desodorantes _3

7/21/2019 desodorantes _3

1/14

Sect ion I

A nt ipersp iran ts and

Deodorants


2/14

2

Cosmetic and Toiletry Formulations

Antiperspirant Lot ion

Th is formu lat ion is des igne d for roll -on con tainers.

I n g r e d i e n t s :

w / w

1 . D i s t i l l e d Water t -4 2 .5 0

2 . Veegum 1 . 2 5

3 . R i t a p r o 165 7 . 5 0

4 . R i t a c h o l 2 . 0 0

5 . L a n e t o 100 1 . o o

6 . P r o p yl e n e G l y c o l 3 . 7 5

7 . R i t a c h l o r ( 5 0 ) 4 2 . 0 0

8 . Fra g ra n c e

Q S

Compounding Procedure:

Weigh and add i tem 1 i n t o a c o n ta i n e r a nd b eg in s t i r r i n g . A

v a r i a b l e speed p r o p e l l e r - t y p e s t i r r e r i s recommended. Add i t e m

2 and s t i r u n t i l d i s p e r s i o n i s co m pl e t e . Weigh a nd add i t e m s 3 ,4

and 5 i n t o a n o th e r c o n t a i n e r . Be g in s t i r r i n g and h e a t in g t h i s

b l e n d t o 70-73C. H eat t h e w a t e r - c o n t a i n i n g b l e n d

t o

70-73C.

When b o t h b l e n d s a re a t 7 0-73C, a dd t h e L a n e t o 1 0 0 - c o n t a i n i n g

b le nd t o t h e w a t e r b l en d . C on ti n ue s t i i r i n g w i t h an a g i t a t o r

s i m i l a r t o t h e one d es c r i b e d above. When a l l t h e L a ne to

100-

c o n t a i n i n g b l e n d ha s been added b e g i n c o o l i n g t h e b a t c h . C oo l

t o 40-43C a nd ad d t h e r e m a i n i n g i n g r e d i e n t s . Pac ka ge a t 2 5-3OC.

Formula t ion HB-89-L-30

Rol l-On Ant iperspirant


1 . H y dr ox y pr op y l M e t h y l c e l l u l o s e

2 . SD A l c o h o l 4 0

3 . L a n e t o 5 0

4 . P a t i o n i c I S L

5 . D i s t i l l e d Water

6 . R i t a c h l o r

7 , C o l o r , F ra gr an ce , P r e s e r v a t i v e s

w / w

0 . 6 5

20 I O 0

4 . 0 0

2 . 0 0

t - 5 3 . 3 5

20 .00

QS


Add t h e a l c o h o l s o l u t i o n t o t h e w at er s o l u t i o n s l o w l y w i t h

g e n t l e s t i r r i n g . Add re ma in in g i n g r e d i e n t s s l o w l y w i t h

g e n t l e s t i r r i n g .

D i s pe r s e i t e m

1

i n t o 2; a dd i t e m 4 . Com bine i t e m s 3 a nd

5 .

Formula t ion HB-89-L-31

SOURCE; R I T A C o r p : S u g g e s t e d F o r m u l a t i o n s


3/14

ntiperspirants and Deodorants

3

Ant iperspirant St ick

I n n r e d i e n t

:

Methy l S te a ro xy D imeth i con e Mas i lwax 135

Cyc lometh i cone M a s i l SF-V

POE 6000 D i s t e a r a t e Mapeg 6000DS

PEG-32 Mac ol E1450

T a l c S u p r a

A 1

Z r T e t r a c h l o r h y d r e x G l y R ez al 36GP

Fra g ra n c e

S t e a r y l A l c o h o l

CO-

1895

Wt.4/o

3 . 0

4 5 . 5

3 . 0

2 . 0

2 4 . 0

2 . 0

2 0 . 0

0 . 5

Appearance: W hi te , u n i f o r m s t i c k . E x c e l l e n t a p p l i c a t i o n

M e l t P o i n t : 52C

O b s er va t i on : S i g n i f i c a n t l y l e s s sy ne re s i s vs . s i m i l a r s t i c k s

p r o p e r t s .

w i t h o u t Masi l w a x .

P ro c e d u re :

65C ( 1 5 0 F ) . Keep b a t c h c o v e r e d t o a v o i d S i l i c o n e l o s s . Add

S t e a ry l A l c o h o l . When u n i f o rm , add t a l c a nd Re za l 36GP. M i x

w i t h good shear u n t i l t h e s o l i d s a r e u n i f o r m l y d i s p er s ed . Cool

t o 55C ( 130F) , add f r a g ra n c e , a nd

f i l l .

C h i l l s t i c k s a t 5C

(40-45F) t o speed s o l i d i f i c a t i o n .

