El Catálogo Oficial

de Plaguicidas de México 2004.

Límites Máximos de Residuos (LMR) para Zarzamora indicados en Enviromental

Protection Agency (EPA) Estados Unidos.

Límites Máximos de Residuos (LMR) para Zarzamora indicados en Electronic Code of

Federal Regulations, (e-CFR TM) Estados Unidos.

1. El cliente tiene cinco días naturales posteriores a la emisión de resultados**** para poder hacer alguna observación o reclamación al respecto, ya que en caso de no hacerlo en este

periodo de tiempo se considerará este informe como aceptado.

2. Las muestras podrán ser desechadas a los 5 días después de la emisión de resultados****, únicamente las muestras para análisis microbiológico serán desechadas 24 h después de ser

recibidas.

3. La información inscrita en el presente "Informe de resultados de análisis" se trata con estricto apego al aviso de privacidad de Análisis Técnicos S.A. de C.V. acatando a los artículos

tercero transitorio, 16 y 17 de la Ley Federa de Protección de Datos Personales en Posesión de los Particulares, con la finalidad de regular su tratamiento legítimo, controlado e informado, a

efecto de garantizar la privacidad y el derecho a la autodeterminación informativa de las personas.

4. Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas.

5. Análisis Técnicos S.A. de C.V. no se encuentra acreditado en muestreo.

6. Los LMR de los paises son un dato de referencia, solicitando revisar los sitios oficiales de cada país ya que pueden cambiar o modificarse.

7. El resultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A. de C.V., por lo cual no se hace responsable de la representatividad del resultado para el

total del producto

8. Este formato de interpretación está protegido y registrado ante el Instituto Nacional del Derecho de Autor (INDAUTOR), así mismo, los logotipos y nombre de Agrolab y sus filiales se

encuentran registrados ante el Instituto Mexicano de la propiedad Industrial (IMPI). Se prohibe su reproducción total o parcial, para otro fin que no sea la interpretación de resultados, sin

previa autorización.

9. El presente informe de resultados no será válido si presenta raspaduras, tachaduras o enmendaduras.

10. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.

11. El laboratorio Análisis Técnicos S.A. de C.V. no es responsable de la actualización de los LMR's ya que son considerados como un dato informativo. Es responsabilidad del usuario del

Informe revisar los sitios oficiales para LMR de cada país ya que la información puede cambiar o modificarse.

12. La detección del residuo del plaguicida por arriba del límite de cuantificación se reporta como ppm (mg//Kg) , por debajo del límite de cuantificación se reportar como <LCL ppm (mg/Kg)

y por debajo del LD se considera como no determinado.

****La emisión del resultados, contempla el informe final destinado a ser enviado al cliente (PDF). La entrega de resultados al cliente, se encuentra sujeta a confirmación de pago.

13.La regla de decisión no incluye la incertidumbre.


Información adicional y complementaria

Información general

Fecha de reporte: 2018-10-15 7 de 7 Revisión:Página:

Final del informe

AR271-TS-61

Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El resultado representa la muestra que fue recibida en las instalaciones de

Análisis Técnicos S.A. de C.V. , por lo cual no se hace responsable de la representatividad del resultado para el total del producto. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.




Report Date: 2018-10-15 Page: 1 of 7 Revision AR272-TS-61


Client Information

Applicant: ALFREDO OSEGUERA DÍAZ Company: SUN BELLE MÉXICO S.A. DE C.V.


[email protected],

[email protected]

Address: Km 1 Carr. los Reyes-Jacona S/N City or Town: Los Reyes

State: Michoacán ZIP Code: 60330

Telephone: 3545427328 Ext. 133 E-mail:


Billing Information

Corporate name: Fruits-Giddings SA de CV RFC SBM040520QN6

Address: Km. 1 Carretera los Reyes- Jacona Sn City or Town: Los Reyes

State: Michoacán ZIP Code: 60330

Sample Reg. No. P-18-24827 Registry Book: oct-18

Receipt Date: 2018-10-11 Start Date: Termination Day: 2018-10-152018-10-11

Sample Information

Telephone: 3545420170 Ext. SD E-mail:[email protected], [email protected],

[email protected]


Pesticides Multiresidual Analysis


Tupy|Otras

Analyzed part: Fruit Sample status: Frozen Less Than 1.5Kg

Variety:

Amount recieved:

Common Name: Blackberry Scientific Name: Rubus Ulmifoli

Sampling Place: DIRECCION: LOS REYES,

MICHOACÁNSampling Method: Random SDWarehouse RFC:

Producer:NEFTALI ARMANDO GONZALEZ

VAZQUEZHarvest Place: LA TIJERA, LOS REYES MICH SDSAGARPA Reg.:

Commercial use: Human Commercial Destination: National And Foreign Market

Sampling date: 10/09/2018

Sample received in conditions for analysis.

2906-01 SECTOR 1

Final Destination:

Observations:

SDCustoms House:

USA AND EU

Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued result only affects the sample received at the facility of Análisis Técnicos S.A. de C.V, therefore it́ s not responsible for the

representation of the result for the total product. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.

This form of interpretation is protected and registered with the Instituto Mexicano de la Propiedad IntelectualIts total or partial reproduction without authorization is prohibited. This report will not be valid if you have scratches, erasures or amendments.

Controlled document ISO/IEC 17025:2005


B B

B B

B B

B B

B B

B BB BB B

B B

B BB BB BB BB B

B B


B B

B BB BB BB BB B

B B

B B

B B

B B

B V

B B

B B

B BB BB B

B B

B BB B

B B

B B

B B

B B

B B

B B

B BB BB BB B

B B

B B


KOR CHN

1.5 0.5

3 1

- - - -

- - - -

0.01 0.1

- - - -

0.01 0.05

- - - -

0.05 0.1

0.01 - -

0.01 0.01

0.01 2

- - - -

- - - -

- - - -

0.7

0.01 - -

0.02 1

- - - -

0.01 0.1

OXYDEMETON

METHYL

METABOLITE

OXYDEMETON

METHYL METABOLITE

0.01 - -

- - - -

0.2 0.5

0.01 0.5

0.5 2

0.05 0.1

0.05 0.05

- - - -

- - - -

- - - -

- -

0.01 1

0.01 - -

0.01 - -

0.01 0.05

- - - -

0.01 0.4

0.01 1

0.05 0.1

- - - -

- - - -

0.02 - -

3 1

0.01 0.05

- - - -

0.02

0.01 - -

0.01 0.5

0.01 0.05

0.01 0.3

0.1 - -

0.01 1

0.02 0.02

0.01 - -

20 5

0.01 0.5

THIOPHANATE

METHYL/ BENOMYL

METABOLITE

THIOPHANATE

METHYL/ BENOMYL

METABOLITE

0.01 - -

0.01 0.05

0.05 0.05

1 0.7

- - - -

0.01

- -

0.1

- - - -

10 5

0.01 0.1

- - - -

0.01 5

0.05 - -

1.5 - -

0.05 1

0.01 - -

0.01 0.5

0.01 0.01

0.01 0.01

0.01 0.01

0.01 0.01

7 7

0.01 0.05

1 1

0.01 1

- - - -

0.01 - -

0.02 - -

0.05 0.3

5 1

- - - -

0.05 0.05

0.01 0.02

0.01 0.02

0.01 0.05

0.02 0.02

0.02 0.02

0.02 0.02

0.01 0.01

0.01 0.05

0.01 - -

- - - -

0.05 - -

- - - -

- - - -

LINURON


- - - -

0.08 0.05

0.01 1

2 0.3

0.01 0.02

0.02 1

Report Date: 2018-10-15 Page: 2 of 7 Revision: AR272-TS-61

Chromatogram GC: P-18-24827 10-11-2018.D Chromatogram LC: P-18-24827 10-14-2018.d


Analysis Results


VAZQUEZOrchard: LA TIJERA, LOS REYES MICH SAGARPA Reg.: SD

Client: SUN BELLE MÉXICO S.A. DE C.V. Sample: Blackberry Lab Reg. No.: P-18-24827

US JPMX CA EU

JP CA CHN

2, 4-D Methyl ester GC/MSMS 0.2 0.2 0.1 0.1 0.1

US JP CA CHN MX US

Banned pesticides residues have been detected

Analyte Analyzed by

Authorized use

MRL (ppm) Obtained amount in mg/kg

(ppm)Analyte Analyzed by

Authorized use

MRL (ppm) Obtained amount in mg/kg

(ppm)MX EU KOR EU KOR

0.1 0.05

0.1 0.01 < LCL

2,6 Dichlorobenzonitrilo GC/MSMS - - - - - - - - - -

< LCL Chlordimeform GC/MSMS - - - - 0.01

0.1 0.02 < LCL

2,3 dihydro-2,2dimethylbenzofuran 7-ol GC/MSMS - - - - - - - - - -

< LCL Chlordane- a GC/MSMS 0.1 0.1 0.02

0.1 - - < LCL

3-Hydroxy carbofuran LC/MSMS - - - - - - - - - -

< LCL Chlorfenvinphos LC/MSMS - - - - 0.05

0.1 - - < LCL

3,4 Dichloroaniline GC/MSMS LINURON METABOLITELINURON

METABOLITE

LINURON

METABOLITE

LINURON


< LCL Chlorfenapyr GC/MSMS - - - - 0.01

0.1 - - < LCL

Acephate LC/MSMS - - - - 0.01 0.1 0.5

< LCL Chloridazon (Pyrazon) LC/MSMS - - - - 0.01

0.1 - - < LCL

Abamectin LC/MSMS 0.2 0.2 0.01 0.2 - -

< LCL Chlorfluazuron LC/MSMS - - - - 2

0.1 - - < LCL

Acetochlor LC/MSMS - - - - 0.01 0.1 - -

< LCL Chlorobenzilate GC/MSMS - - - - 0.01

0.1 - - < LCL

Acetamiprid LC/MSMS 1.6 1.6 2 4 2

< LCL Chlormequat LC/MSMS - - - - 0.05

- - - - < LCL

Alachlor LC/MSMS - - - - 0.01 0.1 - -

< LCL Chloropropylate GC/MSMS - - - - - -

0.1 - - < LCL

Acrinathrin GC/MSMS - - - - 2 0.1 - -

< LCL Chloroneb GC/MSMS - - - - 0.01

0.1 - - < LCL

Aldicarb sulfone LC/MSMS - - - - 0.01 0.1 0.02

< LCL Chlorotoluron LC/MSMS - - - - 0.01

0.1 - - < LCL

Aldicarb LC/MSMS - - - - 0.01 0.1 0.02

< LCL Chlorothalonil GC/MSMS - - - - 10

0.1 - - < LCL

Aldrin GC/MSMS 0.05 0.05 0.05 0.1 0.05

< LCL Chlorpropham GC/MSMS - - - - 0.01

0.1 - - < LCL

Aldicarb-sulfoxide (Aldoxicarb) LC/MSMS - - - - 0.01 0.1 0.02

< LCL Chloroxuron LC/MSMS - - - - 0.01

0.1 - - < LCL

Ametryn GC/MSMS - - - - 0.01 0.1 - -

< LCL Chlorpyrifos methyl GC/MSMS - - - - 0.05

0.1 - - < LCL

Ametoctradin LC/MSMS - - - - 0.01 0.1 - -

< LCL Chlorpyrifos GC/MSMS - - - - 1

- - - - < LCL

Atrazine GC/MSMS - - - - 0.02 0.1 - -

< LCL Chlortal dimethyl GC/MSMS - - - - - -

0.1 - - < LCL

Aminocarb LC/MSMS - - - - - - - - - -

< LCL Chlorsulfuron LC/MSMS - - - - 0.01

0.1 - - < LCL

Azamethiphos LC/MSMS - - - - 0.01 0.1 - -

< LCL Clodinafop-propargyl LC/MSMS - - - - 0.02

- - - - < LCL

Atrazine-2-hydroxy LC/MSMS - - - - - - - - - -

< LCL Chlorthiophos GC/MSMS - - - - - -

0.1 - - < LCL

Azinphos-methyl GC/MSMS - - - - 0.01 2 1

< LCL Clomazone* LC/MSMS - - - - 0.02

0.1 - - < LCL

Azinphos-ethyl LC/MSMS - - - - 0.01 0.1 - -

< LCL Clofentezine LC/MSMS - - - - 0.01

< LCL

0.1 - - < LCL

Azoxystrobin GC/MSMS 5 5 5 5 - -

< LCL Cloquintocet-mexyl LC/MSMS - - - - 0.01

Coumaphos GC/MSMS - - - - - - 0.1 0.05 < LCL0.01 - -

< LCLBenalaxyl GC/MSMS - - - - 0.05 0.1 - -

0.02 - -

Baycarb LC/MSMS - - - - - - - - - - < LCL Crimidine LC/MSMS - - - - - - - - - -

0.1 - -

- - - -

0.01 - -

0.01 < LCL

Bensulfuron-methyl LC/MSMS - - - - 0.01 0.1 - -

< LCL Cyantraniliprole* LC/MSMS - - - - 0.01Bendiocarb LC/MSMS - - - - 0.01 0.1 - - 0.7

0.01 2

0.1 - - < LCL

Benzoximate LC/MSMS - - - - 0.01 0.1 - -

< LCL Cycloate LC/MSMS - - - - 0.01

< LCL

Bensulide LC/MSMS - - - - 0.01 0.1 - -

< LCL Cyazofamid LC/MSMS - - - - 0.01

0.01 - -

0.01 0.2 < LCL

BHC lindane beta GC/MSMS 0.5 0.5 0.3 0.1 - -

< LCLCyhalothrin (Isomero Lambda

y gamma)**GC/MSMS - - - - 0.5

0.1 - - < LCL

BHC lindane alpha GC/MSMS 0.5 0.5 0.3 0.1 - -

< LCL Cyfluthrin GC/MSMS - - - - 0.02

0.1 - - 0.013

BHC lindane gamma GC/MSMS 0.5 0.5 0.3 0.1 - -

< LCLCypermethrin a (Zeta-

Cypermethrin)**GC/MSMS 0.8 0.8 0.5

4 - - < LCL

BHC lindane delta GC/MSMS 0.5 0.5 0.3 0.1 - -

< LCL Cymoxanil LC/MSMS 4 4 4

10 - - < LCL

Bifenox GC/MSMS - - - - 0.01 0.1 - -

< LCL Cyprodinil GC/MSMS 10 10 10

0.1 - - < LCL

Bifenazate LC/MSMS 5 5 7 5 7

< LCL Cyproconazole LC/MSMS - - - - 0.5

- - - - < LCL

Bitertanol LC/MSMS - - - - 0.05 0.1 - -

< LCL DDD-o,p GC/MSMS - - - - - -

0.1 - - < LCL

Bifenthrin GC/MSMS 1 1 1 1 1

< LCL Cyromazine LC/MSMS - - - - 0.01

- - - - < LCL

Boscalid LC/MSMS 10 10 10 6 - -

< LCL DDE-o,p GC/MSMS - - - - - -

- - - - < LCL

Bolstar GC/MSMS - - - - - - - - - -

< LCL DDD-p,p GC/MSMS - - - - - -

- - - - < LCL

Bromophos methyl GC/MSMS - - - - - - - - - -

< LCL DDT-o,p GC/MSMS - - - - - -

- - - - < LCL

Bromacil GC/MSMS - - - - 0.01 0.1 - -

< LCL DDE-p,p GC/MSMS - - - - - -

- - - - < LCL

Bromuconazole* LC/MSMS - - - - 0.01 0.1 - -

< LCLDEET (Diethyl-m-toluamide,

N,N-)GC/MSMS - - - - - -

- - - - < LCL

Bromopropylate GC/MSMS - - - - 2 0.1 - -

< LCL DDT-p,p GC/MSMS - - - - - -

- - - - < LCL

Buprofezin GC/MSMS - - - - 0.01 0.1 - -

< LCL Demeton O GC/MSMS - - - - - -

0.1 - - < LCL

Bupirimate LC/MSMS - - - - 0.01 0.1 - -

< LCL Deltamethrin GC/MSMS - - - - 0.1

OXYDEMETON

METHYL

METABOLITE

< LCL

Butocarboxim-sulfoxide LC/MSMS - - - - 0.01 0.1 - -

< LCL Demeton-s-methyl-sulfone LC/MSMSOXYDEMETON

METHYL

METABOLITE

OXYDEMETON

METHYL

METABOLITE

OXYDEMETON

METHYL

METABOLITE

0.1 0.02 < LCL

Butocarboxim* LC/MSMS - - - - 0.01 0.1 - -

< LCL Demeton S GC/MSMS - - - - 0.4

0.01

0.1 - -

< LCL Desmetryn GC/MSMS - - - - - -

0.1 - - < LCL

Buturon LC/MSMS - - - - - - - - - -

< LCL Desmedipham LC/MSMS - - - - 0.01- -

- - - -

0.01 - -

12 12 10 10 - -

< LCL Diazinon GC/MSMS 0.75 0.75 0.1

- - - - < LCL

Captan GC/MSMS 25 25 0.01 0.1 - -

< LCL Dialifos LC/MSMS - - - - - -Butylate GC/MSMS - - - - 0.01

Carbetamide LC/MSMS - - - - 0.01 0.1 - -

TRACES Dichlorvos GC/MSMS - - - - 0.1

- - - - < LCL

Carbendazim LC/MSMSTHIOPHANATE

METHYL/ BENOMYL

METABOLITE

THIOPHANATE

METHYL/ BENOMYL

METABOLITE

THIOPHANATE

METHYL/ BENOMYL

METABOLITE

THIOPHANATE

METHYL/ BENOMYL

METABOLITE

THIOPHANATE

METHYL/ BENOMYL

METABOLITE

< LCL Dichloran GC/MSMS - - - - - -

< LCL

Carbaryl GC/MSMS

- - 0.01 0.1 - -

- - < LCL

Carboxin LC/MSMS - - - - 0.01 0.1 - -

< LCL Diclofop methyl GC/MSMS - - - - 0.01Carbofuran GC/MSMS - - - - 0.3 0.1 0.02 0.1