SOURCE:

PPG

I n d u s t r i e s , I n c . : F o r m u l a t io n Q-101

He at M a s i l wa x , M a s i l S F - V , Mac ol E1450 and Mapeg 6000DS t o

An tipersp i rant G el

T h i s p ro d uc t i n g e l f o r m w i l l s e r v e a s

a

m o i s t u r i z e r f o r t h e

s k i n w i t h e f f e c t i v e a n t i p e r s p i r a n t a c t i o n .

I t w i l l

h e l p t o e n su re

t h a t t h e a c t i v e i n g r e d i e n t s t a y s i n u n i f o r m s us pe ns ion d u r i n g

p r o c e s s i n g and c o o l i n g .

Lexquat AMG-0

L i p o c o l

0 20

AZG-368 So l u t i on

(w/w)

35 .00

3 5 . 0 0

30 .00

Pro c e d u re :

C ha rg e b a t c h v e s s e l w i t h L e xq u at AMG- 0 . B e g i n m i x i n g a n d

h e a t i n g t o 65C. S l o w l y ad d t h e AZG-368 w i t h s l o w m i x i n g . When

c o m p l e t e l y m ix ed , a dd t h e L i p o c o l 0-2 0 ( p r e v i o u s l y m e l t e d ) .

M i x u n t i l u n i f o r m . C ool t o 40C. Pour i n t o c o n t a i n e r a nd c o o l

t o 25C.

SOURCE: I n o l e x C h e m i c a l Co. F o r m u l a t i o n A D - 1 0 0


4/14

4


Clear Rol l -On Ant iperspirant

T h i s aqueous s ys te m c o n t a i n s s u f f i c i e n t e t h a n o l t o d r y q u i c k -

l y on t h e s k i n ; once d r y , i t i s n o n - ta c k y. The u se o f L an et o 1 0 0

r ed uc es t h e u s ua l t a c k i n e s s

o f

t h e a1 umi num a n t i p e r s p i r a n t

a c t i v e g re d i e n t s ,

I n s r e d i e n t s :

P a r t A :

1 . C e l l o s i z e

QP

4 4 0 0

2 .

D i s t i l l e d Water

P a r t B :

3 . B e nz et ho ni um c h l o r


5 . A l c o h o l S 40

6 . L a n e t o

50

P a r t C :

7 . R i t a c h l o r 5 0

e

W / W

0 . 2 0

2 9 . 7 0

0 . 1 0

8 . 0 0

2 0 . 0 0

7 . 0 0

35 I O 0

Compounding Procedures:

P r e p a r e P a r t

A

i n advance, t o a l l o w t h e gum t o h y d r a t e f u l l y

b e f o r e i n c o r p o r a t i o n i n t o t h e p r o d u c t . S lo w ly a dd P a r t B t o

P a r t A a t room t e m p e ra t u r e w i t h h i g h speed p r o p e l l e r a g i t a t i o n .

F i n a l l y , s l o w l y add Phase

C

w i t h h i g h speed s t i r r i n g . Perfume,

i f

any , i s added t o P a r t B .

Formu l a t n 101 1 32/HB-89-1-19

Antiperspirant Lot ion

The l o t i o n a n t i p e r s p i r a n t has been an a t t r a c t i v e f o r m u la

o v er t h e y e ar s , due t o i t s v e r s a t i l i t y and va r i o u s a p p l i c a t i o n s .

n q r e d i e n t s :

1 . R i t a p r o 200

2 . L a n e t o 5 0

3 .

M i n e r a l

O i l

( 65 /7 5 V i s c o s i t y )

4 . R i t a c h l o r 50%

5 .

D i s t i l l e d W ater

W / W

4 . 6 0

8 . 8 0

9 . 0 0

40 .00

3 7 . 6 0


and Laneto 50 and mi x t o f o r m e m u l s i o n . When c o o l , add R i t a c h l o r

5 0

s l o w l y . C on t i nu e m ix i n g u n t i l c om p l et e.

M e l t R i t a p r o 2 0 0 and m i n e r a l o i l a t 75C. Add p r e h e a te d w a t e r

Formula t ion 101-131/HB-89-L-20

SOURCE: R . 1 , T . A .

C o r p , : S u g g e st e d F o r m u l a t i o n s


5/14


1 .

SD A l c o h o l 4 0

2 . P r o p y l e n e G l y c o l

3 . Lane to 50

4 . G r i l l o c i n HY-77

5 . Me thy lpa raben

6.

Perfume

7. D i s t i l l e d Water

Antiperspirants and Deodorants

Deodorant Cologne

w /w

60 . 00

3 . 0 0

2 . 0 0

3 . 0 0

0 . 1 5

QS

31 .85


and wa rm in g. Warm t h e A l c o h o l t o 50-55C and ad d a l l o f t h e

i n g r e d i e n t s

W I T H

THE E X C E P T I O N OF THE PERFUME. S t i r u n t i l a

homogeneous b l e n d r e s u l t s . B e gi n c o o l i n g t h e b l e n d , w h i l e

s t i r r i n g c o n t i n u o u s l y . Cool t o 40-43C and add t h e r e m a i n i n g

i n g r e d i e n t s . Cool t o 25-30C w h i l e s t i r r i n g c o n t i n u o u s l y .