0.1 0.02 < LCL< LCL Dieldrin

1.8 2 0.9 1

0.05 0.05

0.1 - - < LCL

0.1 - - < LCL

Carfentrazone ethyl LC/MSMS 0.1 0.1 0.1 0.1 - -

< LCL Dicrotophos LC/MSMS - - - - 0.01

0.01 0.1

0.01 0.05Chinometionate GC/MSMS - -

< LCL Difenoxuron LC/MSMS - - - - - -

0.1 - - < LCL

< LCL Diethofencarb LC/MSMS - - - - 0.01

Chlorbromuron LC/MSMS - - - - - - - - - -

< LCL Difenoconazole LC/MSMS - - - - 0.01Chlorantraniliprole LC/MSMS 1.8

GC/MSMS 0.05

< LCL

Cyanazine LC/MSMS - - - - 0.01 0.1 - - < LCL

- - - - < LCL

- - - - < LCLDiclobutrazol* LC/MSMS - - - - - -

0.1 0.2 < LCL

0.1 0.1 < LCL

- - - - < LCL

OXYDEMETON

METHYL

METABOLITE

* Analyte not declared in the scope accredited and / or licensed accredited obtained by method and / or authorized. The colored bands are visual aids based on MRLs of Mexico and are not a result. 1Maximum Resuide Limits (MRL) expressed in ppm for every country using ISO 3166 -1 alfa-2. LCL = Lowest Calibration Level ppm = Parts per million = mg/kg GC/MSMS = Gass Chromatography /Mass/Mass LC/MSMS = Liquid Chromatography /MassMass

Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued res ult only affects the sample received at the facility of Análisis Técnicos S.A. de C.V, therefore it ´s not responsible for the representation of the result for the total product.

Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product. This form of interpretation is protected and registered with the Instituto Mexicano de la Propiedad Intelectual. Its total or partial reproduction without authorization is prohibited. This report will not be valid if you have scratches, erasures or ame ndments.



Authorizes Lic. Carlos Sepúlveda Ibarra

General Director

B BB BB BB BB BR BB BB BB BB BB BB BB BB B

B B

B BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB B

B B

B B

B B

B B

B B

B BB B

B B

B BB B

B B

B B

B B

B B

B B

B BB B

0.01 0.3MALATHION

METABOLITE

MALATHION

METABOLITE

0.02 0.5

0.02 0.01

0.05 5

0.01 0.1

- - - -

0.01 0.05

4 3

0.02 - -

0.1 - -

0.02 - -

0.02 0.4

0.01 0.02

0.01 0.3

0.01 1

0.01 1

0.1 - -

0.05 0.05

0.01 - -

0.02 0.02

0.02 1

0.01 - -

0.01 0.05

0.01 0.05

0.5 1

0.05 2

0.01 3

30 30

- - - -

0.01 0.01

0.05 - -

5 0.04

0.05 0.05

0.5 0.5

0.01 - -

- - - -

0.03 3

0.01 0.05

- - - -

0.01 - -

0.01 0.05

0.01 0.02

0.01 0.05

0.01 0.01

0.01 0.01

0.01 - -

0.01 - -

- - - -

0.01 - -

0.03 0.5

0.01 0.2

0.01 1

0.01 - -

5 5

0.05 0.05

0.05 0.3

0.01 - -3 0.7

0.01 - -

0.01 - -

0.01 - -

0.01 0.3

0.01 0.5

0.01 - -

0.01 - -

0.7 0.5

- - - -

0.01 0.02

- - - -

0.02 0.02

- - - -

0.01 0.01

1 1

0.01 0.3

0.01 2

0.01 0.2

- - - -

0.005 0.05

0.01 0.5

0.05 0.5

5 2

0.01 - -

- - - -

15 15

0.01 0.3

0.01 0.05

0.05 0.5

0.02 0.1

0.02 0.2

0.05 0.2

0.05 0.2

0.01 0.01

0.05 0.5

0.02 - -

- - - -

0.01 0.05

0.01 5

0.01 5

0.01 0.05

0.01 0.1

0.01 0.1

0.01 1

0.01 - -

0.01 - -

0.01 0.2

0.01 0.03

0.05 0.2

- - - -

- - - -

0.01 - -

0.01 0.01

0.01 1

0.05 1

0.01 1

0.01 1

0.01 - -




Analysis Results

Producer:NEFTALI ARMANDO

GONZALEZ VAZQUEZOrchard: LA TIJERA, LOS REYES MICH SAGARPA Reg.: SD

Client:SUN BELLE MÉXICO S.A. DE

C.V.Sample: Blackberry Lab Reg. No.: P-18-24827

US JP CA EUMX

JP CA CHN

Diflufenican LC/MSMS - - - - 0.01 0.1 - -

US JP CA CHN MX US


AnalyteAnalyzed

by

Authorized use

MRL (ppm) Obtained amount in

mg/kg (ppm)Analyte

Analyzed

by

Authorized use


mg/kg (ppm)MX EU KOR EU KOR

0.01 - -

0.1 - - < LCL

Dimepax GC/MSMS - - - - - - - - - -

< LCL Fluchloralin GC/MSMS - - - - 0.01

0.1 - - < LCL

Dimefuron LC/MSMS - - - - - - - - - -

< LCL Flubendiamide LC/MSMS - - - - 0.01

0.1 - - < LCL

Dimethenamid LC/MSMS - - - - 0.01 0.1 - -

< LCL Flufenacet LC/MSMS - - - - 0.01

7 - - < LCL

Dimethachlor LC/MSMS - - - - 0.01 0.1 - -

< LCL Fludioxonil GC/MSMS 5 5 5

0.1 - - < LCL

Dimethomorph LC/MSMS - - - - 0.01 0.1 - -

0.251 Fluometuron LC/MSMS - - - - 0.02

0.1 - - < LCL

Dimethoate GC/MSMS - - - - 1 0.1 - -

< LCL Flufenoxuron LC/MSMS - - - - 0.01

0.1 - - < LCL

Dinotefuran LC/MSMS - - - - 0.01 0.1 - -

< LCL Fluoroglycofen-ethyl LC/MSMS - - - - 0.01

0.1 - - < LCL

Diniconazole LC/MSMS - - - - 0.01 0.1 - -

< LCL Fluopicolide LC/MSMS - - - - 0.01

0.1 - - < LCL

Diphenamid LC/MSMS - - - - 0.01 0.1 - -

< LCL Flurtamone LC/MSMS - - - - 0.01

0.1 - - < LCL

Dioxathion GC/MSMS - - - - 0.01 0.1 - -

< LCL Fluoxastrobin LC/MSMS - - - - 0.01

0.1 - - < LCL

Disulfoton-sulfone LC/MSMS - - - - 0.05 0.1 - -

< LCL Flutriafol LC/MSMS - - - - 0.01

0.1 - - < LCL

Disulfoton GC/MSMS - - - - 0.05 0.1 - -

< LCL Flusilazole LC/MSMS - - - - 0.01

25 - - < LCL

Dodemorph LC/MSMS - - - - 0.01 0.1 - -

< LCL Folpet GC/MSMS - - - - 0.01

- - - - < LCL

Diuron (Karmex)* LC/MSMS 0.1 0.1 0.05 0.1 - -

< LCL Fluvalinate GC/MSMS - - - - - -

- - - - < LCL

Edifenphos LC/MSMS - - - - 0.01 0.1 - -

< LCL Formetanate LC/MSMS - - - - - -

0.1 - - < LCL

Dyfonate GC/MSMS - - - - 0.01 0.1 0.01

< LCL Forchlorfenuron LC/MSMS - - - - 0.1

0.1 - - < LCL

Endosulfan I (alpha isomer) GC/MSMS - - - - 0.5 0.1 - -

< LCL Furathiocarb LC/MSMS - - - - 0.01

0.1 - - < LCL

Emamectin Benzoate LC/MSMS - - - - 0.1 0.1 - -

< LCL Fuberidazole LC/MSMS - - - - 0.01

0.1 - - < LCL

Endosulfan sulfate GC/MSMS - - - - 0.5 0.1 - -

< LCL Haloxyfop-methyl LC/MSMS - - - - 0.05

0.1 0.02 < LCL

Endosulfan II (beta isomer) GC/MSMS - - - - 0.5 0.1 - -

< LCL g Chlordan GC/MSMS 0.1 0.1 0.02

0.1 0.01 < LCL

Epoxiconazole LC/MSMS - - - - 0.01 0.1 - -

< LCL Heptachlor exo-epoxide (isomer GC/MSMS 0.05 0.05 0.01

0.1 0.01 < LCL

Endrin GC/MSMS - - - - 0.01 0.1 0.05

< LCL Heptachlor GC/MSMS 0.05 0.05 0.01

0.1 - - < LCL

Etaconazole (Etaconazole I y II) LC/MSMS - - - - - - - - - -

< LCL Hexachlorobenzene GC/MSMS 0.05 0.05 0.01

0.1 - - < LCL

Esfenvalerate + Fenvalerate* (**) GC/MSMS 1 1 1 0.1 0.2

< LCL Heptenophos LC/MSMS - - - - 0.01

0.1 - - < LCL

Ethiofencarb LC/MSMS - - - - 0.01 0.1 - -

< LCL Hexazinone GC/MSMS - - - - 0.01

0.1 - - < LCL

Ethalfluralin GC/MSMS - - - - 0.01 0.1 - -

< LCL Hexaconazole LC/MSMS - - - - 0.01

0.1 - - < LCL

Ethirimol LC/MSMS - - - - - - - - - -

< LCL Imazalil LC/MSMS - - - - 0.02

1.5 - - < LCL

Ethiofencarb-sulfone LC/MSMS - - - - 0.01 0.1 - -

< LCL Hexythiazox LC/MSMS 1 1 0.01

0.1 - - < LCL

Ethylan GC/MSMS - - - - - - - - - -

< LCL Imazaquin LC/MSMS - - - - 0.05

0.1 - - < LCL

Ethoprop GC/MSMS - - - - 0.01 0.1 0.02

< LCL Imazapyr LC/MSMS - - - - 0.01

0.1 - - < LCL

Etofenprox GC/MSMS 5 5 0.01 0.1 - -

< LCL Imidan GC/MSMS - - - - 0.1

2.5 - - < LCL

Etion GC/MSMS - - - - 0.3 0.1 - -

< LCL Imidacloprid LC/MSMS 2.5 2.5 4

25 - - < LCL

Famoxadone LC/MSMS 10 10 10 10 - -

< LCL Iprodione GC/MSMS 25 25 12

0.1 - - < LCL

Etoxazole LC/MSMS 1.5 1.5 0.01 1.5 - -

< LCL Indoxacarb GC/MSMS - - - - 0.01

- - - - < LCL

Fenarimol LC/MSMS - - - - 1 0.1 - -

< LCL Irgarol LC/MSMS - - - - - -

0.1 - - < LCL

Fenamiphos LC/MSMS - - - - 0.02 0.1 0.02

< LCL Iprovalicarb LC/MSMS - - - - 0.01

0.1 0.01 < LCL

Fenbuconazol LC/MSMS - - - - 0.01 0.1 - -

< LCL Isofenphos LC/MSMS - - - - 0.01

0.1 0.01 < LCL

Fenazaquin LC/MSMS - - - - 0.01 0.1 - -

< LCL Isazophos LC/MSMS - - - - 0.01

0.1 - - < LCL

Fenchlorphos GC/MSMS - - - - 0.01 0.1 - -

< LCL Isoproturon LC/MSMS - - - - 0.01

0.1 - - < LCL

Fenbutatin oxide* LC/MSMS - - - - 1 0.1 - -

< LCL Isoprocarb LC/MSMS - - - - 0.01

3 - - < LCL

Fenhexamid LC/MSMS 20 20 15 20 15

< LCL Kelthane*** GC/MSMS - - - - 3

0.1 - - < LCL

Fenfuram LC/MSMS - - - - - - - - - -

< LCL Isoxaflutole LC/MSMS - - - - 0.01

0.1 - - < LCL

Fenoxaprop-ethyl LC/MSMS - - - - 0.1 0.1 - -

< LCL Lenacil LC/MSMS - - - - 0.3

0.1 - - < LCL

Fenitrothion GC/MSMS - - - - 0.8 0.1 0.5

< LCL Kresoxim-methyl LC/MSMS - - - - 0.01

0.1 - - < LCL

Fenpropathrin GC/MSMS 12 12 5 12 5

< LCL Lufenuron LC/MSMS - - - - 0.01

0.1 - - < LCL

Fenoxycarb LC/MSMS - - - - 0.05 0.1 - -

< LCL Linuron LC/MSMS - - - - 0.2

8 - - < LCL

Fenpropimorph LC/MSMS - - - - 0.05 0.1 - -

< LCL Malathion GC/MSMS 8 8 8

MALATHION

METABOLITE

MALATHION

METABOLITE< LCL

Fenpropidin LC/MSMS - - - - 0.01 0.1 - -

< LCL Malaoxon LC/MSMSMALATHION

METABOLITE

MALATHION

METABOLITE

MALATHION

METABOLITE

0.1 - - < LCL

Fenson GC/MSMS - - - - - - - - - -

< LCL Mandipropamid LC/MSMS - - - - 0.01

0.1 5 < LCL

Fenpyroximate LC/MSMS - - - - 0.01 0.1 - -

< LCL Mancozeb LC/MSMS - - - - 5

0.1 - - < LCL

Fenthion GC/MSMS - - - - 0.01 0.1 0.05

< LCL Mecarbam LC/MSMS - - - - 0.01

- - - - < LCL

Fensulfothion GC/MSMS - - - - 0.01 0.1 - -

< LCL Mebendazole LC/MSMS - - - - - -

0.1 - - < LCL

Fipronil GC/MSMS - - - - 0.01 0.1 0.02

< LCLMetalaxyl-M (Mefenoxam, R-

enantiomero de metalaxyl)GC/MSMS 0.7 0.7 0.2

0.1 - - < LCL

Fenuron LC/MSMS - - - - - - - - - -

< LCL Mepanipyrim LC/MSMS - - - - 0.01

0.1 - - < LCL

Flamprop-isopropyl LC/MSMS - - - - - - - - - -

< LCL Metazachlor LC/MSMS - - - - 0.01

0.1 - - < LCL

Flamprop methyl LC/MSMS - - - - 0.01 0.1 - -

< LCL Metamitron LC/MSMS - - - - 0.01

LC/MSMS - - - - 0.01 0.1 - -

< LCL Methabenzthiazuron LC/MSMS - - - - 0.01

0.1 - - < LCL

Flazasulfuron LC/MSMS - - - - 0.1 0.1 - -

< LCL Metconazole LC/MSMS - - - - 0.01

0.01 0.05

0.01 0.1

CHNKOR

0.1 0.05 < LCL< LCL Methidathion LC/MSMS - - - - 0.2

0.1 0.05 < LCL

Fluazifop-butyl LC/MSMS - - - - 0.01 0.1 - -

< LCL Methamidophos LC/MSMS - - - - 0.01

0.1 - - < LCL

Flonicamid

*Analyte not declared in the scope accredited and / or licensed accredited obtained by method and / or authorized. The colored bands are visual aids based on MRLs of Mexico and are not a result. 1Maximum Resuide Limits (MRL) expressed in ppm for every country using ISO 3166-1 alfa-2. LCL = Lowest Calibration Level ppm = Parts per million = mg/kg GC/MSMS = Gass Chromatography /Mass/Mass LC/MSMS = Liquid Chromatography /MassMass

Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued result only affects the sample received at the facility of Análisis Técnicos S.A. de C.V, therefore it´s not responsible for the

representation of the result for the total product. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.

This form of interpretation is protected and registered with the Instituto Mexicano de la Propiedad Intelectual. Its total or partial reproduction without authorization is prohibited. This report will not be valid if you have scratches, erasures or amendments.




General Director

B BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB B

B B

B B

B BB B

B B

B B

B B

B B

R B

B B

B B

B BB BB BB BB BB BB BB BB B

B B

B

B

B

B

B

BBBBBBBBBBBB

0.02 - -

0.05 0.1

0.05 1

0.01 0.01

0.05 0.05

0.01 - -

0.01 - -

- - - -

0.1 1

0.01 0.25

0.01 0.05

0.01 0.05

0.01 7

0.01 - -

0.01 - -

0.01 0.5

0.05 0.05

0.01 - -

0.01 - -

0.01 - -

0.01 2

0.01 2

- - - -

- - - -

- - - -

0.01 0.05

- - - -

0.02 - -

0.01 0.1

0.01 - -

0.05 5

0.01 - -

0.01 0.5

- - - -

0.01 0.05

0.01 0.05

0.01 0.05

0.01 5

- - - -

0.05 0.3

0.01 0.2

0.1 0.2

0.05 2

0.05 0.05

QUINTOCENE

(PENTACHLORONITR

OBENZENE)METABOL

ITE

QUINTOCENE

(PENTACHLORON

ITROBENZENE)M

ETABOLITE

- - - -

0.02 0.01

- - - -

DIMETHOATE

METABOLITE

DIMETHOATE

METABOLITE

0.02 1

- - - -

0.01 1

0.01 0.5

0.01 - -

0.05 0.05

0.5 0.05

0.01 - -

1 1

- - - -

0.1 0.05

- - - -

0.01 0.3

0.01 0.2

0.01 0.1

0.01 1

0.01 0.05

0.01 - -

- - - -

0.01 5

0.1 0.05

0.01 - -

0.01 0.5

- - - -

0.01 - -

EU KOR EU KOR

0.2 0.05

0.2 0.05

0.2 0.05

0.01 1

- - - -

0.01 14

0.01 0.5

0.01 2

- - - -

- - 0.05

0.01 0.05

4 1

0.01 0.02

0.01 1

Pencycuron LC/MSMS - - - - 0.01 0.1 - - < LCL

Penconazol LC/MSMS - - - - 0.2

LA TIJERA, LOS REYES MICH SAGARPA Reg.: SD

US JP CA EU

Piperalin


AnalyteAnalyzed

by

Authorized use

MRL (ppm)

MX JP CA CHN

0.2

7 0.1 - -

- - - -

0.2 0.1 - -

0.01< LCL Pirimiphos-ethyl

0.1< LCL Pirimicarb 1

- -

< LCL Primisulfuron-methyl

- -

- -

- - < LCL

0.03

Sethoxydim* LC/MSMS 5 5 1 5 - -

Simazine GC/MSMS

0.1 - -

Analysis Results

AnalyteAnalyzed

by

Authorized use


mg/kg (ppm)CA CHN

LC/MSMS 6 6 0.01

Methiocarb sulfone GC/MSMS - - - - 0.05

Methoprotryne LC/MSMS - - - - - -

Methomyl LC/MSMS - - - -

Methiocarb sulfoxide GC/MSMS

Methoxyfenozide

Methoxychlor GC/MSMS - - - -

- -

< LCL Picoxystrobin


P-18-24827SUN BELLE MÉXICO S.A. DE C.V. Sample: Blackberry Lab Reg. No.:Client:


VAZQUEZOrchard:

US JP MX US

Chromatogram GC: P-18-24827 10-11-2018.D Chromatogram LC:

Obtained amount in

mg/kg (ppm)

P-18-24827 10-14-2018.d MXAgrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab

- - - -

LC/MSMS - - - - 0.01 < LCL

8 < LCL

0.1

- -LC/MSMS 8 8 8

- -

Methiocarb GC/MSMS - - - - 0.05 0.1 - -

- - < LCL- -< LCL

0.1 - -

LC/MSMS - -0.1

- - - - 0.05 0.1 - -

0.011 LC/MSMS - - - -0.1 0.2

< LCL Piperonyl Butoxide

< LCL Piperophos < LCL

< LCLLC/MSMS - - - - 0.1< LCL Pirimiphos-methyl6

0.1 - - < LCLLC/MSMS - - - - 0.01

Metolachlor LC/MSMS 0.1- - - - 0.01 0.1 - -

0.01 0.2

0.05 0.1

0.01 - -

0.05 1

Metolcarb LC/MSMS - - - - 0.01 0.1 - -

< LCL Prochloraz < LCLLC/MSMS - -

< LCLLC/MSMS - - - - 0.5

Metobromuron LC/MSMS - - - - 0.01 0.1 - -

0.1 - - < LCLLC/MSMS - - - -

< LCL Procymidone

0.1

0.1

- - 0.05

- - < LCLGC/MSMS - - - - 1.5

< LCL Profluoralin

< LCL Promecarb

< LCL

Metoxuron LC/MSMS - - - - - - - - - -

< LCL Profenofos GC/MSMS - - - - 0.01

- - - - < LCLGC/MSMS - - - - - -

Metosulam LC/MSMS - - - - 0.01 0.1 - -

Metribuzin GC/MSMS - - - - 0.01 0.1 - - < LCL

GC/MSMS - - - - - -

- - < LCL

Metrafenone LC/MSMS - - - - 0.01 0.1 - -

Mexacarbate LC/MSMS - - - - - - - -

Mevinphos GC/MSMS - - - - 0.01 0.1 - - < LCL

Metsulfuron-methyl* LC/MSMS - - - - 0.01 0.1

< LCL

Monolinuron LC/MSMS - - - - 0.01 0.1 - - < LCL

Monocrotophos LC/MSMS - - - - 0.01 0.1

Mirex GC/MSMS - - - - 0.01 0.1 0.01 < LCL

0.01 0.2

0.01 - -

- - < LCL

Napropamide LC/MSMS 0.1 0.1 0.1 0.1 - - < LCL

N-2,4-Dimethylphenyl formamide

(2,4-DMPF)LC/MSMS - - - - - - - -

- - < LCL

Myclobutanil GC/MSMS 2 2 1 2 - - < LCL

Monuron LC/MSMS - - - - 0.01 0.1

- - < LCL

Norflurazon LC/MSMS 0.1 0.1 0.1 0.1 - - < LCL

Nitrapyrin GC/MSMS - - - - 0.01 0.1

- - < LCL

Nicosulfuron LC/MSMS - - - - 0.01 0.1 - - < LCL

Neburon LC/MSMS - - - - - - - -

DIMETHOATE

METABOLITE0.226

op Dicofol*** GC/MSMS - - - - 3 3 - - < LCL

Omethoate LC/MSMSDIMETHOATE

METABOLITE

DIMETHOATE

METABOLITE

DIMETHOATE

METABOLITE

DIMETHOATE

METABOLITE

- - < LCL

Ofurace LC/MSMS - - - - - - - - - - < LCL

Novaluron* LC/MSMS - - - - 0.01 0.1

< LCL

Oxydemeton-methyl LC/MSMS - - - - 0.02 0.1 - - < LCL

Oxamyl LC/MSMS - - - - 0.01 0.1

- - < LCL

Oxadixyl LC/MSMS - - - - 1 0.1 - - < LCL

Ovex GC/MSMS - - - - - - - -

Paraoxon-methyl LC/MSMS - - - - - - - - - - < LCL

Paraoxon LC/MSMS - - - - - - - -

- - < LCL

Paclobutrazol (Bonzi) LC/MSMS - - - - 0.01 0.1 - - < LCL

Oxyfluorfen GC/MSMS 0.05 0.05 0.01 0.1

- - - -

GC/MSMS - - - - - - - - - -

0.01 < LCL

Parathion methyl GC/MSMS - - - - 0.2 0.1 0.02 < LCL

Parathion GC/MSMS - - - - 0.5 0.1

- - < LCLPendimethalin LC/MSMS 0.1 0.1 0.05 0.1

- - < LCL

Permethrin GC/MSMS - - - - 1 0.1 1 < LCL

Pentachlorophenol GC/MSMS - - - - 0.01 0.1

0.1

Pentachloronitrobenzene GC/MSMS - - - - 0.02 0.1 - - < LCL

Pentachloroaniline GC/MSMS

QUINTOCENE

(PENTACHLORON

ITROBENZENE)M

ETABOLITE

QUINTOCENE

(PENTACHLORONIT

ROBENZENE)META

BOLITE

QUINTOCENE

(PENTACHLORONI

TROBENZENE)MET

ABOLITE

QUINTOCENE

(PENTACHLORONI

TROBENZENE)MET

ABOLITE

QUINTOCENE

(PENTACHLORONIT

ROBENZENE)META

BOLITE

< LCL

Pentachloroanisol

Phorate GC/MSMS - - - - 0.05 0.024 0.01 < LCL

Phenyl valerate GC/MSMS - - - - - - - -

- - < LCL

Phenthoate LC/MSMS - - - - 0.01 0.1 - - < LCL

Phenmedipham LC/MSMS - - - - 0.01 0.1

Phosphamidon LC/MSMS - - - - 0.01 0.1 0.05 < LCL

Phosalone LC/MSMS - - - - 0.01 0.1

0.01 < LCL

Phorate-sulfoxide LC/MSMS - - - - 0.05 0.024 0.01 < LCL

Phorate-sulfone LC/MSMS - - - - 0.05 0.024

0.01 0.2

Picolinafen LC/MSMS - - - - 0.01 0.1 - - < LCL

Phoxim LC/MSMS - - - - 0.02 0.1 0.01 0.05

0.01 - -

- - - - < LCL

Prometon GC/MSMS - - - - - - - - - - < LCL

0.05 < LCL

- - < LCL

- - < LCL

< LCL

- - < LCL

- - < LCL

- -

Propachlor LC/MSMS - - - - 0.01 0.1 - - < LCL

Propamocarb LC/MSMS - - - - 0.05 0.1 - - < LCL

Prometryn GC/MSMS - - - - 0.01 0.1 - - < LCL

Pronamide LC/MSMS - - - - - - - - - - < LCL

Propazin GC/MSMS - - - - 0.01 0.1 - - < LCL

Propetamphos LC/MSMS - - - - 0.01 0.1 - - < LCL

Propanil LC/MSMS - - - - 0.1 0.1 - - < LCL

Propargite (Omite) LC/MSMS - - - - 0.01 0.1 - - < LCL

Propiconazole GC/MSMS 1 1 0.05 1 - - < LCL

Propoxur LC/MSMS - - - - 1 0.1 - - < LCL

Propyzamide LC/MSMS 0.05 0.05 0.01 0.1 - -

1 1 0.01 0.1 - -

- - - - 0.01 0.1

< LCL

Prosulfocarb LC/MSMS - - - - 0.01 0.1 - - < LCL

- -

- - - - 0.01 0.1 - -

< LCL

< LCL

< LCL

< LCL

< LCL

< LCL

< LCL

4

Rotenone

Sebuthylazine

LC/MSMS

LC/MSMS

LC/MSMS

LC/MSMS

LC/MSMS

LC/MSMS

GC/MSMS

LC/MSMS

LC/MSMS

LC/MSMS

LC/MSMS

LC/MSMS

GC/MSMS

Prosulfuron

Pymetrozine

Pyraclostrobin

Pyrazophos

Pyridaben

Pyrimethanil

Pyriproxyfen

Quinalphos

Quinoxyfen

Quizalofop-ethyl

Rimsulfuron

4 3 3.5 - -

- - - - 0.01 0.1 - -

- - - - 0.01 0.1 - -

15 15 10 15 - -

3 0.5

3 3

0.01 1

0.5 1

15 15

< LCL

< LCL

< LCL

< LCL

< LCL

< LCL

0.01 0.01 0.01 0.01 - -

- -

- - - - 0.02 0.1 - -

- - 0.01 0.1 - -

- - - - 0.01 0.1 - -

- - - - 0.05 0.1 - -

S-Metolachlor LC/MSMS 0.1 0.1 0.01 0.1 - - < LCL

- - - - - - - - - -

< LCL

< LCL

0.2

LC/MSMS - - - - 0.01 0.1 - - < LCLSimetryn

CHNKOR

* Analyte not declared in the scope accredited and / or licensed accredited obtained by method and / or authorized. The colored bands are visual aids based on MRLs of Mexico and are not a result. 1Maximum Resuide Limits (MRL) expressed in ppm for every country using ISO 3166-1 alfa-2. LCL = Lowest Calibration Level ppm = Parts per million = mg/kg GC/MSMS = Gass Chromatography /Mass/Mass LC/MSMS = Liquid Chromatography /MassMass

Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued result only affects the sample received at the facility of Análisis Técnicos S.A. de C.V, therefore it́ s not responsible for the representation of the result for the total

product. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.