Package f 1 t o s u i a b 1e c o n t a i n e r s ,

N O T E : E x p l o s io n p r o o f

m i

x i ng and hand1 g equipment sho ul d

Weigh and add t h e A l c o h o l i n t o a c o n t a i n e r and b e g i n s t i r r i n g

be used .

Formula t ion H-89-G-4

Deodorant Spray (Pump Dispensing)

T h i s f o r m u l a t i o n combines d eo do ra nt , a n t i - m i c r o b i a l e f f e c t s

and a p l e a s a n t f r a g r a n c e . G r i l l o c i n HY-77 h as good d e o d or a n t

p r o p e r t i e s t h a t e l i m i n a t e t h e p res en ce and p e r c e p t i o n o f

u n p l ea s an t o d or . T h i s p r o d uc t i s de s ig n ed f o r p a ck a gi ng i n t o a

c o n t a i n e r f i t t e d w i t h a pump.

I n q r e d i e n t s :

1. SD A l c o h o l 4 0

2. G r i l l o c i n HY-77

3 . L a n e t o

50

4 . T r i c l o s a n

5 . F r a g r a n c e

6 .

C o l o r

w /w

92 .90

5 . 0 0

2 . 0 0

0 . 10

QS

QS


m i x i n g e q u ip m e n t s h o u l d b e e q u i p p e d s o t h a t i t i s e x p l o s i on

p r o o f . S t i r u n t i l a u n i f o r m d i s p e r s i o n r e s u l t s . Package f i l l

i n t o s u i t a b l e c o n t a i n e rs .

Weigh and add a l l i n g r e d i e n t s i n t o a s u i t a b l e c o n t a i n e r .

A l l


SOURCE: R. I .T .A . Co rp . : Sug ges ted Fo rm ul a t io ns


6/14

6 Cosmetic and Toiletry Formulations

Deodorant Stick Without Alcohol

A

s t i c k f o r m u l a w hi ch c ombats od or and i n h i b i t s o do r d e v e l-

opment.

I n s r e d i e n t s : w /w

1 . D i s o rb e n e

2 . 5 0

2 . De hyd rol LS 3 4.0 0

3 .

PEG

200 2 0 . 0 0

4 . D i p r o p y l e n e gl y c o l 5 0 . 0 0

5 .

1 , 2 P r o p y l e ne g l y c o l 10.00

6.

G r i l l o c i n

CW 90

1 . 5 0

7 . FD&C B l ue #1 (1% i n H20

0 . 0 5

8. Per fume QS

9 . D i s t i l l e d Water 1 1.9 5


e n e g l y c o l b y h e a t i n g and m i x i n g ( a b o ut 85 C) . Add G r i l l o c i n CW 90

and Dehydro l L S

3 .

S t o p h e a t i n g . Add w a t e r a nd c o o l t o a b o ut

70C. Add p er fu m e a nd c o l o r i n g a g e n t . P ou r i n f i n a l p a c k ag i n g a nd

c o o l down u n t i l room t e m p e r a t u r e .

S O U R C E : R . I . T . A . C o r p . : F o r m u l a t i o n 11 1-1 85

Antiperspirant Cream

D i s s o l v e D i sorbene PEG

2 0 0 ,

D i p r o p y l e n e g l y c o l and P r o p y l -

M i n e r a l o i l

1 0 . 0 %

I o n o l

C . P .

a n t i o x i d a n t ) P a r t A 0 . 1 %

Monamid 150-1s

1

2 . 0

C hl o r h y d r o l

50

)

40 .0%

Monawet SNO-35 ) P a r t

B 1 . 4

Water , de i on i zed

1

46 .5%

M i x P a r t A a n d P a r t

B

s e p a r a t e l y , i n t h e o r d e r l i s t e d , t h e n

a d d Pa r t B t o P a r t A w i t h r a p i d m ech an ica l s t i r r i n g . T h i s cream

i s a heavy, w a t e r - i n - o i l e m ul s i on w h ic h has e x c e l l e n t s t a b i l i t y .

SOURCE:

Mona I n d u s t r i e s , I n c . : S u gge ste d F o r m ul a t i o n

An t iperspi rant G el

T h i s p r o d u c t i n g e l f o r m w i l l s e rv e as a m o i s t u r i z e r f o r t h e

s k i n w i t h e f f e c t i v e a n t i p e r s p i r a n t a c t i o n .

I t

w i l l h e l p t o en sure

t h a t t h e a c t i v e i n g r e d i e n t s t a y s i n u n i f o r m su sp e n s io n d u r i n g

p r o c e s s i n g and c o o l i n g .