General Director

BBBBBBBBBBBBBBBBBBBBBBBBB

B

BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBVinclozolin GC/MSMS - - - - 5 0.1 0.01 5

Vamidothion LC/MSMS - - - - 0.01 0.1 0.01 0.05 - -

< LCL

Trimidal LC/MSMS - - - - - - - - - - - - - - < LCL

Triforine LC/MSMS - - - - 0.01 0.1 0.01 0.5

< LCL

< LCL

< LCL

1.5

0.02

Spinetoram J LC/MSMS 0.8 0.8 0.7 0.05 - - < LCL0.5 1

1

Spirodiclofen LC/MSMS - - - - 0.01 1 - -

Spinosad A LC/MSMS 1 1 1 10.5

0.1

Report Date: 2018-10-15 Page: 5 de 7 Revision: AR272-TS-61


Producer: NEFTALI ARMANDO GONZALEZ VAZQUEZ Orchard: LA TIJERA, LOS REYES MICH SAGARPA Reg.: SD

Client: SUN BELLE MÉXICO S.A. DE C.V. Sample: Blackberry Lab Reg. No.: P-18-24827


MX US JP CA EU KOR

CA EU

Analysis ResultsBanned pesticides residues have been detected

CHN

Analyte Analyzed by

Authorized use

LMR (ppm)Obtained

amount in

mg/kg (ppm)MX US JP KOR CHN

- - < LCL

Spiromesifen LC/MSMS - - - - 0.01 10.1

2

0.02

0.1

- - < LCL

Spirotetramat LC/MSMS - - - - 0.01 0.2

- - < LCL

Sulfentrazone LC/MSMS 0.15 0.15 0.05 - - - - < LCL

Spiroxamine LC/MSMS - - - - 0.01 - -0.1

0.15

0.01

0.01

- - < LCL

Sulfotep LC/MSMS - - - - 0.01 - - 0.01 < LCL

Sulfosulfuron LC/MSMS - - - - 0.01 - -0.1

0.1

0.01

0.01

- - < LCL

Sumithrin GC/MSMS - - - - 0.01 0.1 - - < LCL

Sulfoxaflor LC/MSMS - - - - 0.01 0.50.1

0.1

0.01

0.02

- - < LCL

Tebufenozide LC/MSMS 3 3 3 1 - - < LCL

Tebuconazole GC/MSMS - - - - 0.01 0.50.1

0.1

0.5

0.05

Tebuthiuron LC/MSMS - - - - 0.01 - - - - < LCL

- - < LCL

Tebutam LC/MSMS - - - - 0.01 - - - - < LCL

Tebufenpyrad GC/MSMS - - - - 2 0.5

- - < LCL

Terbacil GC/MSMS 0.2 0.2 0.1 - - - - < LCL

Teflubenzuron LC/MSMS - - - - 0.01 1

0.01

- - < LCL

Terbuthylazine GC/MSMS - - - - 0.01 0.1 - - < LCL

Terbumeton LC/MSMS - - - - - - - -

0.05

- -- -

0.1

- - < LCL

Terbutryn GC/MSMS - - - - 0.01 0.05 - - < LCL

Terbuthylazine-desethyl LC/MSMS - - - - - - - -- -

0.01

- -

0.1

- - < LCL

Tetrachlorvinphos, E-isomer GC/MSMS - - - - 0.01 - - - - < LCL

Terrazole GC/MSMS - - - - - - - -- -

0.1

- -

0.01

- - < LCL

Tetrahydrophthalimide, cis-1,2,3,6-(THPI) GC/MSMS CAPTAN METABOLITE CAPTAN METABOLITE CAPTAN METABOLITE CAPTAN METABOLITE CAPTAN METABOLITE < LCL

Tetradifon GC/MSMS - - - - 1 10.1

CAPTAN METABOLITE

0.01

CAPTAN METABOLITE

- - < LCL

Thiabendazole LC/MSMS - - - - 3 3 - - < LCL

Tetramethrin LC/MSMS - - - - 0.01 - -0.1

0.1

0.01

0.01

1 < LCL

Thiamethoxam LC/MSMS 0.35 0.35 0.5 1 - - < LCL

Thiacloprid LC/MSMS - - - - 5 0.70.1

0.5

1

0.01

0.1 0.01 0.05

- - < LCL

Thifensulfuron-methyl LC/MSMS - - - - 0.01 0.05 - - < LCL

Thidiazuron LC/MSMS - - - - 0.01 0.20.1

0.1

0.01

0.01

< LCL

- -

- -

Triflusulfuron-methyl LC/MSMS - - - - 0.01 0.1 0.01 - - - -

Trifluralin GC/MSMS - - - - 0.05 < LCL

< LCL

- - < LCL

0.05

0.01

0.01

0.01

0.1

0.1

0.1

0.1

0.1

< LCL

Thiobencarb LC/MSMS - - - - 0.01 0.1 0.01 0.05 - -

Thiocyclam hydrogen oxalate GC/MSMS - - - - 3 0.1 0.01 1 - -

< LCL

Thionazin LC/MSMS - - - - - - - - - - - - - - < LCL

Thiodicarb LC/MSMS - - - - 1 0.1 0.01 1 - -

< LCL

Tokution GC/MSMS - - - - - - - - - - - - - - < LCL

Thiophanate-methyl LC/MSMS - - - - 3 6 0.1 2 - -

< LCL

Triadimefon GC/MSMS - - - - 0.1 0.1 0.01 0.05 - - < LCL

Tolyfluanid GC/MSMS - - - - 5 0.1 0.02 2 5

< LCL

Triasulfuron LC/MSMS - - - - 0.01 0.1 0.05 - - - - < LCL

Triadimenol GC/MSMS - - - - 0.5 0.1 0.01 0.5 - -

< LCL

Tribenuron-methyl LC/MSMS - - - - 0.01 0.1 0.01 - - - - < LCL

Triazophos GC/MSMS - - - - 0.01 0.1 0.01 0.05 - -

< LCL

Trichloronate GC/MSMS - - - - - - - - - - - - - - < LCL

Trichlorfon LC/MSMS - - - - 0.5 0.1 0.01 0.05 0.2

< LCL

Tricyclazole GC/MSMS - - - - 0.02 0.1 0.01 0.05 - - < LCL

Triclocarban LC/MSMS - - - - - - - - - - - - - -

< LCL

Trifloxystrobin LC/MSMS - - - - 0.01 0.1 3 0.7 - - < LCL

Trietazine LC/MSMS - - - - - - - - - - - - - -

< LCL

Triflumuron LC/MSMS - - - - 0.02 0.1 0.05 0.5 - - < LCL

Triflumizole LC/MSMS - - - - 0.01 0.1 0.1 2 - -

* Analyte not declared in the scope accredited and / or licensed accredited obtained by method and / or authorized. The colored bands are visual aids based on MRLs of Mexico and are not a result. 1Maximum Resuide Limits (MRL) expressed in ppm for every country using ISO 3166 -1 alfa-2. LCL = Lowest Calibration Level ppm = Parts per million = mg/kg GC/MSMS = Gass Chromatography /Mass/Mass LC/MSMS = Liquid Chromatography /MassMass Trazas/Traces = < 0.010 ppm.

Attention: Análisis Técnicos S.A. de C.V does not have the authority nor the faculty to deny, accept or authorize crops. The issued resu lt only affects the sample received at the facility of Análisis Técnicos S.A. de C.V, therefore it ´s not responsible for the representation of the result for the total product.

Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product. This form of interpretation is protected and registered with the Instituto Mexicano de la Propiedad Intelectual. Its total o r partial reproduction without authorization is prohibited. This report will not be valid if you have scratches, erasures or ame ndments.




General Director

Triflumuron 0.010

Trifluralin 0.010

Lufenuron 0.005 Pendimethalin 0.005 Spinetoram J 0.005

0.005 Paraoxon 0.005 Rotenone 0.005

Isofenphos 0.005 Oxyfluorfen 0.010 Quizalofop-ethyl 0.005

Triflusulfuron-methyl 0.005

Triforine 0.010

Malathion 0.010 Pentachloroanisol 0.010 Spirodiclofen 0.005

Malaoxon 0.005 Pentachloroaniline 0.010 Spinosad A 0.005

Trimidal 0.005

Vamidothion 0.005

Vinclozolin 0.010

Mandipropamid 0.005 Pentachlorophenol 0.010 Spirotetramat 0.005

Mancozeb 0.005 Pentachloronitrobenzene 0.010 Spiromesifen 0.005

Mecarbam 0.005 Phenmedipham 0.005 Sulfentrazone 0.005

Mebendazole 0.005 Permethrin 0.010 Spiroxamine 0.005

Metalaxyl-M (Mefenoxam, R-

enantiomero de metalaxyl)0.010 Phenyl valerate 0.010 Sulfotep 0.005

Mepanipyrim 0.010 Phenthoate 0.005 Sulfosulfuron 0.005

Metazachlor 0.005 Phorate-sulfone 0.005 Sumithrin 0.020

Metamitron 0.005 Phorate 0.010 Sulfoxaflor 0.005

Methabenzthiazuron 0.005 Phosalone 0.010 Tebufenozide 0.005

Metconazole 0.005 Phorate-sulfoxide 0.005 Tebuconazole 0.010

Methidathion 0.005 Phoxim 0.010 Tebutam 0.005

Methamidophos 0.005 Phosphamidon 0.005 Tebufenpyrad 0.010

Triflumizole 0.005

Trifloxystrobin 0.005

Trietazine 0.005

Tricyclazole 0.010

Report Date 2018-10-15 Page 6 of 7 Revision: AR272-TS-61


Lowest Calibration Level per analyteAnalyte LCL (ppm) Analyte LCL (ppm) Analyte LCL (ppm) Analyte LCL (ppm)

Endosulfan I (alpha isomer) 0.010

2,3 dihydro-2,2dimethylbenzofuran 0.020 Butocarboxim-sulfoxide 0.005 Cyproconazole 0.005 Endosulfan II (beta isomer) 0.0102, 4-D Methyl ester 0.010 Butocarboxim* 0.010 Cypermethrin a (Zeta- 0.010

Endosulfan sulfate 0.010

3,4 Dichloroaniline 0.010 Butylate 0.020 Cyromazine 0.005 Endrin 0.0102,6 Dichlorobenzonitrilo 0.010 Buturon 0.005 Cyprodinil 0.010

Epoxiconazole 0.005

Abamectin 0.005 Carbaryl 0.010 DDD-p,p 0.010 Esfenvalerate + Fenvalerate* (**) 0.0103-Hydroxy carbofuran 0.005 Captan 0.010 DDD-o,p 0.010

Etaconazole (Etaconazole I y II) 0.010

Acetamiprid 0.005 Carbetamide 0.005 DDE-p,p 0.010 Ethalfluralin 0.010Acephate 0.005 Carbendazim 0.005 DDE-o,p 0.010

Ethiofencarb 0.005

Acrinathrin 0.020 Carboxin 0.005 DDT-p,p 0.010 Ethiofencarb-sulfone 0.005Acetochlor 0.005 Carbofuran 0.010 DDT-o,p 0.010

Ethirimol 0.005

Aldicarb 0.005 Chinometionate 0.010 Deltamethrin 0.010 Ethoprop 0.010Alachlor 0.005 Carfentrazone ethyl 0.005 DEET (Diethyl-m-toluamide, N,N-) 0.010

Ethylan 0.010

Aldicarb-sulfoxide (Aldoxicarb) 0.005 Chlorbromuron 0.005 Demeton S 0.010 Etion 0.010Aldicarb sulfone 0.005 Chlorantraniliprole 0.005 Demeton O 0.010

Etofenprox 0.010

Ametoctradin 0.005 Chlordimeform 0.010 Desmedipham 0.005 Etoxazole 0.005Aldrin 0.010 Chlordane- a 0.010 Demeton-s-methyl-sulfone 0.005

Famoxadone 0.010

Aminocarb 0.005 Chlorfenvinphos 0.005 Dialifos 0.005 Fenamiphos 0.005Ametryn 0.010 Chlorfenapyr 0.010 Desmetryn 0.010

Fenarimol 0.005

Atrazine-2-hydroxy 0.005 Chloridazon (Pyrazon) 0.005 Dichloran 0.010 Fenazaquin 0.005Atrazine 0.010 Chlorfluazuron 0.005 Diazinon 0.010

Fenbuconazol 0.005

Azinphos-ethyl 0.005 Chlorobenzilate 0.010 Diclobutrazol* 0.010 Fenbutatin oxide* 0.010Azamethiphos 0.005 Chlormequat 0.005 Dichlorvos 0.010

Fenchlorphos 0.010

Azoxystrobin 0.010 Chloropropylate 0.010 Dicrotophos 0.005 Fenfuram 0.005Azinphos-methyl 0.010 Chloroneb 0.010 Diclofop methyl 0.020

Fenhexamid 0.005

Benalaxyl 0.010 Chlorotoluron 0.005 Diethofencarb 0.005 Fenitrothion 0.020Baycarb 0.005 Chlorothalonil 0.010 Dieldrin 0.010

Fenoxaprop-ethyl 0.005

Bensulfuron-methyl 0.005 Chlorpropham 0.010 Difenoxuron 0.005 Fenoxycarb 0.005Bendiocarb 0.005 Chloroxuron 0.005 Difenoconazole 0.005

Fenpropathrin 0.010

Benzoximate 0.005 Chlorpyrifos methyl 0.010 Dimefuron 0.005 Fenpropidin 0.005Bensulide 0.005 Chlorpyrifos 0.010 Diflufenican 0.005

Fenpropimorph 0.005

BHC lindane beta 0.010 Chlortal dimethyl 0.010 Dimethachlor 0.005 Fenpyroximate 0.005BHC lindane alpha 0.010 Chlorsulfuron 0.005 Dimepax 0.010

Fenson 0.020

BHC lindane gamma 0.010 Clodinafop-propargyl 0.005 Dimethoate 0.010 Fensulfothion 0.010BHC lindane delta 0.010 Chlorthiophos 0.020 Dimethenamid 0.005

Fenthion 0.010

Bifenox 0.020 Clomazone* 0.005 Diniconazole 0.005 Fenuron 0.005Bifenazate 0.005 Clofentezine 0.005 Dimethomorph 0.005

Fipronil 0.020

Bitertanol 0.005 Dioxathion 0.010 Flamprop methyl 0.010Bifenthrin 0.010 Cloquintocet-mexyl 0.005 Dinotefuran 0.005

Flamprop-isopropyl 0.010Coumaphos 0.010

Boscalid 0.005 Disulfoton 0.010 Flazasulfuron 0.005Bolstar 0.010 Diphenamid 0.005Crimidine 0.005

Cyanazine 0.005Flonicamid 0.010

Bromophos methyl 0.010 Cyazofamid 0.005 Diuron (Karmex)* 0.010 Fluazifop-butyl 0.005Bromacil 0.010 Cyantraniliprole* 0.010 Disulfoton-sulfone 0.005

Flubendiamide 0.010Bromuconazole* 0.010 Cyfluthrin 0.010 Dyfonate 0.010 Fluchloralin 0.020Bromopropylate 0.010 Cycloate 0.005 Dodemorph 0.005

Fludioxonil 0.010

Buprofezin 0.010 Cymoxanil 0.005 Emamectin Benzoate 0.005 Flufenacet 0.005

Bupirimate 0.005Cyhalothrin (Isomero Lambda y

gamma)**0.010 Edifenphos 0.005

Analyte LCL (ppm)

Flufenoxuron 0.005 Methomyl 0.005 Piperonyl Butoxide 0.005 Terbumeton 0.005

Analyte LCL (ppm) Analyte LCL (ppm) Analyte LCL (ppm)

Terbuthylazine 0.010

Fluopicolide 0.005 Methoxychlor 0.010 Pirimicarb 0.005 Terbuthylazine-desethyl 0.005

Fluometuron 0.005 Methoprotryne 0.005 Piperophos 0.005

Terbutryn 0.010

Fluoxastrobin 0.005 Metobromuron 0.010 Pirimiphos-methyl 0.005 Terrazole 0.010

Fluoroglycofen-ethyl 0.005 Methoxyfenozide 0.005 Pirimiphos-ethyl 0.005

Tetrachlorvinphos, E-isomer 0.010

Flusilazole 0.005 Metolcarb 0.010 Prochloraz 0.005 Tetradifon 0.010

Flurtamone 0.005 Metolachlor 0.005 Primisulfuron-methyl 0.005

Tetrahydrophthalimide, cis-1,2,3,6-

(THPI)0.010

Fluvalinate 0.010 Metoxuron 0.005 Profenofos 0.010 Tetramethrin 0.005

Flutriafol 0.005 Metosulam 0.005 Procymidone 0.010

Thiabendazole 0.005

Forchlorfenuron 0.005 Metribuzin 0.010 Promecarb 0.010 Thiacloprid 0.005

Folpet 0.010 Metrafenone 0.005 Profluoralin 0.020

Thiocyclam hydrogen oxalate 0.010

Thiamethoxam 0.005

Fuberidazole 0.005 Mevinphos 0.010 Prometryn 0.010 Thidiazuron 0.005

Formetanate 0.005 Metsulfuron-methyl* 0.005 Prometon 0.010

Thifensulfuron-methyl 0.005

g Chlordan 0.010 Mirex 0.010 Propachlor 0.005 Thiobencarb 0.010

Furathiocarb 0.005 Mexacarbate 0.005 Pronamide 0.005

Heptachlor 0.010 Monolinuron 0.005 Propanil 0.005Haloxyfop-methyl 0.005 Monocrotophos 0.005 Propamocarb 0.005