(w/w)

Lexquat AMG-0

3 5 . 0

L i p o c o l 0 -2 0 3 5 . 0

AZG-368 S o l u t i o n 30 .0

Pro c e d u re :

Cha rg e b a t c h v e s s e l w i t h L e x q ua t AMG-0. Be g i n m i x i n g a nd

h e a t i n g t o 65C. S l o w l y add t h e AZG-368 w i t h s l o w m i x i n g . When

c o m p l e t e l y mi xe d, add t h e L i p o c o l 0-20 ( p r e v i o u s l y m e l t e d ) .

M i x u n t i l u n i f o r m . C ool t o 40C. Pour i n t o c o n t a i n e r a nd c o o l

t o 25C.

SOURCE: I n o l e x C h e m i c a l Co.

:

Formula t ion AD-100


7/14

Antiperspirants and Deodorants 7

Deodorant

Stick

The d e od o ra n t s t i c k i s d e s ig n e d t o b e d i sp e n se d by p u s h i n g

up a m ov able b o t to m p l a t e o r b y r o t a t i n g a s c r e w - l i k e m echanism .

The f o r m u l a t i o n w h i c h c an b e p l e a s a n t l y s c en t ed , c r e a t e s a c o o l -

i n g s e ns a t io n due t o t h e e va p o ra t i on o f v o l a t i l e s o l v e n t .


1 .

SD Alcoho l 40

2 . P r o p y l e n e G l y c o l


4 . P a t i o n i c I S L

5 . Sodium S t e a r a t e C-7


7 . C o l o r , F r a gr a n ce


i n g r e d i e n t s 6 and 3. M i x u n t i l u n i f o r m . C oo l t o 60C. Add

r em a i n in g i n g r e d i e n t s . F i l l a t 5%.

Com bine i n g r e d i e n t s 1 , 2 , 4 and

5 ;

t h e n h e a t t o 7 0C. Add


w /w

6 2 . 2 5

1 5 . 0 0

3 . 0 0

1 . 7 5

8 . 0 0

10.00

QS

Deodorant Cream

G r i l l o c i n PY-88 h as good d eo do ra nt p r o p e r t i e s t h a t e l i m i n a t e

t h e p r es e nc e and p e r c e p t i o n o f u n p l e a s a n t o d o r s .

I n a r e d i e n t s :

P a r t A :

1 . R i t a GMS

2 . I s o p r o p y l M y r i s t a t e

3 . R i t a CA

4. R i t a c e t - 2 0

5 .

G r i l l o c i n PY 88 P e l l e t s

6 .

Beeswax

P a r t

B :

7 . D i s t i l l e d W ate r (9OC)

P a r t

C :

8 . P a t l a c LA

9 . Perfume

10 .Euxy l K 400

w /w

4 . 0 0

4 . 0 0

2 . 7 0

2 . 0 0

2 . 0 0

1 . 0 0

83.75

0 . 2 0

0 . 20

0 . 1 5


H e a t P a r t A up t o 80C. S t i r h o t w at er i n t o P a r t A . Add the

o t h e r i n g r e d i e n t s a t 35C.

Fo r m u l a t i on 1 11-162

SOURCE:

R . I . T . A . C o r p . : S u g ge s te d F o r m u l a t i o n s


8/14

8 Cosmetic

and

Toiletry Formulations

Deodorant Stick

T h i s p r o d u c t i s a s o l i d s t i c k d eo d o ran t f o r use i n a c y l i n d -

r i c a l d i s pe ns ng c o n t a i n e r . I t a p p l i e s e a s i l y and sm o o th l y,

d r i e s q u i c k l y and o f f e r s e x c e l l e n t de o d o ran t c h a r a c t e r i s t i c s .

G r i l l o c i n HY- 7 h as been i n c l u d e d b eca use o f i t s u n i q u e o d o r -

r e m o v i n g a b i

1

t y .


1 .

SD

A l c o h o l

3 . T r i c l o s a n

2 . PEG-8

4


5 . Sod ium S te a ra te C-7


7 . C o l o r

8 . F r a g r a n c e

w /w

70 .90

1 0 . 0 0

0 .10

3.50

7 . 5 0

8 . 0 0

QS

QS


Weigh and add i n g r e d i e n t 1 i n t o a c o n t a i n e r and b e gi n s t i r -

r i n g and h e a t i n g . A l l h e a t i n g and s t i r r i n g e qu ip men t s ho u ld b e

e q u i p p e d so t h a t

i t

i s e x p l o s i o n p r o o f .

A

v a r i a b l e s peed a g i t -

a t o r e qu ip pe d w i t h a p r o p e l l e r - t y p e s t i r r e r i s recommended.

Weigh and add i n g r e d i e n t 5 (S od iu m S t e a r a t e C-71, s t i r r i n g

c o n t i n u o u s l y w h i l e c o n t i n u i n g t o h e a t. Weigh and add i n g r e d i e n t s

2, 3,

4

and 6 and c o n t i n u e s t i r r i n g and h e a t i n g . H ea t t o a pp ro x-

i m a t e l y 55-60C u n t i l a l l t h e S odium S t e a r a t e C-7 i s m e l t ed .

A f t e r t h e S t e a r a t e i s m e l t ed and t h e p r o d u c t i s u n i fo rm ,

b e g i n c o o l i n g t h e b a t c h . C oo l t o a bo u t 55-6OC. Package i n t o

s u i t a b l e c o n t a i n e r s . The c o n t a i n e r s w i l l have t o b e p l ac ed i n

m olds t o a ccomodate s u f f i c i e n t s t i c k mass t o a l l o w f o r s h r i nk a ge .


Glycerin-Based Deodorant Gel


1 . P a t i o n i c S S L

2 .

G l y c e r i n


4 .

S t e a r i c A c i d

5 . Sodium Hy dro x id e (18% S o l u t i o n )


7 , C o l o r , F r ag r an c e, P r e s e r v a t i v e s

w /w

10.00

73.10

0 . 8 0

+E.

40

+ - 1 . 20

6.50

QS


C o m b i n e i n g r e d i e n t s

1

and

2

and h e a t w i t h m i x i n g t o 65C;

add i n g r e d i e n t 3 . H ea t t o 65C. Add i n g r e d i e n t 4 . M a i n t a i n 6 5 C .

Combine b o t h phases w i t h m i x i n g . C ool w i t h s t i r r i n g ' t o 50C and

a dd re m a i n i ng i n g r e d i e n t s . F i 11 i n t o p ro p e r c o n t a i n e r s . M i x

w h i l e f i l l i n g .

SOURCE: R . I . T . A . C o r p .: S u gg e st e d F o r m u l a t i o n s



9/14


Liquid Ant iperspirant Emulsion

L i q u i d a n t i p e r s p i r a n t s have been a t t r a c t i v e fo rm u l as o ve r

t h e y e a r s , due

t o

t h e i r v e r s a t i l i t y and v a r i ou s a p p l i c a t i o n s .


P a r t A :

1 . R i t a p r o 165

P a r t 8 :

2 . Laneto 50

3 . R i t a c h l o r 50%


Pa r t C :

5 .

Perfume

w/w

13 .00

4 . 0 0

40 .00

43 .00

Q S


add w a t er p ha se t o o i l phase. Cool t o 45C. Add per fume.

H e a t P a r t

A

t o 70C. H ea t P a r t B t o 72C. W i t h m i x in g , s l o w l y

F o r m u l a t i o n 1 0 1 - 1 3 3

Stick Deodorant

A sod ium s t e a r a t e s t i c k

which comba

d ev elo pm en t w i t h p r o p y le n e g l y c o l , G r i


1 . S t e a r i c A c i d XXX

2 . SD A l c o h o l 4 0

3 . Sodium H yd ro x id e USP (20% s o l u t i o n

4. P r o p yl e ne G l y c o l


6. Per fume

ComDoundina Procedure:

w a t e r )

s

o do r and i n h i b i t s o do r

l o c i n and p e rf um e.

w /w

7 . 0 0

41

O O

15 .00

35 .00

2 .0 0

QS

n d i s t i l l e d

Weigh and add i n g r e d i e n t s 1 -2 i n t o a c o n t a i n e r and b e g i n

s t i r r i n g and h e a t i n g . H eat t o 75-78C. Weigh and add i n g r e d i e n t s

4

and

5

i n t o an ot he r c o n t a i ne r and b eg i n s t i r r i n g and h e a t i n g .

Hea t t h e b l e n d o f i n g r e d i e n t s 4 a nd 5 t o 75-78C. When t h e 1 -2

i n g r e d i e n t b l e n d and t h e 4 and 5 i n g r e d i e n t b l e n d a r e b o t h a t

75-78C, add t h e 4 and 5 i n g r e d i e n t b l e n d t o t h e 1-2 i n g r e d i e n t

b l e n d . Add i n g r e d i e n t

3.

M ix u n t i l u n i f o rm . B eg in c o o l i n g w h i l e

s t i r r i n g c o n t i n u o u s l y . A t 60C, add i n g r e d i e n t

6.

Package a t

approx ima te l y 55C.

N o te : E x p l o s i v e p r o o f m i x i n g an d h a n d l i n g e qu ip m en t s h o u l d

be used.

F o r m u l a t i o n H - 8 9 - G - 3

SOURCE:

R . I . T . A .