0.005

0.010

Hexaconazole 0.005 Napropamide 0.005 Propiconazole 0.010

Hexachlorobenzene 0.010N-2,4-Dimethylphenyl formamide (2,4-

DMPF)0.010 Propetamphos 0.005

Heptenophos 0.005 Myclobutanil 0.010

Heptachlor exo-epoxide (isomer B) 0.010 Monuron 0.005 Propargite (Omite)

Propazin

Hexythiazox 0.005 Nicosulfuron 0.005 Propyzamide 0.005

Hexazinone 0.010 Neburon 0.005 Propoxur 0.005

Imazapyr 0.005 Norflurazon 0.005 Prosulfuron 0.005

Imazalil 0.005 Nitrapyrin 0.010 Prosulfocarb 0.005

Imidacloprid 0.005 Ofurace 0.005 Pyraclostrobin 0.005

Imazaquin 0.005 Novaluron* 0.010 Pymetrozine 0.005

Indoxacarb 0.010 op Dicofol*** 0.010 Pyridaben 0.005

Imidan 0.010 Omethoate 0.005 Pyrazophos 0.005

Iprovalicarb 0.005 Oxadixyl 0.005 Pyriproxyfen 0.010

Iprodione 0.010 Ovex 0.010 Pyrimethanil 0.005

Isazophos 0.010 Oxydemeton-methyl 0.005 Quinoxyfen 0.005

Irgarol 0.005 Oxamyl 0.005 Quinalphos 0.005

Methiocarb sulfoxide 0.020 Piperalin 0.005 Terbacil 0.010

Linuron 0.005 Pencycuron 0.005 S-Metolachlor 0.005

Methiocarb sulfone 0.020 Picoxystrobin 0.005 Teflubenzuron 0.010

Methiocarb 0.010 Picolinafen 0.005 Tebuthiuron 0.005

0.005

0.005

0.010

0.010

Thiodicarb

Thionazin

Thiophanate-methyl

Tokution

Lenacil 0.005 Penconazol 0.005 Simetryn 0.005

0.010

Kelthane*** 0.010 Parathion 0.010 Sethoxydim* 0.010

Triasulfuron

Triazophos

Kresoxim-methyl

0.005

0.005

0.005

0.010

0.010

0.010

0.010

0.005

0.010

Tolyfluanid

Triadimefon

Triadimenol

0.010

Isoxaflutole 0.010

Tribenuron-methyl

Trichlorfon

Trichloronate

Triclocarban

0.005 Parathion methyl 0.010

Isoprocarb 0.005 Paclobutrazol (Bonzi) 0.005 Rimsulfuron

Paraoxon-methyl 0.005 Sebuthylazine

Simazine

0.005

Isoproturon

Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued res ult only affects the sample received at the facility of Análisis Técnicos S.A. de C.V, therefore it ´s

not responsible for the representation of the result for the total product. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.



ppm = Parts per million = mg/kg Uncertainty = 50 % according to "Method validation and quality control procedures for pesticide residues analysis in food and feed". No. de Documento SANCO/10684/2009. Punto 91

Data corresponding to page 2, page 3, page 4 and page 5

Report Date: 2018-10-15 Page: 7 of 7 Revision AR272-TS-61

End of Report


Additional and complementary information

General Information

1. The customer has five calendar days of issuance of the results**** in order to make any comment or complaint about it, because if not done within this time period will be considered this

report has been accepted.

2. Samples may be disposed within 5 days after the issue of results**** only samples for microbiological analysis shall be discarded 24 hours after being received

3. The information recorded in this "Report test results" is treated with strict adherence to privacy notice Análisis Técnicos S.A. de C.V complying with Articles third transient, 16 and 17 of Law

Protection Federation Personal Data Held by Private Parties, in order to regulate their treatment legitimate, controlled and reported, in order to ensure privacy and the right to self-determination

informative individuals.

4.Análisis Técnicos S.A. de C.V not have the authority, or the right to deny, accept or approve cuts or harvests.

5. Análisis Técnicos S.A. de C.V. is not accredited in sampling.

6. MRLs of the countries are a reference data, requesting check the official sites of each country and that can be changed or modified.

7. The result represents the sample that was received on the premises of Análisis Técnicos S.A. de C.V , which is not responsible for the representation of the result for the total product

8. This form of interpretation is protected and registered with the Instituto Nacional del Derecho de Autor (INDAUTOR), likewise, logos and Agrolab name and its subsidiaries are registered with

the Instituto Mexicano de la Propiedad Intelectual (IMPI). Reproduction is prohibited in whole or in part, for any purpose other than the interpretation of results, without permission.

9. This report is not valid if you have scratches, erasures or amendments.

10. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.

11. Análisis Técnicos S.A. de C.V. It is not responsible for updating the MRL's because they are considered as a piece of information. It is your responsibility to review the report LMR official

sites for each country since the information can be changed or modified.

12. The detection of the pesticide residue above the quantification limit is reported as ppm (mg / kg), below the limit of quantification reported as <LCL ppm (mg / kg) and below the LD is

considered as undetermined.

13.The decision rule does not include uncertainty.

**** The issuance of the results includes the final report in PDF format. Delivering results to the client, is subject to confirmation of payment.


References

International Maximum Residue Level Database

http://www.mrldatabase.com/

EU Pesticides Database

http://ec.europa.eu/sanco_pesticides/public/index.cfm

Electronic Code of Federal Regulation

http://ecfr.gpoaccess.gov/cgi/t/text/text-idx?

Health Canada

http://pr-rp.hc-sc.gc.ca/mrl-lrm/index-eng.php

Normas Alimentarias FAO/OMS

http://www.codexalimentarius.net/pestres/data/pesticides/search.html

Positive List System for Agricultural Chemical Residues in Foods (Japón)

http://m5.ws001.squarestart.ne.jp/foundation/search.html

1. The laboratory Análisis Técnicos S.A. de C.V. is accredited before EMA, in the test of determination of residues of pesticides in fruits, vegetables, agricultural food and seeds (incorporating

QuEChERS extraction), by GASS CHROMATOGRAPHY / MASS / MASS to the ISO / IEC 17015:2005.

2. The laboratory Análisis Técnicos S.A. de C.V. is accredited before EMA, in the test of determination of residues of pesticides in fruits, vegetables, agricultural food and seeds (incorporating

QuEChERS extraction), by LIQUID CHROMATOGRAPHY / MASS / MASS to the ISO / IEC 17015:2005.

3. * = Analyte not declared in the scope accredited and / or licensed accredited obtained by method and / or authorized.

4.Authorized use of the pesticide in the relevant country code specified in ISO 3166-1 alpha-2. RML for each country are indicated in the same results table.

5. If no pesticide was detected a green band is shown. If a pesticide was detected within the allowed limits a yellow band is shown. If a pesticide was detected outside of the allowed limits a red

band is shown. If a forbidden pesticide was detected a red band is shown.

6. The colored bands are visual aids based on MRLs of each country and are not a result.

7. ** = The MRL of Isomero Lambda is taken for the molecule Cyhalothrin (Isomero Gamma and Lambda), for Cypermethrin a (Zeta-Cypermethrin) the MRL for Zeta-Cypermethrin is taken and

for the MRL for Esfenvalerate + Fenvalerate, the one for Esfenvalerate is taken.

8. 2 =For Canada the MRL of 0.1 ppm default is considered according to the point 5.2.1.4.2 Food and Drug Regulations of the Canada Food Inspection Agency

http://www.inspection.gc.ca/food/meat-and-poultry-products/manual-of-procedures/chapter-5/eng/1395150894222/1395150895519?chap=2.

9. *** = Dicofol MRL is the sum of p, p-dicofol and o, p-dicofol.

10. The color bands of each molecule are visual support based on the MRLs of each country and do not represent a result.

Information corresponding to page 5 and 6

1. In the corresponding table it´s represented the lower calibration poing (LCL).

2.The correspondig table is NOT A RESULT. It represents quality information data.

3. Uncertainty = 50 % according to "Method validation and quality control procedures for pesticide residues analysis in food and feed". No. de Documento SANCO/10684/2009. point 91

Glosario

GC/MSMS = Gass/Mass/Mass AGILENT 225/MS, 240/MS

LC/MSMS = Liquid/Mass/Mass QQQ (AGILENT 6460)

LCL = Lowest Calibration Level

MRL = Maximum Resuide Limits

ppm = Parts per million = mg/Kg

SD = No Data

Traces = < 0.010 ppm.

MX= Mexico

US= United States

JP= Japan

CA= Canada

EU= European Union

KOR= Korea

CHN= China

Maximum Residue Limits (MRLs) for Blackberry listed in The Official Catalog of Mexico

Pesticide 2004.

Maximum Residue Limits (MRLs) for Blackberry indicated in Environmental Protection

Agency (EPA) United States.

Maximum Residue Limits (MRLs) for Blackberry indicated in Electronic Code of Federal

Regulations (e-CFR TM) United States.

Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued result only affects the sample received at the facility of Análisis Técnicos S.A.

de C.V, therefore it´s not responsible for the representation of the result for the total product. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.

This form of interpretation is protected and registered with the Instituto Mexicano de la Propiedad. Its total or partial reproduction without authorization is prohibited. This report will not be valid if you have scratches, erasures or amendments.



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