Co rp . : Su gg e st e d Fo rm u l a t i o n s


10/14

10

Cosmetic

and

Toiletry Formulations

Dry Rol l -On Ant iperspirant-A


Phase A :

C e ty l D ime th i cone ( A b i l Wax 9801)

I s o p r o p y l M y r i s t a t e ( T e g o s o f t M)

Cyc lome th icon e ( A b i l B 8839/DC 344)

Q u a t ern i um 1 8 H e c t o r i t e (Be n to n e 38 Po wd er )

E t h a n o l

-

2 0 0 p r o o f

o r

E t h a n o l

-

1 9 0 p r o o f

Phase :



Phase

C :

A1 umi num C h l o r o h y d r a t e

Phase D :

Perfume

Dry Rol l -On Ant iperspirant-B


Phase A :

C e ty l D ime th i cone ( A b i l Wax 9801)


Cy c l o m e t h i c o n e ( A b i l 8839/DC 344)

Q u a t e rn i u m 1 8 H e c t o r i t e (Be n to n e 38 p owd e r )

E t h a n o l

-

200 p r o o f o r E t h a n o l

-

1 9 0 p r o o f

Phase B :

He x y l L a u ra t e (Hen k e l

-

Standamul

C T A

o r C e t r o l

A )


Phase C :

A l u m i n u m Ch l o ro h y d ra t e

Phase D :

Perfume

w /w

0 . 5 0

5 . 0 0

4 0 . 0 0

2 . 0 0

2 . 0 0

5 . 0 0

20 .50

2 5 . 0 0

QS

w /w

0 50

5 . 0 0

4 0 . 0 0

2 . 0 0

2 . 0 0

3 . 0 0

22.50

2 5 . 0 0

Q.S.

Pro c e d u re :

1 .

Blend A b i l Wax 9801, A b i l

B

8839 and I s o p r o p y l M y r i s t a t e .

S p r i n k l e i n B en to ne 38 pow der, a v o i d i n g lum ps, w h i l e u s i n g

a h i g h sp ee d m i x e r .

2 .

Add E thano l . 19 p r o o f i s p r e f e r r e d .

M i x .

P r o c e s s t h r o u g h

homogenizer w i t h s he ar u n t i l a c l e a r s o f t g e l

o r

c l e a r

medi um v i s c o s i t y 1 u i d f or me d,

3 . M i x Phase 8 . Add A lu min um C h l o r o h y d r a t e . M i x u n t i l u n i f o r m .

Add t o Phase A g e l . M ix /h om og en iz e u n t i l w e l l d i s p e r s e d .

4 . Add per fu me. M ix .

SOURCE:

Goldschmid t Chemica l Corp . : S u g g e s t e d F o r m u l a t i o n s


11/14

Antiperspirants and Deodorants

I

Nonwhitening Ant iperspirant Sol id

A c y c l o m e t h i c o n e / s t e a r y l a l c o h o l s us pe ns oid s o l i d w i t h

n o n o i l y a p p l i c a t i o n and n o n wh i t en in g p r o p e r t i e s p r ov i de d

by

M a s i l 7 5 6 .

P a r t : I n a r e d i e n t s :

W t .

A S t e a r y l A l c oh o l

CO-

1895 22.0

Hydrogena ted Cas to r O i l Cas to rwax 1 . o

G l y c e r y l S t e a r a t e ( an d)

PEG-100 Steara te

Ma zo l 165C 1 . o

T e t r a b u t o x y p r o p y l M e t h ic o n e M a s i l 756 5 . 0

B A1

Z r

Te t r a c h l o r h y d r e x G l y Re za l 36GP 2 0 . 0

T a l c

O l y m p i c T a l c 2 . 0

C

Cy c l o m e t h i c o n e

M a s i l SF-V 49.0

F ra g ra n c e

Q . S .

Pro c e d u re :

B l en d and h e a t t h e p a r t A i n g re d i e n t s t o 65C. When m o l t e n

and u n i f o r m , add t h e p a r t i n g r e d i e n t s w i t h good a g i t a t i o n t o

d i s p e r s e . Add t h e cy c l o m e t h ic o n e , m a i n t a i n i n g t h e t e m p e r a t u r e

a t 60-65C. When un i f o r m , co o l t o 55C and add f r ag ra nc e

i f

d e s i r e d , a n d f i l l . C h i l l t h e s t i c k s a t a pp r ox im a te l y 5C t o

speed s o l i d i i c a t i o n .

Formu la t i on Q-102


A

f i r m ,

u n i f o r m su sp en so id s o l i d w i t h smooth a p p l i c a t i o n ,

n ong re asy a f t e r f e e l , and l e s s w h i t e r e s i d u e .

P a r t : I n g r e d i e n t :

A

Cy c l o m e t h i c o n e

PPG-10 Bu tan edi o l

wt.

M a s i l SF-V 43.0

Macol 57 12 .0

B e n z y l L a u r a t e

Mazon EE-1 3 . 0

B

S t e a r y l A l c o h o l

CO-1895 20.0

Hydrogena ted Cas to r O i l Cas to rwax

2 . 0

C

A1

Z r

T e t r a c h lo r h y d r e x GLY Reza l 36GP 20 .0

F ra g ra n c e

QS

Pro c e d u re :

and u n i f o r m , add t h e p a r t B i n g r e d i e n t s , m a i n t a i n i n g t h e

t e m p er a tu r e and m i x i n g u n t i l d i s s o l v e d . Add t h e a n t i p e r s -

p i r a n t s a l t w i t h good m i x i n g t o wet o u t and s uspend t h e

powder. Cool t o 55C, add f ra g r an ce

i f

d e s i r e d , a n d

f i l l

C h i l l t h e s t i c k s a t 5C t o speed s o l i d i f i c a t i o n .

SOURCE:

PPG

I n d u s t r i e s , I n c . : S ug ge ste d F o r m ul a t i o ns

B l e nd and h e a t t h e p a r t

A

i n g r e d i e n t s t o 65C. When m o l t e n

Formula t ion (1-103


12/14

2



A f i r m , u n i f o r m su sp en so id s o l i d w i t h smooth a p p l i c a t i o n ,

n ong re asy a f t e r f e e l , and l e s s w h i t e r e s i d u e .

P a r t : I n g r e d i e n t

W t .

A

C y c l o m e t h i c o n e

M a s i l SF-V 43 .0

PPG-10 Butanedio l M a co l 57 1 2 . 0

Ben zy l La ur a t e Mazon EE-1 3 . 0

B S t e a r y l A1 coho1 CO-1895 20 .0

Hy d ro g e n a t e d Ca s t o r O i l Ca s t o rwa x 2 . 0

C A1 Z r T e t r a ch lo ro h yd re x GLY Reza l 36GP 20. 0

F r a g r a n c e

QS

P r o c e d u r e :

B le n d and h e a t t h e p a r t A i n g r e d i e n t s t o 65C. When m o l t e n

and u n i f o r m , add t h e p a r t B i n g r e d i e n t s , m a i n t a i n i n g t h e

t e m p e r a t u r e a n d

m i

x i ng u n t i 1 d i s s o lv e d . Add t h e a n t i p e r s p i r a n t

s a l t w i t h good m i x i n g t o we t o u t and suspend t h e p ow de r. C oo l

t o 55C, ad d f r a g r a n c e i f d e s i r e d , a n d f i l l . C h i l l t h e s t i c k s

a t 5C t o speed s o l i d i f i c a t i o n .

SOURCE: PPG I n d u s t r i e s , I n c . : F o r m u l a t i o n

Q-103

Antiperspirant Sol id

M a t e r i a l s :

SF-1 202

SF-96-1 00

S t e a r y l A l c oh o l

C a s t o r Wax 70

T a l c

A r l a c e l 1 65

Aluminum Z i r con ium Te t ra ch l o ro hyd rex -G l y (ZAG)

P a r t / W t ( % )

4 5 . 0

5 . 0

1 9 . 0

3 . 0

4 . 0

2 . 0

2 2 . 0

Pro c e d u re :

1 ) M i x SF1202 and s t e a r y l a l c o h o l .

2) Add

Z A G ,

t a l c and A r l a c e l 165.

3 )

H ea t t o 75C and s t i r w i t h m odera te a g i t a t i o n u n t i l

i s m el t e d.

4 P r e- m el t c a s t e r wax and add t o m i x t u r e as a l i q u i d

f o r 15 m i n u t e s .

5 ) C oo l m i x t u r e t o 55C w i t h c o n t i n u e d m i x i n g and p o u r

c o n t a i n e r . C ool ( a v o i d a i r e nt ra pm en t d ue t o ex ce s

s p e e d s ) .

SOURCE: GE S i l i c o n e s : F o r m u l a t i o n APlOOA

and s t

i n t o

v e m i x

a l l wax

r

ng


13/14


R ol l-On D eodo rant Ant iperspi rant

A r o l l - o n f o r m u l a w hi ch does n o t d r y t a c k y and does n o t

con ta in gums .


1 . R i t a c h o l 1 0 0 0

2. I s o p r o p y l M y r i s t a t e

3. G r i l l o c l n H i-7 7

4. R i t a c h l o r (A lum inu m C h l o r o h y d r a t e 50%)

5 .

S o r b i t o l


7 . Per fume

w /w

5 .00

5 . 0 0

1 .oo

50.00

5 .0 0

34 .00

QS


s t i r r i n g and h e a t i n g t h e b l e n d . H ea t t o 70-73C. Weigh and

add i n g r e d i e n t s 4-6 i n t o a no th er c o n t a i n e r and b e g i n s t i r r i n g

a nd h e a t i n g . H ea t t h e 4 -6 i n g r e d i e n t b l e n d t o 70-73C. Add t h e

4-6 i n g r e d i e n t b l e n d t o t h e 1-3 g r ed i e n t b l e n d whi l e c o n t i n -

u o us ly s t i r r i n g t o e ns ur e good e m u l s i f i c a t i o n . Cool t o 30-35C

and add i n g r e d i e n t 7 . Package a t 25-28C.

Weigh and add i n g r e d i e n t s 1 - 3 i n t o a c o n t a i n e r . B e g in


Deodorant Ant iperspirant St ick

A t r i - f u n c t i o n p r od u ct w h ich u t i l i z e s sodium s t e a r a t e made

i n

s i t u . P re ve nt s p e r s p i r a t i o n , d e l i v e r s f ra g r an ce , c o n t r o l s

o b j e c t i o n a b l e o d or .



2 . R i a c h 1 o r (A1 umi num C h l o rh vd ra te

50 )

w /w

2 . 0 0

50 . 00

3 . S t e a r i c A c i d XXX

7 . 0 0

4 . P r o p y l e n e G l y c o l 2 4 .0 0

5.

D i s t i l l e d Water 5.00

6. Sodium Hy dr ox id e USP (15% s o l u t i o n i n d i s t i l l e d

w a t e r ) 1 2 . 0 0

7 . Perfume QS


Weigh and a dd i n g re d i e n t s

4 , 5

and 6 i n t o a c o n t a i n e r .

Commence s t i r r i n g a nd h e a t i n g t h i s b l e n d . Heat t h e b l e n d t o

70-73C and m a i n t a i n t h i s t e m p e r a t u r e . Combine 1- 3 , m i x t h o r o u g h l y

and add t h i s t o t h e b a t ch . C on t i nu e s t i r r i n g and m a i n t a i n i n g

t h e temp era tu r e a t 70-73C. Cool t o 55-60C. Add pe r fume and

package.

SOURCE R.I.T.A. C o r p . : S u gg e st e d F o r m u l a t i o n s

F o r m u l a t io n H - 8 9 4 2


14/14

4


Sol id St ick Ant iperspirant-A


Lanette 18 DE0

Castorwax MP-80

F l u i d

A P

C y c l o m e t h i c o n e ( A b i l B 8839)

C e t y l D i m e t h i c o n e ( A b i l Wax 9 8 0 1 )

T a l c

Aluminum Z i r c o n i um T e t r a c h l o r o h y d r e x - G l y

F ra g ra n c e

Sol id St ick Ant iperspirant-B


L a n e t t e 1 8 D E 0

Castorwax MP-80

F l u i d AP

C y c l o m e t h i c o n e ( A b i l B 8839)

S t e a r o x y D i me th i co n e ( A b i l

Wax

2434)

T a l c

A1 umi num Z i r c o n i um Te t ra c h l o ro h y d r e x - G l y

F ra g ra n c e

Solid Stick Antiperspirant C

I n g r e d i e n t :

Lanet te 18 DE0

Castorwax MP-80

F l u i d AP

C y c l o m e t h i c o n e ( A b i l

B

8839)

C e t y l D im e th ic on e ( A b i l

B

9801)

S t e a r o x y D i meth i cone (A b i 1 Wax 2434)

T a l c

A 1 umi num Z i r c on i um T e t ra ch l o rohydrex -G1 y

F ra g ra n c e

w / w

1 5 - 0 0

4 . 0 0

1 . 5 0

51 - 5 0

0 . 5 0

5 . 0 0

22 .00

0 . 5 0

w / w

1 5 . 0 0

4 . 00

1 . 5 0

51.50

0 .50

5 . 0 0

22.00

0 .50

w / w

15 .00

4 .00

1 . 50

51 .50

0 . 2 5

0 . 2 5

5 . 0 0

22 .00

0 . 50

Pro c e d u re :

1 . Add t h e C y c l o m et h ic o n e t o a c o v e re d m i x i n g t a n k e q ui pp e d

2 . Add t h e F l u i d A P , L a n e t t e , C a st or w ax and A b i l w axe s. B r i n g

w i t h a t u r b i n e p r o p e l l e r . Be g in h e a t i n g .

t e m p e r a t u r e t o 85-87C . H o l d

30

m i nu te s a t t em p er a tu r e w h i l e

m i x i n g.

75C d u r i n g a d d i t i o n . M a i n t a i n t e m p er a tu r e a t 80-85C w h i l e

m i x i n g f o r 10-15 m i n u t e s .

4 . Add t h e A luminum-Z i rcon ium Comp lex. Do no t a l l o w t h e tempera -

t u r e t o d r o p b el ow 70C d u r i n g a d d i t i o n . M i x f o r 15-20 m in -

u te s a t 175-18OC.

3 . Add t h e T a l c . Do n o t a l l o w t h e t e m p e r a tu r e t o d r o p b e lo w

5 . C oo l w h i l e m i x i n g t o 60-62C. Add f r a g r a n c e .

6 . D is pe ns e t o c o n t a i n e r s a t 58-61C.

SOURCE: G o l d s c h m i d t Ch em ic al C o rp . : Su g g e st e d Fo rm u l a t i o n s

desodorantes _3

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Transcript of desodorantes _3